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公开(公告)号：US06252111B1
公开(公告)日：2001-06-26
申请号：US09504113
申请日：2000-02-15
IPC分类号： C07C30334
CPC分类号： C07C303/40 , C07C311/48
摘要： The invention relates to a method for producing a sulfonimide or its alkali metal salt. The method includes the steps of (a) reacting a precursory salt of the sulfonimide with a base contained in a basic aqueous solution, thereby producing a first aqueous solution containing the alkali metal salt and an amine; (b) removing the amine from the first aqueous solution to obtain a second aqueous solution containing the alkali metal salt; and (c) crystallizing the alkali metal salt in the second aqueous solution. The base is potassium hydroxide, sodium hydroxide or lithium hydroxide. The base is added to the second aqueous solution to generate the crystallization. The precursory salt is formed when the sulfonimide is reacted with a tertiary amine or a heterocyclic amine. The alkali metal salt is produced easily and economically in an industrial scale production with high purity and high yield.
摘要翻译： 本发明涉及磺酰亚胺或其碱金属盐的制备方法。 该方法包括以下步骤：（a）将磺酰亚胺的前体盐与碱性水溶液中所含的碱反应，由此制备含有碱金属盐和胺的第一水溶液; （b）从第一水溶液中除去胺，得到含有碱金属盐的第二水溶液; 和（c）使第二水溶液中的碱金属盐结晶。 碱是氢氧化钾，氢氧化钠或氢氧化锂。 将碱加入到第二水溶液中以产生结晶。 当磺酰亚胺与叔胺或杂环胺反应时，形成前体盐。 碱金属盐在高纯度和高产率的工业规模生产中容易且经济地生产。
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公开(公告)号：US5723664A
公开(公告)日：1998-03-03
申请号：US525439
申请日：1995-09-07
IPC分类号： C07C303/38 , C07C311/09 , C07C311/48 , C07D213/20
CPC分类号： C07D213/20 , C07C303/38
摘要： The invention relates to a method of preparing a sulfonimide, a first salt thereof, or a second salt thereof. The method includes the step of: (a) reacting one or two sulfonyl fluorides with nonhydrous ammonia and an amine component which is one of a tertiary amine and a heterocyclic amine, so as to prepare the first salt. Alternatively, the method includes the step of: (a) reacting the sulfonyl fluoride with the amine component and a sulfonamide, so as to prepare the first salt. The method further optionally includes, after the step (a), the step of: (b) reacting, in an aqueous solution, the first salt with a metal compound, so as to prepare the second salt. The method still further optionally includes, after the step (a), the step of: (c) reacting the first salt with a strong acid so as to prepare the sulfonimide. Alternatively, the method further optionally includes, after the step (b), the step of: (d) reacting the second salt with a strong acid so as to prepare the sulfonimide. The sulfonimide, the first salt or the second salt is easily economically prepared in an industrial scale production with high purity and high yield.
摘要翻译： 本发明涉及制备磺酰亚胺，其第一种盐或其第二种盐的方法。 所述方法包括以下步骤：（a）使一种或两种磺酰氟与非水氨反应，和作为叔胺和杂环胺之一的胺组分反应，以制备第一种盐。 或者，该方法包括以下步骤：（a）使磺酰氟与胺组分和磺酰胺反应，以制备第一种盐。 该方法进一步任选地包括在步骤（a）之后的步骤：（b）在水溶液中使第一盐与金属化合物反应，以制备第二种盐。 该方法还可任选地在步骤（a）之后包括以下步骤：（c）使第一种盐与强酸反应，以制备磺酰亚胺。 或者，该方法进一步任选地包括在步骤（b）之后的步骤：（d）使第二盐与强酸反应，以制备磺酰亚胺。 磺酰亚胺，第一盐或第二盐在工业规模生产中以高纯度和高产率容易地经济地制备。
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公开(公告)号：USD522038S1
公开(公告)日：2006-05-30
申请号：US29218660
申请日：2004-12-07
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公开(公告)号：US4627053A
公开(公告)日：1986-12-02
申请号：US595411
申请日：1984-03-30
申请人： Yooji Yamaki , Shigenori Sakai
发明人： Yooji Yamaki , Shigenori Sakai
摘要： In a method of repairing a semiconductor memory device having spare lines, all possible solutions of remedy using spare lines or spare blocks are obtained based on the result of test for the device, and then the possible solutions are screened under conditions related to the quality and reliability of the device so as to determine the best solution.
摘要翻译： 在修复具有备用线路的半导体存储器件的方法中，基于设备的测试结果获得使用备用线路或备用块的所有可能的解决方案，然后在与质量和条件相关的条件下筛选可能的解决方案 设备的可靠性，以确定最佳解决方案。
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5.发明授权Method and apparatus for finishing cut surface of work produced by wire cut discharge process 失效通过线切割放电工艺生产的切割工作表面的方法和装置
公开(公告)号：US4826580A
公开(公告)日：1989-05-02
申请号：US13811
申请日：1987-02-12
申请人： Takahisa Masuzawa , Shigenori Sakai
发明人： Takahisa Masuzawa , Shigenori Sakai
CPC分类号： C25F3/16 , B23H7/02 , Y10S204/09
摘要： A method and a device for finishing the cut surface of a work which is cut from a metal blank by a wire cut discharge process. The work and the waste piece of the metal blank are positioned in the same condition as just after the process. Electrolyte is fed through a clearance between the work and the waste piece and, at the same time, current is caused to flow from the work to the remainder. This subjects the cut surface of the work to electrolytic treatment to thereby make it smooth while removing oxide films and degenerated surface layers therefrom.
摘要翻译： 一种通过线切割放电处理从金属坯料切割的工件的切割表面的方法和装置。 金属坯料的工件和废件位于与刚刚过程相同的状态。 电解液通过工件和废件之间的间隙进给，同时电流从工件流到剩余部分。 这使得工件的切割表面进行电解处理，从而使其平滑，同时从其中去除氧化膜和退化的表面层。
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公开(公告)号：USD552149S1
公开(公告)日：2007-10-02
申请号：US29238356
申请日：2005-09-14
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公开(公告)号：USD544516S1
公开(公告)日：2007-06-12
申请号：US29218639
申请日：2004-12-07
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公开(公告)号：USD564565S1
公开(公告)日：2008-03-18
申请号：US29273429
申请日：2007-03-05
申请人： Yukihiko Oota , Katsumi Sakaguchi , Junsi Lee , Shigenori Sakai , Naoto Fukasawa
设计人： Yukihiko Oota , Katsumi Sakaguchi , Junsi Lee , Shigenori Sakai , Naoto Fukasawa
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公开(公告)号：USD517588S1
公开(公告)日：2006-03-21
申请号：US29218667
申请日：2004-12-07
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公开(公告)号：US6156930A
公开(公告)日：2000-12-05
申请号：US472885
申请日：1999-12-28
IPC分类号： C07C303/22 , C07C309/80 , C07C309/06
CPC分类号： C07C303/22
摘要： The present invention provides a method for producing trifluoromethanesulfonyl chloride. This method includes the step of reacting trifluoromethanesulfonic acid with phosphorous trichloride and chlorine. With this method, trifluoromethanesulfonyl chloride can be easily and highly selectively produced at high yield. The reaction may be carried out at about atmospheric pressure. Furthermore, the reaction may be carried out in the presence of phosphorus oxychloride either under a pressurized condition or at about atmospheric pressure.
摘要翻译： 本发明提供三氟甲磺酰氯的制造方法。 该方法包括使三氟甲磺酸与三氯化磷和氯反应的步骤。 通过这种方法，可以高产率容易且高选择性地制备三氟甲磺酰氯。 反应可以在约大气压下进行。 此外，反应可以在磷酰氯的存在下，在加压条件下或在大气压下进行。
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