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公开(公告)号:US20240102797A1
公开(公告)日:2024-03-28
申请号:US18256246
申请日:2020-12-09
发明人: Azusa Ishii , Shingo Mineta , Soichi Oka
摘要: A coating film evaluation structure includes a laminate including a first sheet, a second sheet, and a third sheet which are laminated. The second sheet is disposed on the first sheet, and the third sheet is disposed on the second sheet. In the laminate, the area of each sheet gradually reduces in the lamination direction, and a stepped portion is provided at an end portion. The coating film to be evaluated and the plurality of sheets have different colors. The coating film evaluation structure includes a coating film layer formed on the sheet having the largest area among the plurality of sheets so as to cover the other sheets and having a flat surface.
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公开(公告)号:US20220034828A1
公开(公告)日:2022-02-03
申请号:US17417672
申请日:2019-12-13
发明人: Azusa Ishii , Takashi Miwa , Masamitsu Watanabe , Soichi Oka
IPC分类号: G01N24/08
摘要: In a first step, a sample formed of a polyester or decomposition products of a polyester is dissolved in a pretreatment liquid containing a secondary amine to obtain a reaction product (amide) of the sample. In a second step, the obtained reaction product, amide, is mixed into a solvent containing deuterated chloroform and deuterated 1,1,1,3,3,3-hexafluoro-2-propanol to fabricate a sample liquid. In a third step, the amount of the amide in the sample liquid is measured through a nuclear magnetic resonance spectroscopy aiming at hydrogen atoms to determine the amount of acid anhydride in the sample.
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公开(公告)号:US20210116357A1
公开(公告)日:2021-04-22
申请号:US17047591
申请日:2019-04-05
发明人: Takashi Miwa , Azusa Ishii
摘要: A painting fiber probe having a measurement surface on which a coating film is formed with the same painting specification as that of a sample (painted steel sheet) is placed in a test tank together with the sample. A cycle consisting of three steps of saline water spraying, drying and wetting is repeated on the sample and the painting fiber probe. In the drying step of the cycle, absorbance at a specific wavelength of the coating film formed on the painting fiber probe is measured at a regular interval and drying is ended when the measured absorbance satisfies a predetermined condition.
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公开(公告)号:US20240150613A1
公开(公告)日:2024-05-09
申请号:US18257545
申请日:2020-12-15
发明人: Azusa Ishii , Takashi Miwa , Shingo Mineta , Soichi Oka
IPC分类号: C09D201/00 , C09D1/00
CPC分类号: C09D201/00 , C09D1/00
摘要: A coating material is a coating material used for applying a coating film formed on a coating made of a zinc-containing material formed in contact with a surface of a metal material and is composed of a binder, a first inorganic material, and a second inorganic material. The binder is composed of an organic resin and does not contain metallic zinc and a zinc alloy. The first inorganic material is composed of a sulfate having a solubility lower than 5 g/100 mL with respect to water. The second inorganic material is soluble in water, exhibits alkalinity if dissolved in water, and has a solubility lower than 5 g/100 mL with respect to water.
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公开(公告)号:US20220380879A1
公开(公告)日:2022-12-01
申请号:US17774067
申请日:2019-11-06
发明人: Takashi Miwa , Azusa Ishii , Masamitsu Watanabe , Soichi Oka
摘要: A zinc spraying material comprises a zinc material containing zinc; and a sulfate salt whose solubility in water is 1/8 or more of the solubility of calcium sulfate. The content of the sulfate salt in the zinc spraying material can be 0.006 to 0.14 mol based on 100 g of the content of the zinc material. Note that the sulfate salt can be at least one of potassium sulfate, sodium sulfate, magnesium sulfate, calcium sulfate, ferric sulfate, ferrous sulfate, lithium sulfate, calcium sulfate, and aluminum sulfate. Also, the zinc material is zinc. Alternatively, the zinc material can also be a zinc alloy containing zinc as the main component and at least one metal selected from aluminum and magnesium.
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公开(公告)号:US20210293694A1
公开(公告)日:2021-09-23
申请号:US17258381
申请日:2019-06-28
发明人: Yosuke Takeuchi , Azusa Ishii , Takuya Kamisho , Soichi Oka
IPC分类号: G01N17/02 , G01N27/28 , G01N27/416 , G01N1/32
摘要: A test time for measuring hydrogen diffusion in a steel material is improved. The reproducibility of a position where hydrogen exists in the steel material is improved. A control terminal controls a solution supply/discharge control device, a gas supply control device, a first potentiostat/galvanostat, and a second potentiostat/galvanostat on the basis of a predefined procedure, so that a plurality of processing steps, which are performed for analyzing hydrogen diffused from the inside to the surface of a steel material to be measured, are performed continuously. Further, the processing of inactivating the surface of the steel material to be measured is performed before the main processing using a metal ion replacement method, or an inert gas is injected into the solution during the main processing.
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公开(公告)号:US20210181129A1
公开(公告)日:2021-06-17
申请号:US17056217
申请日:2019-05-10
发明人: Azusa Ishii , Takashi Miwa
IPC分类号: G01N24/08
摘要: In a first step, a sample liquid is fabricated by mixing a sample formed of a polyester or decomposition products of a polyester into a solvent. The solvent used here contains chloroform and 2,2,2-trifluoroethanol and has an organic base added thereto. The organic base is at least one of a primary amine, a secondary amine, a tertiary amine and a heterocyclic amine. Next, in a second step, each of the amount of the terephthalic acid terminal and the amount of the hydroxy group terminal in the sample liquid is measured through a nuclear magnetic resonance spectroscopy aiming at hydrogen atoms. Subsequently, in a third step, the number average molecular weight of the sample is calculated from the amount of the terephthalic acid terminal and the amount of the hydroxy group terminal measured in the second step.
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公开(公告)号:US11921068B2
公开(公告)日:2024-03-05
申请号:US17056217
申请日:2019-05-10
发明人: Azusa Ishii , Takashi Miwa
IPC分类号: G01N24/08
CPC分类号: G01N24/08 , G01N24/088
摘要: In a first step, a sample liquid is fabricated by mixing a sample formed of a polyester or decomposition products of a polyester into a solvent. The solvent used here contains chloroform and 2,2,2-trifluoroethanol and has an organic base added thereto. The organic base is at least one of a primary amine, a secondary amine, a tertiary amine and a heterocyclic amine. Next, in a second step, each of the amount of the terephthalic acid terminal and the amount of the hydroxy group terminal in the sample liquid is measured through a nuclear magnetic resonance spectroscopy aiming at hydrogen atoms. Subsequently, in a third step, the number average molecular weight of the sample is calculated from the amount of the terephthalic acid terminal and the amount of the hydroxy group terminal measured in the second step.
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公开(公告)号:US11920059B2
公开(公告)日:2024-03-05
申请号:US17257201
申请日:2019-05-27
发明人: Takashi Miwa , Masamitsu Watanabe , Azusa Ishii , Soichi Oka
IPC分类号: C09D5/08 , C08K3/08 , C08K3/30 , C09D201/00
CPC分类号: C09D5/084 , C08K3/08 , C08K3/30 , C09D201/00 , C08K2003/0893 , C08K2003/3063 , C08K2003/3072 , C08K2003/3081
摘要: A coating material is allowed to contain a sulfate having a higher degree of solubility in water than that of calcium sulfate. The sulfate is an additive for coating materials which is used for reducing the consumption of zinc (including zinc oxide) in a coating film formed from the coating material and the corrosion of a base material when the coating film is scratched. The content of the sulfate can be 0.004 to 0.65 mol per 100 g of the content of zinc. Alternatively, the content of the sulfate may be 0.006 to 0.186 mol per 100 g of a heating residue (except for the sulfate added) of a coating film.
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公开(公告)号:US20240044637A1
公开(公告)日:2024-02-08
申请号:US18252293
申请日:2020-11-11
发明人: Yurina Tanaka , Azusa Ishii , Soichi Oka
CPC分类号: G01B11/06 , G06T7/60 , G06T2207/10101 , G06T2207/30184
摘要: A storage unit stores a reference image. A camera captures a film thickness measuring portion of a coating film to be measured. A determination circuit determines whether or not an image captured by the camera and the reference image match. A film thickness meter measures a film thickness of the coating film at the film thickness measuring portion in a case where the determination circuit determines that the image and the reference image match. The film thickness meter measures a film thickness of the coating film by, for example, optical coherence tomography.
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