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    Method for producing titanium metal
    2.
    发明授权
    Method for producing titanium metal 有权
    钛金属的制造方法

    公开(公告)号：US08871303B2

    公开(公告)日：2014-10-28

    申请号：US13322779

    申请日：2010-05-28

    Applicant: Gang Han ,  Shujiroh Uesaka ,  Tatsuya Shoji ,  Mariko Fukumaru (nee ABE) ,  Maher I. Boulos ,  Jiayin Guo ,  Jerzy Jurewicz

    Inventor： Gang Han ,  Shujiroh Uesaka ,  Tatsuya Shoji ,  Mariko Fukumaru (nee ABE) ,  Maher I. Boulos ,  Jiayin Guo ,  Jerzy Jurewicz

    IPC: C23C16/00 ,  C22B4/00 ,  C22B5/04 ,  C22B34/12 ,  C22B4/08

    CPC classification number: C22B34/1272 ,  C22B4/005 ,  C22B4/08 ,  C22B5/04

    Abstract: Disclosed is a method for producing titanium metal, which comprises: (a) a step in which a mixed gas is formed by supplying titanium tetrachloride and magnesium into a mixing space that is held at an absolute pressure of 50-500 kPa and at a temperature not less than 1700° C.; (b) a step in which the mixed gas is introduced into a deposition space; (c) a step in which titanium metal is deposited and grown on a substrate for deposition; and (d) a step in which the mixed gas after the step (c) is discharged. In this connection, the deposition space has an absolute pressure of 50-500 kPa, the substrate for deposition is arranged in the deposition space, and at least a part of the substrate for deposition is held within the temperature range of 715-1500° C.

    Abstract translation: 本发明公开了一种钛金属的制造方法，其特征在于，包括：（a）在保持绝对压力为50〜500kPa的混合空间和温度下，将四氯化钛和镁供给形成混合气体的工序 不低于1700℃。 （b）将混合气体导入沉积空间的步骤; （c）将钛金属沉积并生长在用于沉积的基板上的步骤; 和（d）步骤（c）之后的混合气体排出的步骤。 在这方面，沉积空间的绝对压力为50-500kPa，用于沉积的衬底被布置在沉积空间中，并且用于沉积的衬底的至少一部分保持在715-1500℃的温度范围内 。

    Induction plasma synthesis of nanopowders
    3.
    发明授权
    Induction plasma synthesis of nanopowders 有权
    纳米粉末的感应等离子体合成

    公开(公告)号：US08013269B2

    公开(公告)日：2011-09-06

    申请号：US11341211

    申请日：2006-01-27

    Applicant: Maher I. Boulos ,  Jerzy Jurewicz ,  Jiayin Guo

    Inventor： Maher I. Boulos ,  Jerzy Jurewicz ,  Jiayin Guo

    IPC: B23K10/00

    CPC classification number: C01G17/02 ,  B01J19/088 ,  B01J2219/0871 ,  B01J2219/0875 ,  B01J2219/0877 ,  B01J2219/0879 ,  B01J2219/0894 ,  B22F9/12 ,  B22F2999/00 ,  B82Y30/00 ,  C01B13/30 ,  C01B32/956 ,  C01G1/00 ,  C01G1/02 ,  C01P2004/64 ,  C01P2006/12 ,  H05H1/30 ,  B22F2202/13

    Abstract: A process and apparatus for synthesizing a nanopowder is presented. In particular, a process for the synthesis of nanopowders of various materials such as metals, alloys, ceramics and composites by induction plasma technology, using organometallic compounds, chlorides, bromides, fluorides, iodides, nitrites, nitrates, oxalates and carbonates as precursors is disclosed. The process comprises feeding a reactant material into a plasma torch in which is generated a plasma flow having a temperature sufficiently high to yield a superheated vapor of the material; transporting said vapor by means of the plasma flow into a quenching zone; injecting a cold quench gas into the plasma flow in the quenching zone to form a renewable gaseous cold front; and forming a nanopowder at the interface between the renewable gaseous cold front and the plasma flow.

    Abstract translation: 提出了一种用于合成纳米粉末的方法和装置。 具体地，公开了通过使用有机金属化合物，氯化物，溴化物，氟化物，碘化物，亚硝酸盐，硝酸盐，草酸盐和碳酸盐作为前体，通过感应等离子体技术合成各种材料的纳米粉末的方法，例如金属，合金，陶瓷和复合材料 。 该方法包括将反应物材料进料到等离子体焰炬中，其中产生具有足够高的温度以产生材料的过热蒸气的等离子体流; 通过等离子体流将所述蒸气输送到淬火区域; 将淬火气体注入淬火区域中的等离子体流中以形成可再生气态冷锋; 以及在可再生气态冷锋和等离子体流之间的界面处形成纳米粉末。

    Plasma synthesis of nanopowders
    5.
    发明授权
    Plasma synthesis of nanopowders 有权
    纳米粉末的等离子体合成

    公开(公告)号：US08859931B2

    公开(公告)日：2014-10-14

    申请号：US11683792

    申请日：2007-03-08

    Applicant: Maher I. Boulos ,  Jerzy Jurewicz ,  Jiayin Guo ,  Xiaobao Fan ,  Nicolas Dignard

    Inventor： Maher I. Boulos ,  Jerzy Jurewicz ,  Jiayin Guo ,  Xiaobao Fan ,  Nicolas Dignard

    IPC: B23K9/00 ,  B01J8/02 ,  H05H1/42 ,  B22F9/12

    CPC classification number: H05H1/42 ,  B22F9/12 ,  B22F2202/13

    Abstract: A process and apparatus for preparing a nanopowder are presented. The process comprises feeding a reactant material into a plasma reactor in which is generated a plasma flow having a temperature sufficiently high to vaporize the material; transporting the vapor with the plasma flow into a quenching zone; injecting a preheated quench gas into the plasma flow in the quenching zone to form a renewable gaseous condensation front; and forming a nanopowder at the interface between the renewable controlled temperature gaseous condensation front and the plasma flow.

    Abstract translation: 提出了一种制备纳米粉末的方法和装置。 该方法包括将反应物材料进料到等离子体反应器中，在等离子体反应器中产生具有足够高的气体以蒸发材料的等离子体流; 将蒸汽与等离子体流输送到淬火区域; 将预热的骤冷气体注入淬火区域中的等离子体流中以形成可再生气态冷凝前沿; 并在可再生的受控温度的气体冷凝前沿和等离子体流之间的界面处形成纳米粉末。

    Plasma reactor for the synthesis of nanopowders and materials processing
    6.
    发明授权
    Plasma reactor for the synthesis of nanopowders and materials processing 有权
    用于合成纳米粉末和材料加工的等离子体反应器

    公开(公告)号：US09516734B2

    公开(公告)日：2016-12-06

    申请号：US13259760

    申请日：2010-03-24

    Applicant: Maher I. Boulos ,  Jerzy Jurewicz ,  Jiayin Guo

    Inventor： Maher I. Boulos ,  Jerzy Jurewicz ,  Jiayin Guo

    IPC: H05H1/00 ,  H05H1/30 ,  B01J19/08 ,  H05H1/42 ,  H05H1/44

    CPC classification number: H05H1/30 ,  B01J19/088 ,  B01J2219/00148 ,  B01J2219/00252 ,  B01J2219/0871 ,  B01J2219/0879 ,  B01J2219/0894 ,  B22F2999/00 ,  H05H1/42 ,  H05H1/44 ,  B22F9/04 ,  B22F9/06 ,  B22F2202/13

    Abstract: A plasma reactor comprises a torch body comprising a plasma torch for generating plasma, a reactor section in fluid communication with the torch body for receiving the plasma from the plasma torch, and a quench section in fluid communication with the reactor section. The quench section comprises an inner wall defining a quench chamber, the inner wall has a serrated configuration, and the quench chamber has an upstream end adjacent the reactor section and an opposite downstream end. The plasma reactor also comprises at least one heating element in thermal communication with the reactor section, wherein the at least one heating element provides for selectively modulating a temperature within the reactor section.

    Abstract translation: 等离子体反应器包括一个包括用于产生等离子体的等离子体焰炬的炬体，与炬体流体连通的用于从等离子体焰炬接收等离子体的反应器部分和与反应器部分流体连通的骤冷部分。 淬火部分包括限定骤冷室的内壁，内壁具有锯齿状构造，并且骤冷室具有邻近反应器段的上游端和相对的下游端。 等离子体反应器还包括与反应器部分热连通的至少一个加热元件，其中至少一个加热元件提供选择性调节反应器部分内的温度。

    METAL TITANIUM PRODUCTION DEVICE AND METAL TITANIUM PRODUCTION METHOD
    8.
    发明申请
    METAL TITANIUM PRODUCTION DEVICE AND METAL TITANIUM PRODUCTION METHOD 审中-公开
    金属钛生产设备和金属钛生产方法

    公开(公告)号：US20130095243A1

    公开(公告)日：2013-04-18

    申请号：US13639358

    申请日：2011-03-07

    Applicant: Gang Han ,  Tatsuya Shoji ,  Shujiroh Uesaka ,  Mariko Fukumaru (Abe) ,  Maher I. Boulos ,  Jiayin Guo ,  Jerzy Jurewicz

    Inventor： Gang Han ,  Tatsuya Shoji ,  Shujiroh Uesaka ,  Mariko Fukumaru (Abe) ,  Maher I. Boulos ,  Jiayin Guo ,  Jerzy Jurewicz

    IPC: C23C16/06

    CPC classification number: C23C16/06 ,  C22B34/1272 ,  F27B17/00 ,  F27D2099/0015 ,  Y02P10/253

    Abstract: A metal titanium production device comprising: (a) a magnesium evaporation unit in which solid magnesium is evaporated and a first flow path which is communicated with the evaporation unit and through which gaseous magnesium is supplied; (b) a second flow path through which gaseous titanium tetrachloride is supplied; (c) a gas mixing unit which is communicated with the first flow path and the second flow path and in which the gaseous magnesium is mixed with titanium tetrachloride, the absolute pressure is adjusted to 50 to 500 kPa and the temperature is adjusted to 1600° C. or higher; (d) a metal titanium precipitation unit which is communicated with the gas mixing unit and in which a precipitation substrate having at least partially a temperature of 715 to 1500° C. is placed and the absolute pressure is adjusted to 50 to 500 kPa; and (e) a mixed gas discharge unit which is communicated with the metal titanium precipitation unit.

    Abstract translation: 一种金属钛生产装置，包括：（a）镁蒸发单元，其中固体镁被蒸发，并且第一流动路径与蒸发单元连通并通过其供应气态镁; （b）供应气体四氯化钛的第二流动路径; （c）气体混合单元，其与第一流路和第二流路连通，其中气态镁与四氯化钛混合，绝对压力调节至50-500kPa，温度调节至1600℃ C.或更高; （d）金属钛沉淀单元，其与气体混合单元连通，其中放置至少部分温度为715〜1500℃的沉淀基板，绝对压力调节至50〜500kPa; 和（e）与金属钛沉淀单元连通的混合气体排出单元。

    PLASMA REACTOR FOR THE SYNTHESIS OF NANOPOWDERS AND MATERIALS PROCESSING
    9.
    发明申请
    PLASMA REACTOR FOR THE SYNTHESIS OF NANOPOWDERS AND MATERIALS PROCESSING 有权
    用于合成纳米材料和材料加工的等离子体反应器

    公开(公告)号：US20120201266A1

    公开(公告)日：2012-08-09

    申请号：US13259760

    申请日：2010-03-24

    Applicant: Maher I. Boulos ,  Jerzy Jurewicz ,  Jiayin Guo

    Inventor： Maher I. Boulos ,  Jerzy Jurewicz ,  Jiayin Guo

    IPC: H05H1/00

    CPC classification number: H05H1/30 ,  B01J19/088 ,  B01J2219/00148 ,  B01J2219/00252 ,  B01J2219/0871 ,  B01J2219/0879 ,  B01J2219/0894 ,  B22F2999/00 ,  H05H1/42 ,  H05H1/44 ,  B22F9/04 ,  B22F9/06 ,  B22F2202/13

    Abstract: A process and apparatus for producing nanopowders and materials processing is described herein. A plasma reactor comprising a torch body comprising a plasma torch for generating a plasma; a reactor section in fluid communication with the torch body for receiving a plasma discharge and further being in fluid communication with a quench section; and at least one heating element in thermal communication with the reactor section and wherein the at least one heating element provides for selectively modulating the temperature within the reactor section is described herein.

    Abstract translation: 本文描述了用于生产纳米粉末和材料加工的方法和设备。 一种等离子体反应器，其包括用于产生等离子体的等离子体焰炬的炬体; 反应器部分，其与所述割炬主体流体连通，用于接收等离子体放电并且还与骤冷部分流体连通; 以及与反应器部分热连通的至少一个加热元件，并且其中所述至少一个加热元件提供选择性地调节反应器部分内的温度。

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