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    Hydrogenation of substrate and products manufactured according to the process
    1.
    发明授权
    Hydrogenation of substrate and products manufactured according to the process 失效
    根据工艺制造的基板和产品的氢化

    公开(公告)号：US5962711A

    公开(公告)日：1999-10-05

    申请号：US765622

    申请日：1996-12-27

    Applicant: Magnus Harrod ,  Poul M.o slashed.ller

    Inventor： Magnus Harrod ,  Poul M.o slashed.ller

    IPC: B01J3/00 ,  C01B15/029 ,  C07B35/02 ,  C07B41/02 ,  C07C29/149 ,  C11C3/12 ,  C07C51/36

    CPC classification number: C11C3/12 ,  B01J3/008 ,  C01B15/029 ,  C07B35/02 ,  C07B41/02 ,  C07C29/149

    Abstract: A typical traditional reactor for hydrogenation consists of a tank filled with a liquid and a gas and a small particle catalyst. The reaction is carried out at high pressures and high temperatures. Lack of gas on the catalyst surface limits the velocity of reaction. Much work has been done to increase the quantity of gas on the catalyst. It has not been possible to solve this problem effectively with the techniques of today. According to the invention an extra solvent is added to the reaction mixture. By bringing the whole mixture (solvent, substrate, hydrogen and reaction products) to super-critical or near-critical state, a substantially homogeneous mixture can be obtained. By this method it is possible to control the concentration of gas on the catalyst to the desired level. The velocity of reaction is thereby increased considerably. The hydrogenation reactions principally involved comprise hydrogenation of carbon-carbon double bonds (C.dbd.C) in lipids; hydrogenation of COOR to C--OH and HO--R to produce fatty alcohols; and direct hydrogenation of oxygen to hydrogen peroxide.

    Abstract translation: PCT No.PCT / SE95 / 00824 Sec。 371日期1997年12月27日第 102（e）日期1997年12月27日PCT提交1995年7月3日PCT公布。 公开号WO96 / 01304 日期1996年1月18日典型的用于氢化的传统反应器由填充有液体和气体的罐和小颗粒催化剂组成。 反应在高压和高温下进行。 催化剂表面缺乏气体限制了反应速度。 已经做了大量工作来增加催化剂上的气体量。 今天的技术无法有效地解决这个问题。 根据本发明，向反应混合物中加入额外的溶剂。 通过将整个混合物（溶剂，底物，氢气和反应产物）引入超临界或接近临界状态，可获得基本均匀的混合物。 通过该方法，可以将催化剂上的气体浓度控制到所需的水平。 因此反应速度显着增加。 主要涉及的氢化反应包括脂质中碳 - 碳双键（C = C）的氢化; 将COOR氢化成C-OH和HO-R以产生脂肪醇; 并将氧气直接氢化成过氧化氢。

    Selective hydrogenation of functional groups in substrates and partially hydrogenated fatty acids and fatty acid derivatives
    2.
    发明申请
    Selective hydrogenation of functional groups in substrates and partially hydrogenated fatty acids and fatty acid derivatives 审中-公开
    底物和部分氢化脂肪酸和脂肪酸衍生物中官能团的选择氢化

    公开(公告)号：US20070088171A1

    公开(公告)日：2007-04-19

    申请号：US11529761

    申请日：2006-09-29

    Applicant: Magnus Harrod ,  Andre Holmqvist ,  Sander Van Den Hark

    Inventor： Magnus Harrod ,  Andre Holmqvist ,  Sander Van Den Hark

    IPC: C07C51/36

    CPC classification number: C11C3/126 ,  C07C51/36 ,  C07C53/126 ,  C07C57/12

    Abstract: Process for the hydrogenation of functional groups in hydrogenatable substrates, wherein hydrogen gas is mixed with the substrate and a solvent, the mixture is brought into contact with a catalyst. The hydrogenation is carried out under process conditions which are adapted to the activity of the catalyst used, wherein the temperature is sufficiently low, the substrate concentration is sufficiently high and the diffusivity is sufficiently high to provide a selective hydrogenation of the functional group having a higher reactivity than one which has a lower reactivity. The functional groups can for example comprise different C═C-groups in substrates in the form of lipids, primarily fatty acids and fatty acid derivatives, such as triglycerides and methyl fatty acids. Partially-hydrogenated fatty acids/fatty acid derivatives can hereby be obtained, which possess a low content of trans-fatty acid content as well as high selectivity in the form of SLn-number and SLo-number.

    Abstract translation: 在可氢化基底中氢化功能基团的方法，其中氢气与基底和溶剂混合，使混合物与催化剂接触。 氢化是在适合于所用催化剂的活性的工艺条件下进行的，其中温度足够低，底物浓度足够高，扩散性足够高以提供具有较高的官能团的选择性氢化 反应性比具有较低反应性的反应性。 官能团可以例如包括脂质形式的底物中不同的C-C基团，主要是脂肪酸和脂肪酸衍生物，例如甘油三酸酯和甲基脂肪酸。 因此可以获得部分氢化的脂肪酸/脂肪酸衍生物，其具有低含量的反式脂肪酸含量以及高选择性，其形式为S-Ln- Lo - 数字。

    METHOD FOR SEPARATING NEUTRAL AND POLAR LIPIDS AND AN OIL RICH IN POLAR LIPIDS
    5.
    发明申请
    METHOD FOR SEPARATING NEUTRAL AND POLAR LIPIDS AND AN OIL RICH IN POLAR LIPIDS 有权
    在极性脂肪中分离中性和极性脂肪和油的方法

    公开(公告)号：US20120095198A1

    公开(公告)日：2012-04-19

    申请号：US13255869

    申请日：2010-03-10

    Applicant: Magnus Harrod

    Inventor： Magnus Harrod

    IPC: C11B3/00 ,  C11C1/00 ,  C07H15/08

    CPC classification number: C11B7/0083 ,  C07H13/06 ,  C11B3/006 ,  C11B7/0025

    Abstract: A method for separating neutral and polar lipids from an oil of biological material, wherein the oil is fractionated using a mixture of a polar solvent comprising at least one carbon atom, water and an additional substance selected from the group consisting of: mono-, di- and oligosaccharides comprising from 3 to 10 monosaccharide units, said additional substance is present in an amount of at least 0.1 wt % calculated on the total weight of solvent, water and additional substance, to form at least two liquid fractions having different densities, wherein one fraction is rich in polar lipids and another fraction is rich in neutral lipids. An oil rich in polar lipids obtained from the method is disclosed, said oil I contains at least 40, preferably at least 50 lipid % polar lipids as calculated on the total amount of lipids in said oil and that the total amount of polar solvent and water in said oil is between 20 and 30 wt %. An oat oil containing high amounts of estolides of DGDG can further be obtained.

    Abstract translation: 一种从生物材料的油中分离中性和极性脂质的方法，其中使用包含至少一个碳原子的极性溶剂，水和选自以下的另外的物质的混合物将油分馏：单 - ，二 - 和包含3至10个单糖单元的寡糖，所述另外的物质以基于溶剂，水和附加物质的总重量计算的至少0.1重量％的量存在，以形成至少两个具有不同密度的液体馏分，其中 一部分富含极性脂质，另一部分富含中性脂质。 公开了从该方法获得的富含极性脂质的油，所述油I含有至少40种，优选至少50种脂质％极性脂质，根据所述油中脂质的总量计算，并且极性溶剂和水的总量 在所述油中的含量为20-30重量％。 可以进一步获得含有大量的DGDG的耳塞油的燕麦油。

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