Method and composition for depolymerization of cured epoxy resin materials

    公开(公告)号:US10280534B2

    公开(公告)日:2019-05-07

    申请号:US16126580

    申请日:2018-09-10

    Abstract: A cured epoxy resin material is depolymerized by using a composition including a compound represented by the chemical formula of XOmYn (wherein X is hydrogen, alkali metal or alkaline earth metal, Y is halogen, m is a number satisfying 1≤m≤8 and n is a number satisfying 1≤n≤6), and a reaction solvent, wherein X is capable of being dissociated from XOmYn and Y radical is capable of being produced from XOmYn in the reaction solvent. It is possible to carry out depolymerization of a cured epoxy resin material, for example, at a temperature of 200° C., specifically 100° C. or lower, and to reduce processing cost and energy requirement. It is also possible to substitute for a reaction system using an organic solvent as main solvent, so that the contamination problems caused by the organic solvent functioning as separate contamination source may be solved and environmental contamination or pollution may be minimized.

    Nanocarbon composite carbon fiber with low cost and high performance and their preparation method

    公开(公告)号:US10344404B2

    公开(公告)日:2019-07-09

    申请号:US15162052

    申请日:2016-05-23

    Abstract: The present disclosure relates to a preparation method for lowering a production cost of a high performance carbon fiber using a nanocarbon composite carbon fiber precursor fiber crosslinked by electron beam. More particularly, the present disclosure relates to a preparation method of a nanocarbon composite carbon fiber, including a nanocarbon containing step for containing nanocarbon in a structure of a carbon fiber precursor fiber, a nanocarbon composite carbon fiber precursor fiber preparation step for forming a composite of the nanocarbon and the carbon fiber precursor fiber by electron beam irradiation to enable crosslinking for improved heat resistance of the carbon fiber precursor fiber containing the nanocarbon, an oxidation⋅stabilization step for oxidizing⋅stabilizing the nanocarbon composite carbon fiber precursor fiber, and a carbonization step for carbonizing the oxidized⋅stabilized nanocarbon composite carbon fiber precursor fiber, and a nanocarbon composite carbon fiber prepared by the preparation method.

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