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    Feed Mixtures for Extraction Process to Produce Rubber Processing Oil
    1.
    发明申请
    Feed Mixtures for Extraction Process to Produce Rubber Processing Oil 有权
    饲料混合物提取工艺生产橡胶加工油

    公开(公告)号：US20120181220A1

    公开(公告)日：2012-07-19

    申请号：US13007581

    申请日：2011-01-14

    申请人： Chih-Cheng Chang ,  Jung-Huang Wu ,  Cheng-Tsung Hong ,  Jin-Shang Liou ,  Kuo-Min Wei ,  Hung-Chung Shen ,  Fu-Ming Lee

    发明人： Chih-Cheng Chang ,  Jung-Huang Wu ,  Cheng-Tsung Hong ,  Jin-Shang Liou ,  Kuo-Min Wei ,  Hung-Chung Shen ,  Fu-Ming Lee

    IPC分类号： C10G21/16 ,  C10G21/22 ,  C10G21/20

    CPC分类号： C10G21/16 ,  C10G21/003 ,  C10G21/20 ,  C10G21/22 ,  C10G21/27 ,  C10G53/00 ,  C10G2300/1062 ,  C10G2300/1074 ,  C10G2300/30 ,  C10G2300/302 ,  C10G2300/44 ,  C10G2400/30

    摘要： Deasphalted residual oil (DAO) and the aromatics-rich extract that is derived from DAO have low polycyclic aromatics contents, relatively low aniline points, and high flash points. They form blending stocks that improve properties of mixed feedstocks to consistently produce environmentally qualified rubber processing oil (RPO) by extraction under low solvent-to-oil ratios and moderate extraction temperatures. Distilling a petroleum crude oil under atmospheric pressure generates a bottom residual oil which is then subject to vacuum distillation to yield a bottom residual oil. DAO is produced by removing the asphalt from the vacuum bottom residual oil through extraction with light paraffinic solvent. The extract of DAO is a co-product in the production of the bright stock of the lubricating oil through extraction. The feedstock is mixed with the extract from a petroleum fraction boiling in lube oil range. Liquid-liquid counter-current extraction yields a raffinate stream; removal of solvent therefrom produces the RPO.

    摘要翻译： 脱气残油（DAO）和来自DAO的富含芳烃的提取物具有低多环芳烃含量，苯胺点相对较低，闪点高。 它们形成混合原料，以改善混合原料的性能，以通过在低溶剂/油比和中等萃取温度下萃取来一致地生产环保合格的橡胶加工油（RPO）。 在大气压下蒸馏石油原油产生底部残余油，然后进行真空蒸馏以产生底部残余油。 DAO是通过用轻链烷烃溶剂萃取从真空底渣中除去沥青而制得的。 DAO的提取物是通过萃取生产润滑油的亮油的共同产品。 原料与在润滑油范围沸腾的石油馏分的提取物混合。 液 - 液逆流萃取产生萃余液流; 除去溶剂产生RPO。

    Feed mixtures for extraction process to produce rubber processing oil
    2.
    发明授权
    Feed mixtures for extraction process to produce rubber processing oil 有权
    进料混合物用于萃取工艺生产橡胶加工油

    公开(公告)号：US08864981B2

    公开(公告)日：2014-10-21

    申请号：US13007581

    申请日：2011-01-14

    申请人： Chih-Cheng Chang ,  Jung-Huang Wu ,  Cheng-Tsung Hong ,  Jin-Shang Liou ,  Kuo-Min Wei ,  Hung-Chung Shen ,  Fu-Ming Lee

    发明人： Chih-Cheng Chang ,  Jung-Huang Wu ,  Cheng-Tsung Hong ,  Jin-Shang Liou ,  Kuo-Min Wei ,  Hung-Chung Shen ,  Fu-Ming Lee

    IPC分类号： C10G17/04 ,  C10G53/00 ,  C10G21/00 ,  C10G21/27 ,  C10G21/22 ,  C10G21/16 ,  C10G21/20

    CPC分类号： C10G21/16 ,  C10G21/003 ,  C10G21/20 ,  C10G21/22 ,  C10G21/27 ,  C10G53/00 ,  C10G2300/1062 ,  C10G2300/1074 ,  C10G2300/30 ,  C10G2300/302 ,  C10G2300/44 ,  C10G2400/30

    摘要： Deasphalted residual oil (DAO) and the aromatics-rich extract that is derived from DAO have low polycyclic aromatics contents, relatively low aniline points, and high flash points. They form blending stocks that improve properties of mixed feedstocks to consistently produce environmentally qualified rubber processing oil (RPO) by extraction under low solvent-to-oil ratios and moderate extraction temperatures. Distilling a petroleum crude oil under atmospheric pressure generates a bottom residual oil which is then subject to vacuum distillation to yield a bottom residual oil. DAO is produced by removing the asphalt from the vacuum bottom residual oil through extraction with light paraffinic solvent. The extract of DAO is a co-product in the production of the bright stock of the lubricating oil through extraction. The feedstock is mixed with the extract from a petroleum fraction boiling in lube oil range. Liquid-liquid counter-current extraction yields a raffinate stream; removal of solvent therefrom produces the RPO.

    摘要翻译： 脱气残油（DAO）和来自DAO的富含芳烃的提取物具有低多环芳烃含量，苯胺点相对较低，闪点高。 它们形成混合原料，以改善混合原料的性能，以通过在低溶剂/油比和中等萃取温度下萃取来一致地生产环保合格的橡胶加工油（RPO）。 在大气压下蒸馏石油原油产生底部残余油，然后进行真空蒸馏以产生底部残余油。 DAO是通过用轻链烷烃溶剂萃取从真空底渣中除去沥青而制得的。 DAO的提取物是通过萃取生产润滑油的亮油的共同产品。 原料与在润滑油范围沸腾的石油馏分的提取物混合。 液 - 液逆流萃取产生萃余液流; 除去溶剂产生RPO。

    Low-energy extractive distillation process for dehydration of aqueous ethanol
    6.
    发明授权
    Low-energy extractive distillation process for dehydration of aqueous ethanol 有权
    用于乙醇水溶液脱水的低能萃取蒸馏方法

    公开(公告)号：US08002953B2

    公开(公告)日：2011-08-23

    申请号：US11827896

    申请日：2007-07-13

    申请人： Fu-Ming Lee ,  Kuang-Yeu Wu ,  Lindsey Vuong ,  Fong-Cheng Su ,  Tzong-Bin Lin ,  Jyh-Haur Hwang ,  Hung-Chung Shen ,  Po-Sung Cheng ,  Tai-Ping Chang

    发明人： Fu-Ming Lee ,  Kuang-Yeu Wu ,  Lindsey Vuong ,  Fong-Cheng Su ,  Tzong-Bin Lin ,  Jyh-Haur Hwang ,  Hung-Chung Shen ,  Po-Sung Cheng ,  Tai-Ping Chang

    IPC分类号： B01D3/40 ,  B01D3/42 ,  C07C29/84 ,  C07C29/94 ,  C12G3/12

    CPC分类号： C07C29/84 ,  B01D3/002 ,  B01D3/143 ,  B01D3/40 ,  Y02P20/125 ,  Y02P20/57 ,  Y10S203/14 ,  Y10S203/20 ,  C07C31/08

    摘要： An energy-efficient extractive distillation process for producing anhydrous ethanol from aqueous/ethanol feeds containing any range of ethanol employs an extractive distillation column (EDC) that operates under no or greatly reduced liquid reflux conditions. The EDC can be incorporated into an integrated process for producing anhydrous ethanol used for gasoline blending from fermentation broth. By using a high-boiling extractive distillation solvent, no solvent is entrained by the vapor phase to the EDC overhead stream, even under no liquid reflux conditions. The energy requirement and severity of the EDC can be further improved by limiting ethanol recovery in the EDC. In this partial ethanol recovery design, ethanol which remains in the aqueous stream from the EDC is recovered in a post-distillation column or the aqueous stream is recycled to a front-end pre-distillation column where the ethanol is readily recovered since the VLE curve for ethanol/water is extremely favorable for distillation.

    摘要翻译： 从含有任何范围的乙醇的含水/乙醇进料中生产无水乙醇的节能萃取蒸馏方法采用在没有或大大降低的液体回流条件下运行的萃取蒸馏塔（EDC）。 EDC可以并入用于从发酵液中生产用于汽油混合的无水乙醇的整合方法。 通过使用高沸点萃取蒸馏溶剂，即使在没有液体回流条件下，没有溶剂被气相夹带到EDC塔顶馏出物中。 通过限制EDC中的乙醇回收，可以进一步提高EDC的能量需求和严重程度。 在该部分乙醇回收设计中，保留在来自EDC的水流中的乙醇在后蒸馏塔中回收，或将水流循环至前端预蒸馏塔，其中乙醇容易回收，因为VLE曲线 对于乙醇/水非常有利于蒸馏。

    Homogeneous catalysts for biodiesel production
    7.
    发明授权
    Homogeneous catalysts for biodiesel production 失效
    用于生物柴油生产的均相催化剂

    公开(公告)号：US08624073B1

    公开(公告)日：2014-01-07

    申请号：US13759644

    申请日：2013-02-05

    申请人： Shih-Chieh Yang ,  Jen-Ray Chang ,  Maw-Tien Lee ,  Tzong-Bin Lin ,  Fu-Ming Lee ,  Cheng-Tsung Hong ,  Jeng-Cheng Lee

    发明人： Shih-Chieh Yang ,  Jen-Ray Chang ,  Maw-Tien Lee ,  Tzong-Bin Lin ,  Fu-Ming Lee ,  Cheng-Tsung Hong ,  Jeng-Cheng Lee

    IPC分类号： C07C1/00 ,  C11C3/00

    CPC分类号： C11C3/10 ,  C07C67/03 ,  Y02E50/13 ,  C07C69/52

    摘要： Non-basic and non-acidic homogeneous catalysts organo-metallic compound of the formula: M(OCH3)x wherein M is B, Na, Mg, K, Ca, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ga, Ge, Al, Sn, Sb, Mo, Ag, and Cd and x is an integer from 2, 3 or 4 can catalyze transesterification of oils and fats having high free fatty acid content and with an acid number from 0.5 to 20, into biodiesel. B(OCH3)3 and Ge(OCH3)4, having low boiling points, are easily recovered from the biodiesel and glycerol phases and recycled for reuse. Continuous biodiesel production with the novel homogenous catalysts is achieved without the complicated and troublesome steps attendant with conventional processes using base or acid homogeneous catalyst. The high purity biodiesel is produced without acid-base neutralization, water wash, filtration, and solid disposal steps for removing the spent catalyst from the product streams associated with prior techniques.

    摘要翻译： 非碱性和非酸性均相催化剂下式的有机金属化合物：M（OCH 3）x其中M为B，Na，Mg，K，Ca，Sc，Ti，V，Cr，Mn，Fe，Co，Ni ，Cu，Zn，Ga，Ge，Al，Sn，Sb，Mo，Ag和Cd，x是2,3或4的整数，可以催化具有高游离脂肪酸含量和酸值的油和脂肪的酯交换反应 从0.5到20，进入生物柴油。 具有低沸点的B（OCH 3）3和Ge（OCH 3）4）容易从生物柴油和甘油相回收并再循环再利用。 使用新型均相催化剂进行连续生物柴油生产，而不需要使用碱或酸均相催化剂的常规方法所需的复杂和麻烦的步骤。 高纯度生物柴油在没有酸碱中和，水洗，过滤和固体处理步骤的情况下生产，用于从与先前技术相关的产品流中除去废催化剂。

    Extractive distillation processes using water-soluble extractive solvents
    8.
    发明授权
    Extractive distillation processes using water-soluble extractive solvents 有权
    使用水溶性萃取溶剂的萃取蒸馏方法

    公开(公告)号：US07871514B2

    公开(公告)日：2011-01-18

    申请号：US12316405

    申请日：2008-12-12

    申请人： Fu-Ming Lee ,  Tzong-Bin Lin ,  Jyh-Haur Hwang ,  Hung-Chung Shen ,  Kuang-Yeu Wu ,  Tsung-Min Chiu ,  Zong-Ying Chen ,  Tung-Hsiung Kuo ,  Yu-Ming Wu

    发明人： Fu-Ming Lee ,  Tzong-Bin Lin ,  Jyh-Haur Hwang ,  Hung-Chung Shen ,  Kuang-Yeu Wu ,  Tsung-Min Chiu ,  Zong-Ying Chen ,  Tung-Hsiung Kuo ,  Yu-Ming Wu

    IPC分类号： C07C7/00

    CPC分类号： B01D3/40 ,  C10G7/08 ,  C10G2400/30

    摘要： Extractive distillation processes whereby water-soluble extractive distillation (ED) solvents are regenerated and recovered employ improved operations of the extractive distillation column (EDC) so that polar hydrocarbons are recovered and purified from mixtures containing polar and less polar hydrocarbons and measurable amounts of hydrocarbons that are heavier than intended feedstock and/or polymers that are generated in the ED process. The improved process can effectively remove and recover the heavy hydrocarbons and/or remove polymer contaminants from the solvent in a closed solvent circulating loop through mild operating conditions with no additional process energy being expended. With the improved process, the overhead reflux of the EDC may be eliminated to further reduce energy consumption and to enhance the loading and performance within the upper portion of the EDC, especially when two liquid phases exists therein.

    摘要翻译： 萃取蒸馏方法，其中水溶性萃取蒸馏（ED）溶剂被再生和回收利用萃取蒸馏塔（EDC）的改进操作，使极性烃从含有极性和极性较小的烃的混合物中回收和纯化， 比在ED过程中产生的预期原料和/或聚合物重。 改进的方法可以在封闭的溶剂循环回路中通过温和的操作条件有效地除去和回收重质烃和/或从溶剂中除去聚合物污染物，而不需要额外的工艺能量消耗。 通过改进的方法，可以消除EDC的顶部回流以进一步降低能量消耗并增强EDC上部的负载和性能，特别是当存在两个液相时。

    Low-energy extractive distillation process for dehydration of aqueous ethanol
    9.
    发明授权
    Low-energy extractive distillation process for dehydration of aqueous ethanol 失效
    用于乙醇水溶液脱水的低能萃取蒸馏方法

    公开(公告)号：US08172987B2

    公开(公告)日：2012-05-08

    申请号：US13184540

    申请日：2011-07-17

    申请人： Fu-Ming Lee ,  Tzong-Bin Lin ,  Jyh-Haur Hwang ,  Hung-Chung Shen ,  Kuang-Yeu Wu ,  Lindsey Vuong ,  Fong-Cheng Su ,  Po-Sung Cheng ,  Tai-Ping Chang

    发明人： Fu-Ming Lee ,  Tzong-Bin Lin ,  Jyh-Haur Hwang ,  Hung-Chung Shen ,  Kuang-Yeu Wu ,  Lindsey Vuong ,  Fong-Cheng Su ,  Po-Sung Cheng ,  Tai-Ping Chang

    IPC分类号： B01D3/40 ,  B01D3/42 ,  C07C29/84 ,  C07C29/94 ,  C12G3/12

    CPC分类号： C07C29/84 ,  B01D3/002 ,  B01D3/143 ,  B01D3/40 ,  Y02P20/125 ,  Y02P20/57 ,  Y10S203/14 ,  Y10S203/20 ,  C07C31/08

    摘要： An energy-efficient extractive distillation process for producing anhydrous ethanol from aqueous/ethanol feeds containing any range of ethanol employs an extractive distillation column (EDC) that operates under no or greatly reduced liquid reflux conditions. The EDC can be incorporated into an integrated process for producing anhydrous ethanol used for gasoline blending from fermentation broth. By using a high-boiling extractive distillation solvent, no solvent, is entrained by the vapor phase to the EDC overhead stream, even under no liquid reflux conditions. The energy requirement and severity of the EDC can be further improved by limiting ethanol recovery in the EDC. In this partial ethanol recovery design, ethanol which remains in the aqueous stream from the EDC is recovered in a post-distillation column or the aqueous stream is recycled to a front-end pre-distillation column where the ethanol is readily recovered since the VLE curve for ethanol/water is extremely favorable for distillation.

    摘要翻译： 从含有任何范围的乙醇的含水/乙醇进料中生产无水乙醇的节能萃取蒸馏方法采用在没有或大大降低的液体回流条件下运行的萃取蒸馏塔（EDC）。 EDC可以并入用于从发酵液中生产用于汽油混合的无水乙醇的整合方法。 通过使用高沸点萃取蒸馏溶剂，即使在没有液体回流条件下，也没有溶剂被气相夹带到EDC塔顶馏出物中。 通过限制EDC中的乙醇回收，可以进一步提高EDC的能量需求和严重程度。 在该部分乙醇回收设计中，保留在来自EDC的水流中的乙醇在后蒸馏塔中回收，或将水流循环至前端预蒸馏塔，其中乙醇容易回收，因为VLE曲线 对于乙醇/水非常有利于蒸馏。

    Novel Methods for Regeneration of Solvents for Extractive Processes
    10.
    发明申请
    Novel Methods for Regeneration of Solvents for Extractive Processes 有权
    用于萃取过程溶剂再生的新方法

    公开(公告)号：US20120037542A1

    公开(公告)日：2012-02-16

    申请号：US12854150

    申请日：2010-08-10

    申请人： Kuang-Yeu Wu ,  Tzong-Bin Lin ,  Fu-Ming Lee ,  Tsung-Min Chiu ,  Jyh-Haur Hwang ,  Hung-Chung Shen

    发明人： Kuang-Yeu Wu ,  Tzong-Bin Lin ,  Fu-Ming Lee ,  Tsung-Min Chiu ,  Jyh-Haur Hwang ,  Hung-Chung Shen

    IPC分类号： C10G21/28

    CPC分类号： C07C7/08 ,  C07D333/48 ,  C10G21/28 ,  C10G2300/1081 ,  C10G2300/1088 ,  C10G2300/1096 ,  C10G2300/44 ,  C10G2300/805 ,  C07C15/04 ,  C07C15/06

    摘要： An improved solvent regeneration system for extractive distillation and liquid-liquid extraction processes capable of effectively removing heavy hydrocarbons and polymeric materials that otherwise develop in a closed solvent loop. The improved process employs a light hydrocarbon displacement agent, which is at least partially soluble in the solvent to squeeze the heavy hydrocarbons and polymeric materials out of the solvent, with virtually no additional energy requirement. It has been demonstrated that the light non-aromatic hydrocarbons in the raffinate stream generated from the extractive distillation or the liquid-liquid extractive process for aromatic hydrocarbons recovery can displace not only the heavy non-aromatic hydrocarbons but also the heavy aromatic hydrocarbons from the extractive solvent, especially when the aromatic hydrocarbons in the solvent are in the C10+ molecular weight range.

    摘要翻译： 用于萃取蒸馏和液 - 液萃取方法的改进的溶剂再生系统，其能够有效地除去否则在密闭的溶剂回路中发展的重质烃和聚合材料。 改进的方法采用轻质烃置换剂，其至少部分可溶于溶剂以将重质烃和聚合物材料挤出溶剂，实际上无需额外的能量需求。 已经证明，从萃取蒸馏或用于芳族烃回收的液 - 液萃取过程产生的萃余液流中的轻非芳族烃不仅可以取代重非芳族烃，而且可以取代萃取物中的重芳香烃 溶剂，特别是当溶剂中的芳烃为C10 +分子量范围时。