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公开(公告)号：US07931696B2
公开(公告)日：2011-04-26
申请号：US12520887
申请日：2008-01-22
IPC分类号： A61Q5/10 , C07D333/00
CPC分类号： A61Q5/065 , A61K8/4986 , A61K2800/94 , C09B44/101 , C09B44/107 , C09B55/003
摘要： Disclosed are dyes of formula wherein D is the radical of anthraquinone, acridine, azo, azomethine, hydrazomethine, benzodifuranone, coumarine, diketopyrrolopyrrol, dioxaxine, diphenylmethane, formazane, indigoid, indophenol, naphtalimide, naphthaquinone, nitroaryl, merocyanine, methine, oxazine, perinone, perylene, pyrenequinone, phtalocyanine, phenazine, quinoneimine, quinacridone, quinophtalone, stilbene, styryl, triphenylmethane, xanthene, thiazine dye and thioxanthene dye; and Q is defined herein.
摘要翻译： 公开了下式的染料，其中D是蒽醌，吖啶，偶氮，偶氮甲碱，肼甲基，苯并二呋喃酮，香豆素，二酮吡咯并吡咯，二氧杂环己烷，二苯基甲烷，甲ane烷，靛类，靛酚，萘二甲酰亚胺，萘醌，硝基芳基，部花青，次甲基，恶嗪， ，苝，芘醌，酞菁，吩嗪，醌亚胺，喹吖啶酮，喹诺酮，芪，苯乙烯基，三苯甲烷，呫吨，噻嗪染料和噻吨染料; 并且Q在本文中定义。
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2.发明授权公开(公告)号：US07476260B2
公开(公告)日：2009-01-13
申请号：US11547571
申请日：2005-03-29
CPC分类号： C09B44/16 , A61K8/49 , A61K8/4926 , A61K8/4946 , A61K2800/94 , A61Q5/10 , C09B44/20 , C09B49/00
摘要： Formula (I) wherein R1 and R2 each independently from each other are a residue of an organic dye: Y1 and Y2 each independently from each other are unsubstituted or substituted, straightchain or branched, interrupted or uninterrupted —C1-C10alkylene-; —C5-C10cycloalkylene-; C5-C10arylene; or —C5-C10arylene-(C1-C10alkylene)-; Z1 and Z2 independently from each other are Formula (II) are each independently from each other hydrogen; or unsubstituted or substituted, straight-chain or branched, mono-cyclic or polycyclic, interrupted or uninterrupted C1-C14alkyl; C2-C14alkenyl; C6-C10aryl; C6-C10aryl-C1-C10alkyl; or C5-C10alkyl(C5-C10aryl); r, q and n independently from each other are 0 or 1, if n is 0, Z3 is hydrogen; and if n is 1, Z3 is —S—: with the proviso that the method does not comprise treating the fiber with an enzyme of the type of a protein disulfidisomerase (EC 5.3.4.1). Further, the present invention relates to novel disulfid compounds, compositions thereof, especially comprising other dyes, and to processes for their preparation.
摘要翻译： 式（I）其中R 1和R 2各自独立地是有机染料的残基：Y 1和Y 2各自独立地是未取代或取代的，直链或支链的，间断的或不间断的-C 1 -C 10亚烷基 - ; -C 5 -C 10环亚烷基 - C5-C10亚芳基 或-C 5 -C 10亚芳基 - （C 1 -C 10亚烷基） - ; Z 1和Z 2彼此独立地是式（II）各自独立地为氢; 或未取代或取代的直链或支链的单环或多环，间断或不间断的C 1 -C 14烷基; C2-C14烯基; C6-C10芳基; C 6 -C 10芳基-C 1 -C 10烷基; 或C 5 -C 10烷基（C 5 -C 10芳基）; r，q和n彼此独立地为0或1，如果n为0，则Z 3为氢; 并且如果n为1，则Z 3为-S-，条件是该方法不包括用蛋白质二硫代异构酶类型的EC处理纤维（EC 5.3.4.1）。 此外，本发明涉及新的二硫化物，其组合物，特别是其它染料，以及其制备方法。
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公开(公告)号：US07307155B2
公开(公告)日：2007-12-11
申请号：US10565137
申请日：2004-07-14
申请人： Victor Paul Eliu , Beate Fröhling
发明人： Victor Paul Eliu , Beate Fröhling
CPC分类号： C09B44/16
摘要： The present invention relates to novel the cationic dyes of formula (1) wherein R1 is an unsubstituted or substituted C1-C14 alkyl or an aryl radical; X− is an anion; R3 is an unsubstituted or substituted C1-C14 alkyl, aryl radical, C1-C6 alkoxy, cyanid, nitro or halide; n is 1 or 2; and if n is 1, then R2 is hydrogen, unsubstituted or substituted C1-C14 alkyl; or if n is 2, then R2 is an unsubstituted or substituted C1-C14 alkylen. Further, the present invention relates to compositions thereof, especially comprising other dyes, to processes for the preparation thereof and to the use thereof in the dyeing of organic material, such as keratin, wool, leather, silk, paper, cellulose or polyamides, and preferably human hair
摘要翻译： 本发明涉及新型式（1）的阳离子染料，其中R 1是未取代或取代的C 1 -C 14烷基或 芳基; X 是阴离子; R 3是未取代或取代的C 1 -C 14烷基，芳基，C 1 -C 6烷基， 氰基，硝基或卤素; n为1或2; 并且如果n为1，则R 2为氢，未取代或取代的C 1 -C 14烷基; 或者如果n为2，则R 2为未取代或取代的C 1 -C 14亚烷基。 此外，本发明涉及其组合物，特别是其它染料，其制备方法及其在染色有机材料如角蛋白，羊毛，皮革，丝，纸，纤维素或聚酰胺中的用途，以及 优选人发
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公开(公告)号：US07785375B2
公开(公告)日：2010-08-31
申请号：US11922660
申请日：2006-06-21
IPC分类号： A61Q5/10 , C07D279/00
CPC分类号： A61Q5/10 , A61K8/49 , C07D513/04 , C09B23/0091
摘要： Disclosed is a method of dyeing keratin-containing fibers comprising treating the fiber with at least one compound of formula (1), wherein R1, R2, R3, R4 independently from each other are hydrogen; hydroxy; —S—H; —S—C1-C12alkyl; halogen; C1-C12alkyl or C1-C12alkoxy, which may be substituted by one or more C1-C5alkyl, C1-C5-alkoxy, hydroxy, —(CO)—H or —(CO)—C1-C5alkyl; —NR5R6; —NO2; —(CO)H or (CO)—C1-C5alkyl; C6-C12aryl, C6-C12aryl-C1-C4alkyl or C6-C12aryl-C1-C4alkoxy, wherein the aryl moiety may be substituted by one or more C1-C5alkyl, C1-C5alkoxy, —(CO)—H or —(CO)—C1-C5alkyl; R5 and R6 independently from each other are hydrogen; hydroxy; C1-C12alkyl; hydroxy-C1-C12alkyl; —(CO)—H; —(CO)—C1-C5alkyl; phenyl or phenyl-C1-C5alkyl, wherein the phenyl moiety may be substituted by one or more C1-C5alkyl, C1-C5alkoxy, halogen, —NH2, mono-C1-C5alkylamino, di-C1-C5alkylamino, —NO2, carboxy or hydroxy; and An is an anion. Furthermore, the present invention relates to novel heterocyclic compounds, compositions thereof, especially comprising other dyes, and to processes for their preparation and application to hair dying.
摘要翻译： 公开了一种染色含角蛋白纤维的方法，包括用至少一种式（1）化合物处理纤维，其中R 1，R 2，R 3，R 4彼此独立地为氢; 羟基; -S-H; -S-C 1 -C 12烷基; 卤素; C 1 -C 12烷基或C 1 -C 12烷氧基，其可以被一个或多个C 1 -C 5烷基，C 1 -C 5 - 烷氧基，羟基， - （CO）-H或 - （CO）-C 1 -C 5烷基取代; -NR5R6; -NO2; - （CO）H或（CO）-C 1 -C 5烷基; C 1 -C 12芳基，C 6 -C 12芳基-C 1 -C 4烷基或C 6 -C 12芳基-C 1 -C 4烷氧基，其中芳基部分可被一个或多个C 1 -C 5烷基，C 1 -C 5烷氧基， - （CO）-H或 - （CO） -C 1 -C 5烷基; R5和R6彼此独立地是氢; 羟基; C 1 -C 12烷基; 羟基-C 1 -C 12烷基; - （CO）-H; - （CO）-C 1 -C 5烷基; 苯基或苯基-C 1 -C 5烷基，其中苯基部分可被一个或多个C 1 -C 5烷基，C 1 -C 5烷氧基，卤素，-NH 2，单C 1 -C 5烷基氨基，二-C 1 -C 5烷基氨基，-NO 2，羧基或羟基 ; 而An是阴离子。 此外，本发明涉及新颖的杂环化合物，其组合物，特别是其它染料，以及其制备和应用于染发的方法。
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公开(公告)号：US20100000029A1
公开(公告)日：2010-01-07
申请号：US12310118
申请日：2007-08-08
IPC分类号： A61K8/49 , C09B29/036
CPC分类号： C09B44/16 , A61K8/4946 , A61Q5/065 , A61Q5/10 , C09B49/00 , C09B55/003 , C09B56/18
摘要： Disclosed are thiol dyes of formula (1) wherein L1 is hydrogen; C1-C12alkyl; or phenyl-C1-C4alkyl; X is C1-C12alkylene, C2-C12alkenylene, C5-C10cycloalkylene, C5-C10arylene, or C5-C10arylene-C1-C10alkylene, which may by interrupted by —O—, —NH—, —S—, —CO—, o-SO2—; Y is the residue of an organic dye Z is a group of formula (1b) or —C≡N; wherein A is O; S; or N-L2; B is L3; —OL3; —NL3L4; or —SL3; and L2, L3 and L4, independently from other are hydrogen; C1-C12alkyl; C5-C12aryl-C1-C12alkyl. The compounds are useful for the dyeing of organic materials, such as keratin fibers, preferably human hair.
摘要翻译： 公开了式（1）的硫醇染料，其中L 1是氢; C 1 -C 12烷基; 或苯基-C 1 -C 4烷基; X是C 1 -C 12亚烷基，C 2 -C 12亚烯基，C 5 -C 10亚环烷基，C 5 -C 10亚芳基或C 5 -C 10亚芳基-C 1 -C 10亚烷基，其可以被-O - ， - NH - ， - S-， - CO- SO2-; Y是有机染料的残基Z是式（1b）或-C≡N的基团; 其中A为O; S; 或N-L2; B是L3; -OL3; -NL3L4; 或-SL3; 和L2，L3和L4独立地是氢; C 1 -C 12烷基; C5-C12芳基-C1-C12烷基。 该化合物可用于染色有机材料，例如角蛋白纤维，优选人发。
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公开(公告)号：US20100000028A1
公开(公告)日：2010-01-07
申请号：US11922069
申请日：2006-06-07
IPC分类号： A61K8/49 , C07D401/12 , A61Q5/10
CPC分类号： C09B23/14 , A61K8/4926 , A61Q5/10 , C09B23/145 , C09B49/00
摘要： Disclosed are styryl sulfide dyes of formula (1), wherein R1, R′1, R2, R′2, R3 and R′3, independently from each other are hydrogen; C1-C20alkyl or C1-C20alkoxy, which may be substituted by one or more C1-C5alkoxy, halogen, —NH2, mono-C1-C5alkylamino, di-C1-C5alkylamino, —NO2 or hydroxy; C3-C6cycloalkyl; —C(O)H; —C(O)—C1-C5alkyl; halogen; NO2; OH; phenyl, which may be substituted by one or more C1-C5alkyl, C1-C5alkoxy, halogen, —NH2, mono-C1-C5alkylamino, di-C1-C5alkylamino, —NO2 or hydroxy; or a radical of formula —NR4R5, wherein R4 and R5 independently from each other are hydrogen; C1-C12alkyl, which may be substituted by one or more C1-C5alkyl, C1-C5-alkoxy, hydroxy or —(CO)—H; —(CO)—C1-C5alkyl; phenyl or phenyl-C1-C4alkyl, wherein the phenyl moiety may be substituted by one or more C1-C5alkyl, C1-C5alkoxy, halogen, —N2, mono-C1-C5alkylamino, di-C1-C5alkylamino, —NO2, carboxy or hydroxy; W1, W′1, W2, W′2, W3, W′3, W4 or W′4, independently from each other are —CH— or —N+—; wherein only one of W1/W′1, W2/W′2, W3/W′3, W4/W4′ is —N+; and the bivalent radical -Q-Z-Y—S—S—Y′-Z′-Q′- is bonded to W1 or W2 and W′1 or W′2 respectively; Y1 and Y2 independently from each other are C1-C10alkylene; C5-C10cycloalkylene; C5-C12arylene; or C5-C12arylene-(C1-C10alkylene); Q and Q′ independently from each other are the direct bond; or —C(O)—; —C(O)O—; —OCO—; —N(R6)—; formula (AA); —C(O)N(R6)—; —(R6)NC(O)—; —O—; —S—; —S(O)—; or —S(O)2—; and R6 and R7 independently from each other are hydrogen; C1-C14alkyl; C2-C14alkenyl; C6-C12aryl; C6-C12aryl-C1-C10alkyl; or C1-C10alkyl(C5-C12aryl). Further, the present invention relates to novel styryl sulfide compounds, compositions thereof, especially comprising other dyes, and to processes for their preparation.
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公开(公告)号：US07229479B2
公开(公告)日：2007-06-12
申请号：US10525469
申请日：2003-08-26
申请人： Beate Fröhling , Victor Paul Eliu
发明人： Beate Fröhling , Victor Paul Eliu
IPC分类号： A61K7/13
CPC分类号： A61K8/4966 , A61Q5/065 , C07C245/24 , C09B67/0079
摘要： A method of coloring porous material, especially human hair, is described, which method comprises applying to the material being colored, in any desired order successively, or simultaneously, a) at least one capped diazonium compound and b) at least one cationic water-soluble aromatic coupling component, under conditions such that, initially, coupling does not take place, and then causing the capped diazonium compound present on the material to react with the coupling component.
摘要翻译： 描述了多孔材料，特别是人发的着色方法，该方法包括以任何所需顺序连续地或同时施用着色的材料，a）至少一种封端的重氮化合物和b）至少一种阳离子水溶性聚合物， 在最初不发生偶合的条件下，然后使存在于材料上的封端重氮化合物与偶联组分反应的条件下进行。
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公开(公告)号：US07166711B2
公开(公告)日：2007-01-23
申请号：US10783256
申请日：2004-02-20
申请人： Victor Paul Eliu , Beate Fröhling
发明人： Victor Paul Eliu , Beate Fröhling
CPC分类号： C09B69/065 , A61K8/4946 , A61Q5/065 , C09B44/103
摘要： The present invention relates to novel cationic dye of formula (1) wherein R1 and R7 are each independently of the other hydrogen, hydroxyl; unsubstituted or substituted C1–C6alkyl, aryl radical or C114 C6alkoxy; or —NR3R4, wherein R3 and R4 are each independently of the other hydrogen, unsubstituted or substituted aryl radical or C1–C6alkyl, and R2 is hydrogen, hydroxyl, unsubstituted or substituted C1–C6alkyl, aryl radical or C1–C6alkoxy, —NR3R4, or an organic radical of formula (2) wherein R5 is hydrogen, unsubstituted or substituted aryl radical or C1–C6alkyl, and X− is an anion. Further, the present invention relates to compositions thereof, especially comprising other dyes, to processes for the preparation thereof and to the use thereof in the dyeing of organic material, such as keratin, wool, leather, silk, cellulose or polyamides, and preferably human hair.
摘要翻译： 本发明涉及式（1）的新型阳离子染料，其中R 1和R 7各自独立地为氢，羟基; 未取代或取代的C 1 -C 6烷基，芳基或C 1〜14 C 6烷氧基; 或-NR 3 R 4，其中R 3和R 4各自独立地为另一个氢，未取代的 或取代的芳基或C 1 -C 6烷基，R 2是氢，羟基，未取代或取代的C 1 -C 6烷基， C 1 -C 6烷基，芳基或C 1 -C 6烷氧基，-NR 3 R 或其中R 5为氢的式（2）的有机基团，未取代或取代的芳基或C 1 -C 3 > 6个烷基，X - 是一个阴离子。 此外，本发明涉及其组合物，特别是其它染料，其制备方法及其在染色有机材料如角蛋白，羊毛，皮革，丝，纤维素或聚酰胺，优选人 头发。
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公开(公告)号：US07828858B2
公开(公告)日：2010-11-09
申请号：US11992929
申请日：2006-09-13
IPC分类号： A61Q5/10 , C07D277/26
CPC分类号： A61Q5/10 , A61K8/46 , A61K8/49 , A61K8/492 , A61K8/4926 , A61K8/4946 , A61K8/496 , A61K8/498 , C09B67/0033 , C09B67/0034
摘要： Disclosed are mixtures of sulfide dyes and dyeing compositions comprising mixtures of sulfide dyes. The dye mixtures are useful for the dyeing of organic materials, such as keratin fibers, preferably human hair.
摘要翻译： 公开了硫化染料和包含硫化染料混合物的染色组合物的混合物。 染料混合物可用于染色有机材料，例如角蛋白纤维，优选人发。
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公开(公告)号：US20090300857A1
公开(公告)日：2009-12-10
申请号：US11990813
申请日：2006-08-21
IPC分类号： A61K8/46 , C09B29/036 , C07D213/53 , A61Q5/10
CPC分类号： A61Q5/10 , A61K8/4926 , C09B23/145 , C09B26/04 , C09B44/107
摘要： Disclosed are thiol dyes of formula (1), wherein R1, R2, R3, R4 and R5 independently from each other are hydrogen; unsubstituted or substituted, straight-chain or branched, monocyclic or polycyclic, interrupted or uninterrupted C1-C14alkyl; C2-C14alkenyl; C6-C10aryl; C6-C10aryl-C1-C10alkyl; or C5-C10alkyl(C5-C10aryl); A is a residue of an organic dye; and Y1 is the direct bond; C1-C10alkylene; C5-C10cycloalkylene; C5-C12arylene; or C5-C12arylene-(C1-C10alkylene). The compounds are used to dye hair with or without reducing agents. Furthermore, the present invention relates to compositions comprising thiol dyes of formula (1) and to process for the preparation of theses compounds.
摘要翻译： 公开了式（1）的硫醇染料，其中R 1，R 2，R 3，R 4和R 5彼此独立地为氢; 直链或支链的单环或多环，中断或不间断的C 1 -C 14烷基; C2-C14烯基; C6-C10芳基; C 6 -C 10芳基-C 1 -C 10烷基; 或C 5 -C 10烷基（C 5 -C 10芳基）; A是有机染料的残留物; Y1是直接键; C1-C10亚烷基; C5-C10环亚烷基; C5-C12亚芳基 或C 5 -C 12亚芳基 - （C 1 -C 10亚烷基）。 这些化合物用于染发有或没有还原剂的头发。 此外，本发明涉及包含式（1）的硫醇染料和用于制备这些化合物的方法的组合物。
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