Synthetic quartz growth
    3.
    发明授权
    Synthetic quartz growth 失效
    合成石英生长

    公开(公告)号:US3356463A

    公开(公告)日:1967-12-05

    申请号:US49001865

    申请日:1965-09-24

    CPC classification number: C30B7/00 C30B29/20

    Abstract: 1,153,802. Synthetic quartz. WESTERN ELECTRIC CO., Inc. 8 Sept., 1966 [24 Sept., 1965], No. 40112/66. Heading C1A. Quartz crystals are synthesized by disposing a quartz crystal seed and a mass of nutrient SiO 2 in a pressure vessel, at least 60% of the volume of which is filled with an aqueous medium comprising sodium ions, lithium ions and nitrite anions in concentrations of at least 0À2, 0À02 and 0À02 molar respectively, sealing the vessel and heating it to obtain a temperature of at least 300‹ C. in the aqueous medium while maintaining the temperature of the nutrient mass at least 15‹ C. above that of the seed. The preferred sources of ions are NaOH or Na 2 CO 3 and LiNO 2 . The temperature of the aqueous medium is preferably 350-573‹ C. and the concentration of nitrite ions is preferably 0À02-0À15.

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