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    Multifunctional allyl carbamates and coatings therefrom
    1.
    发明授权
    Multifunctional allyl carbamates and coatings therefrom 失效
    多功能烯丙基氨基甲酸酯及其涂料

    公开(公告)号：US06780951B2

    公开(公告)日：2004-08-24

    申请号：US10314608

    申请日：2002-12-09

    申请人： Daniel B. Pourreau ,  Peter J. Whitman ,  Stephen L. Goldstein ,  Stephen H. Harris

    发明人： Daniel B. Pourreau ,  Peter J. Whitman ,  Stephen L. Goldstein ,  Stephen H. Harris

    IPC分类号： C08L7516

    CPC分类号： C07C271/24 ,  C07C269/02 ,  C07C271/12 ,  C07C2601/14

    摘要： Allyl carbamates are disclosed. The allyl carbamates are prepared by reacting an isocyanate with an allylic alcohol or alkoxylated allylic alcohol. Suitable isocyanates are selected from hexamethylene diisocyanate (HDI), HDI biuret, dimer, HDI trimer, HDI allophanate, isophorone diisocyanate (IPDI), IPDI trimer, IPDI allophanate, bis(isocyanatocyclohexyl)methane, and mixtures thereof. The allyl carbamates have at least two allyl functional groups per molecule. UV-curable and air-drying coatings formulated from the allyl carbamates show excellent chemical resistance and physical properties.

    摘要翻译： 公开了烯丙基氨基甲酸酯。 通过使异氰酸酯与烯丙基醇或烷氧基化烯丙基醇反应来制备烯丙基氨基甲酸酯。 合适的异氰酸酯选自六亚甲基二异氰酸酯（HDI），HDI缩二脲，二聚体，HDI三聚体，HDI脲基甲酸酯，异佛尔酮二异氰酸酯（IPDI），IPDI三聚体，IPDI脲基甲酸酯，双（异氰酸根合环己基）甲烷及其混合物。 烯丙基氨基甲酸酯每分子具有至少两个烯丙基官能团。 由烯丙基氨基甲酸酯配制的紫外线固化和空气干燥涂料显示出优异的耐化学性和物理性能。

    Multifunctional allyl carbamates and coatings therefrom
    2.
    发明授权
    Multifunctional allyl carbamates and coatings therefrom 失效
    多功能烯丙基氨基甲酸酯及其涂料

    公开(公告)号：US06555596B1

    公开(公告)日：2003-04-29

    申请号：US09706629

    申请日：2000-11-06

    申请人： Daniel B. Pourreau ,  Peter J. Whitman ,  Stephen L. Goldstein ,  Stephen H. Harris

    发明人： Daniel B. Pourreau ,  Peter J. Whitman ,  Stephen L. Goldstein ,  Stephen H. Harris

    IPC分类号： C08F246

    CPC分类号： C07C271/24 ,  C07C269/02 ,  C07C271/12 ,  C07C2601/14

    摘要： Allyl carbamates are disclosed. The allyl carbamates are prepared by reacting an isocyanate with an allylic alcohol or alkoxylated allylic alcohol. Suitable isocyanates are selected from hexamethylene diisocyanate (HDI), HDI biuret, dimer, HDI trimer, HDI allophanate, isophorone diisocyanate (IPDI), IPDI trimer, IPDI allophanate, bis(isocyanatocyclohexyl)methane, and mixtures thereof. The allyl carbamates have at least two allyl functional groups per molecule. UV-curable and air-drying coatings formulated from the allyl carbamates show excellent chemical resistance and physical properties.

    摘要翻译： 公开了烯丙基氨基甲酸酯。 通过使异氰酸酯与烯丙基醇或烷氧基化烯丙基醇反应来制备烯丙基氨基甲酸酯。 合适的异氰酸酯选自六亚甲基二异氰酸酯（HDI），HDI缩二脲，二聚体，HDI三聚体，HDI脲基甲酸酯，异佛尔酮二异氰酸酯（IPDI），IPDI三聚体，IPDI脲基甲酸酯，双（异氰酸根合环己基）甲烷及其混合物。 烯丙基氨基甲酸酯每分子具有至少两个烯丙基官能团。 由烯丙基氨基甲酸酯配制的紫外线固化和空气干燥涂料显示出优异的耐化学性和物理性能。

    Urethane compositions
    3.
    发明授权
    Urethane compositions 失效
    聚氨酯组合物

    公开(公告)号：US06245877B1

    公开(公告)日：2001-06-12

    申请号：US09558913

    申请日：2000-04-26

    申请人： Carmen L. Rodriguez ,  Stephen L. Goldstein

    发明人： Carmen L. Rodriguez ,  Stephen L. Goldstein

    IPC分类号： C08G1848

    CPC分类号： C09D175/08 ,  C08G18/12 ,  C08G18/4879 ,  C08G18/307

    摘要： A moisture-cure urethane composition is disclosed. The urethane is formulated from an NCO-terminated alkoxylated phenolic resin that has long oxyalkylene chains. It has greater than 70 wt % solids and has excellent resistance to acids, bases, and chemicals.

    摘要翻译： 公开了一种湿固化的聚氨酯组合物。 氨基甲酸酯由具有长氧化烯链的NCO封端的烷氧基化酚醛树脂制成。 它具有大于70重量％的固体，并具有优异的抗酸，碱和化学物质。

    Process for producing uretidione dimers of isocyanates using catalysts which are bound to inorganic matrices
    5.
    发明授权
    Process for producing uretidione dimers of isocyanates using catalysts which are bound to inorganic matrices 失效
    使用与无机基质结合的催化剂生产异氰酸酯的脲基二酮二聚体的方法

    公开(公告)号：US5315004A

    公开(公告)日：1994-05-24

    申请号：US43075

    申请日：1993-04-05

    申请人： Stephen L. Goldstein ,  Anthony D. Hamer ,  Lawrence E. Katz ,  Michael J. McGeary ,  Curtis P. Smith

    发明人： Stephen L. Goldstein ,  Anthony D. Hamer ,  Lawrence E. Katz ,  Michael J. McGeary ,  Curtis P. Smith

    IPC分类号： C07D229/00 ,  C08G18/79 ,  C08G18/74

    CPC分类号： C07D229/00 ,  C08G18/798

    摘要： This invention relates to a process for preparing a dimer by the steps of: (a) cyclodimerizing a polyisocyanate in the presence of a dimerization catalyst which is covalently bound to an insoluble inorganic matrix by contacting said polyisocyanate with said catalyst at a temperature of between about 20 and about 135.degree. C. in a reaction to form an uretidione-containing cyclodimerized isocyanate wherein a portion of the isocyanate moieties comprising said polyisocyanate are converted to uretidione groups, and (b) separating said catalyst from said cyclodimerized isocyanate in order to stop said reaction after a desired amount of isocyanate moieties in said polyisocyanate have been converted to uretidione moieties.

    摘要翻译： 本发明涉及一种通过以下步骤制备二聚体的方法：（a）在二聚催化剂的存在下使多异氰酸酯进行环二聚，所述二聚催化剂与不溶性无机基质共价结合，所述二聚催化剂通过使所述多异氰酸酯与所述催化剂在约 20和约135℃，以形成含有脲基二酮的环二聚异氰酸酯，其中将包含所述多异氰酸酯的部分异氰酸酯部分转化为脲基二酰基，和（b）从所述环二聚体异氰酸酯分离所述催化剂，以便停止所述 在所述多异氰酸酯中所需量的异氰酸酯部分已经转化成脲基二酮部分后的反应。

    Process for producing low viscosity isocyanate trimers
    6.
    发明授权
    Process for producing low viscosity isocyanate trimers 失效
    生产低粘度异氰酸酯三聚体的方法

    公开(公告)号：US5298431A

    公开(公告)日：1994-03-29

    申请号：US767946

    申请日：1991-09-30

    申请人： Stephen L. Goldstein ,  Edward A. Barsa

    发明人： Stephen L. Goldstein ,  Edward A. Barsa

    IPC分类号： C07D251/34 ,  C08G18/79 ,  C08F6/00 ,  C08F6/10

    CPC分类号： C08G18/791 ,  C07D251/34

    摘要： This invention relates to a multi-step process for isolating a cyclotrimerized isocyanate from mixture containing said cyclotrimerized isocyanate plus an isocyanate oligomer which comprises the steps of: (a) contacting said mixture with a liquid solvent to provide a solvent-containing mixture, (b) extracting said solvent-containing mixture by liquid-liquid extraction to cause said solvent-containing mixture to elute into an extractate and a residue, wherein said extractate is a cyclotrimerized isocyanate that is essentially oligomer-free and is further characterized by having reduced viscosity relative to said solvent-containing mixture, and (c) separating uncyclotrimerized monomer from said extractate to provide a reduced viscosity trimer product that is essentially free of monomer. Also disclosed is the reduced-viscosity product produced by this process.

    摘要翻译： 本发明涉及一种用于从含有所述环化三聚异氰酸酯加异氰酸酯低聚物的混合物中分离环三聚化的异氰酸酯的多步骤方法，其包括以下步骤：（a）使所述混合物与液体溶剂接触以提供含溶剂的混合物，（b ）通过液 - 液萃取萃取所述含溶剂的混合物以使所述含溶剂的混合物洗脱至萃取物和残余物中，其中所述萃取物是基本上无低聚物的环状三聚化的异氰酸酯，并且进一步的特征在于具有降低的粘度相对 到所述含溶剂的混合物，和（c）从所述提取物中分离未环化三聚的单体以提供基本上不含单体的比较粘度的三聚体产物。 还公开了通过该方法生产的降粘产品。

    Low VOC, moisture curable, two-component coating compositions based on organic polyisocyanates
    9.
    发明授权
    Low VOC, moisture curable, two-component coating compositions based on organic polyisocyanates 失效
    基于有机多异氰酸酯的低VOC，可湿固化的双组分涂料组合物

    公开(公告)号：US5506328A

    公开(公告)日：1996-04-09

    申请号：US64996

    申请日：1993-05-24

    申请人： Kiran B. Chandalia ,  Michael J. Morgan ,  James M. O'Connor ,  Stephen L. Goldstein

    发明人： Kiran B. Chandalia ,  Michael J. Morgan ,  James M. O'Connor ,  Stephen L. Goldstein

    IPC分类号： C08G18/18 ,  C08G18/30 ,  C09D175/00 ,  B05D3/04 ,  C08K5/00

    CPC分类号： C09D175/00 ,  C08G18/1825 ,  C08G18/302 ,  C08G18/307

    摘要： This invention relates to a process for coating a substrate comprising contacting the substrate with a low volatile organics, moisture curable, two-component coating composition comprising an admixture of an A-side and a B-side, said A-side comprising an aliphatic polyisocyanate having an isocyanate index relative to the number of isocyanate-reactive groups in said coating composition of at least about 200, preferably at least about 300, more preferably at least about 500, said B-side comprising a tertiary amine catalyst and optionally an isocyanate-reactive compound selected from the group consisting of monoahls, polyols, imines, oxazolidines, and combinations thereof, said coating composition optionally containing a solvent in an amount of less than about 45%, based upon the weight of the polyisocyanate in said coating composition, said coating composition having a viscosity as measured by ZAHN cup 2 of less than about 200 seconds, said composition being essentially free of any volatile mono- and di-isocyanates, and said composition being moisture curable upon exposure to atmospheric moisture. Also claimed is the coating composition itself.

    摘要翻译： 本发明涉及一种涂覆基质的方法，包括使基底与低挥发性有机物，可湿固化的双组分涂料组合物接触，该组合物包含A侧和B侧的混合物，所述A侧包含脂族多异氰酸酯 具有相对于所述涂料组合物中的异氰酸酯反应性基团数量的异氰酸酯指数为至少约200，优选至少约300，更优选至少约500，所述B侧包含叔胺催化剂和任选的异氰酸酯 - 选自单酚，多元醇，亚胺，恶唑烷及其组合的反应性化合物，所述涂料组合物任选地含有基于所述涂料组合物中多异氰酸酯重量的小于约45％的溶剂，所述 具有通过ZAHN杯2测量的粘度小于约200秒的涂料组合物，所述组合物基本上不含任何挥发物 单一和二异氰酸酯，并且所述组合物在暴露于大气湿气时是可湿气固化的。 还要求的是涂料组合物本身。

    Process for producing isocyanurates by cyclotrimerizing isocyanates using polymer-bound catalysts
    10.
    发明授权
    Process for producing isocyanurates by cyclotrimerizing isocyanates using polymer-bound catalysts 失效
    使用聚合物结合的催化剂通过环状三聚异氰酸酯制备异氰脲酸酯的方法

    公开(公告)号：US5221743A

    公开(公告)日：1993-06-22

    申请号：US844265

    申请日：1992-03-02

    申请人： Stephen L. Goldstein ,  Curtis P. Smith

    发明人： Stephen L. Goldstein ,  Curtis P. Smith

    IPC分类号： C07D251/34 ,  C08G18/02 ,  C08G18/16 ,  C08G18/18

    CPC分类号： C08G18/16 ,  C07D251/34 ,  C08G18/022 ,  C08G18/1808 ,  Y10S521/902

    摘要： This invention relates to a process for preparing a trimer by the steps of: (a) cyclotrimerizing a polyisocyanate in the presence a polymer-bound trimerization catalyst by contacting said polyisocyanate with said catalyst at a temperature of between about 20.degree. and about 135.degree. C. in a reaction to form an isocyanurate-containing cyclotrimerized isocyanate wherein a portion of the isocyanate moieties comprising said polyisocyanate are converted to isocyanurate groups, and (b) separating said catalyst from said cyclotrimerized isocyanate in order to stop said reaction after a desired amount of isocyanate moieties in said polyisocyanate have been converted to isocyanurate moieties.

    摘要翻译： 本发明涉及通过以下步骤制备三聚体的方法：（a）在聚合物结合的三聚催化剂存在下，通过使所述多异氰酸酯与所述催化剂在约20℃至约135℃的温度下接触来使多异氰酸酯进行环化三聚 在形成含异氰脲酸酯的环状三聚化异氰酸酯的反应中，其中将包含所述多异氰酸酯的部分异氰酸酯部分转化为异氰脲酸酯基团，和（b）将所述催化剂与所述环化三聚化异氰酸酯分离，以便在所需量的 所述多异氰酸酯中的异氰酸酯部分已经转化为异氰脲酸酯部分。