Toner processes
    4.
    发明授权
    Toner processes 失效
    墨粉处理

    公开(公告)号:US06984480B2

    公开(公告)日:2006-01-10

    申请号:US10603449

    申请日:2003-06-25

    IPC分类号: G03G9/08

    CPC分类号: G03G9/0804 G03G9/09725

    摘要: A process comprising heating a mixture of colorant and latex in the presence of a coagulant and a silicate salt, and wherein said heating comprises a first heating equal to or below about the glass transition temperature of a polymer contained in said latex, and a second heating equal to or about the glass transition temperature of a polymer contained in said latex; wherein said first heating enables the formation of aggregates and said second heating enables the fusion of said colorant and said polymer; and optionally wherein said silicate is contained in an alkali metal hydroxide.

    摘要翻译: 一种方法,包括在凝结剂和硅酸盐存在下加热着色剂和胶乳的混合物,并且其中所述加热包括等于或低于所述胶乳中包含的聚合物的玻璃化转变温度的第一加热,和第二加热 等于或约为所述胶乳中包含的聚合物的玻璃化转变温度; 其中所述第一加热使得能够形成聚集体,并且所述第二加热使得所述着色剂和所述聚合物融合; 并且任选地,其中所述硅酸盐包含在碱金属氢氧化物中。

    Photochromic gyricon display
    7.
    发明授权
    Photochromic gyricon display 有权
    光致变色显示屏

    公开(公告)号:US06549327B2

    公开(公告)日:2003-04-15

    申请号:US09864386

    申请日:2001-05-24

    IPC分类号: G09G308

    CPC分类号: G02B26/026 C07D491/10

    摘要: Disclosed is a display comprising an arrangement of a plurality of optically anisotropic rotatable elements, each of the rotatable elements having a surface in contact with an enabling fluid, the rotatable elements being electrically dipolar in the presence of the enabling fluid and thus being subject to rotation upon application of an electric field, the rotatable elements being free to rotate in place but not free to translate substantially so as to disrupt the arrangement of rotatable elements, wherein a first portion of the surface contains a mixture of a chelating agent and a spiropyran material of the formula wherein n is an integer representing the number of repeat —CH2— units and R is —H or —CH═CH2, and wherein a second portion of the surface contains substantially no spiropyran.

    摘要翻译: 公开了一种显示器,其包括多个光学各向异性可旋转元件的布置,每个可旋转元件具有与启用流体接触的表面,可旋转元件在有效流体存在的情况下是电偶极性的,因此被旋转 在施加电场时,可旋转元件可自由旋转到位,但不能自由平移以便基本上平移以便破坏可旋转元件的布置,其中表面的第一部分包含螯合剂和螺吡喃材料的混合物 其中n是表示重复-CH 2 - 单元的数目的整数,并且R是-H或-CH = CH 2,并且其中该表面的第二部分基本上不含螺吡喃。

    Toner aggregation processes
    8.
    发明授权
    Toner aggregation processes 有权
    调色剂聚合过程

    公开(公告)号:US06210853B1

    公开(公告)日:2001-04-03

    申请号:US09657340

    申请日:2000-09-07

    IPC分类号: G03G9087

    摘要: A process for the preparation of toner including (i) gerating by emulsion polymerization in the presence of an initiator a first resin latex emulsion; (ii) generating by polycondensation a second resin latex optionally in the presence of a catalyst; (iib) dispersing the resin of (ii) in water; (iii) mixing (iib) with a colorant thereby providing a colorant dispersion; (iiib) mixing the resin latex emulsion of (i) with the resin/colorant mixture of (iii) to provide a blend of a resin and colorant; (iv) adding an aqueous inorganic cationic coagulant solution of a polymeric metal salt and optionally an organic cationic coagulant to the resin/colorant blend of (iiib); (v) heating at a temperature of from about 5 to about 10 degrees Centigrade below the resin Tg of (i), to thereby form aggregate particles and which particles are optionally at a pH of from about 2 to about 3.5; (vi) adjusting the pH of (v) to about 6.5 to about 9 by the addition of a base; (vii) heating the aggregate particles of (v) at a temperature of from about 5 to about 50 degrees Centigrade above the Tg of the resin of (i), followed by a reduction of the pH to from about 2.5 to about 5 by the addition of an acid resulting in coalesced toner; (viii) optionally isolating the toner.

    摘要翻译: 一种制备调色剂的方法,包括(i)在引发剂存在下通过乳液聚合第一树脂胶乳乳液; (ii)任选地在催化剂存在下通过缩聚产生第二树脂胶乳; (iib)将(ii)的树脂分散在水中; (iii)将混合(iib)与着色剂混合,从而提供着色剂分散体; (iiib)将(i)的树脂胶乳乳液与(iii)的树脂/着色剂混合物混合以提供树脂和着色剂的共混物; (iv)将聚合金属盐和任选的有机阳离子凝结剂的无机阳离子凝结剂水溶液加入到(iiib)的树脂/着色剂混合物中; (v)在(i)的树脂Tg以下约5至约10摄氏度的温度下加热,从而形成聚集体颗粒,并且哪些颗粒任选处于约2至约3.5的pH值; (vi)通过添加碱将(v)的pH调节至约6.5至约9; (vii)在(i)的树脂的Tg以上约5至约50摄氏度的温度下加热(ⅴ)的聚集体颗粒,随后将pH降低至约2.5至约5 加入导致聚结的调色剂的酸; (viii)任选地分离调色剂。

    Toner processes
    9.
    发明授权
    Toner processes 有权
    墨粉处理

    公开(公告)号:US06190820B1

    公开(公告)日:2001-02-20

    申请号:US09657273

    申请日:2000-09-07

    IPC分类号: G03G9087

    CPC分类号: G03G9/0804 G03G9/0806

    摘要: A process for the preparation of toner by, for example (i) generating by emulsion polymerization in the presence of an initiator a first resin latex emulsion; (ii) generating in the presence of an oil soluble initiator by solution polymerization a second resin latex; (iii) mixing (ii) with a colorant; (iiib) mixing the resin latex emulsion of (i) with the resin/colorant mixture of (iii) to provide a blend of a resin and colorant; (iv) adding an aqueous inorganic cationic coagulant solution of a metal salt and optionally an organic cationic coagulant to the resin/colorant blend of (iiib); (v) heating at a temperature of from about 5° C. to about 10° C. below the resin Tg of (i), to form aggregate particles; (vi) adjusting the pH of (v) by the addition of a base; (vii) heating the aggregate particles of (v) at temperatures of from about 5° C. to about 50° C. above the Tg of the resin of (i), followed by the addition of an acid.

    摘要翻译: 通过例如(i)在引发剂存在下通过乳液聚合产生第一树脂胶乳乳液来制备调色剂的方法;(ii)通过溶解聚合在油溶性引发剂的存在下产生第二树脂胶乳; (iii)将(ii)与着色剂混合;(iiib)将(i)的树脂胶乳乳液与(iii)的树脂/着色剂混合物混合以提供树脂和着色剂的共混物;(iv) (iiib)的树脂/着色剂共混物中的金属盐和任选的有机阳离子凝结剂的阳离子凝结剂溶液;(v)在温度为约5℃至约10℃的温度下加热至( i),以形成聚集体颗粒;(vi)通过加入碱来调节(v)的pH;(vii)在约5℃至约50℃的温度下加热(v)的聚集体颗粒 高于(i)的树脂的Tg,然后加入酸。