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    Process for producing ammonium salts
    2.
    发明授权
    Process for producing ammonium salts 有权
    生产铵盐的方法

    公开(公告)号：US08309048B2

    公开(公告)日：2012-11-13

    申请号：US13088754

    申请日：2011-04-18

    Applicant: Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf ,  Michael J. Bayer

    Inventor： Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf ,  Michael J. Bayer

    IPC: B01D53/58 ,  C01C1/242

    CPC classification number: C07C209/86 ,  B01D15/00 ,  B01D53/58 ,  B01D2251/50 ,  B01D2257/406 ,  C01C1/242 ,  C07D291/06 ,  C07C211/05

    Abstract: The invention relates to a process for producing an ammonium salt composition. The process comprises the step of providing a process stream comprising sulfuric acid, methylene dichloride, and a tertiary amine or a precursor thereof. The process further comprises the step of contacting the process stream with ammonia to form a product stream and a waste stream. The product stream comprises the ammonium salt and the waste stream comprises water, methylene dichloride, ammonia, and the tertiary amine. The process further comprises the step of deriving from the waste stream an off gas stream comprising ammonia and a first amount of methylene dichloride. The process also comprises the step of contacting at least a portion of the off gas stream or a derivative thereof with an adsorbent to separate at least a portion of the off gas into a methylene dichloride stream comprising methylene dichloride.

    Abstract translation: 本发明涉及一种生产铵盐组合物的方法。 该方法包括提供包含硫酸，二氯甲烷和叔胺或其前体的工艺流的步骤。 该方法还包括将工艺流与氨接触以形成产物流和废物流的步骤。 产物流包含铵盐，废物流包含水，二氯甲烷，氨和叔胺。 该方法还包括从废物流中导出包含氨和第一量二氯甲烷的废气流的步骤。 该方法还包括使至少一部分废气流或其衍生物与吸附剂接触以将至少一部分废气分离成包含二氯甲烷的二氯甲烷流的步骤。

    Process for producing ammonium salts
    3.
    发明授权
    Process for producing ammonium salts 有权
    生产铵盐的方法

    公开(公告)号：US08303921B2

    公开(公告)日：2012-11-06

    申请号：US13088734

    申请日：2011-04-18

    Applicant: Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf ,  Michael J. Bayer

    Inventor： Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf ,  Michael J. Bayer

    IPC: B01D53/58 ,  C01C1/242

    CPC classification number: C07C209/86 ,  B01D15/00 ,  B01D53/58 ,  B01D2251/50 ,  B01D2257/406 ,  C01C1/242 ,  C07D291/06 ,  C07C211/05

    Abstract: The invention relates to a process of producing an ammonium salt composition. The process comprises the step of providing a process stream comprising sulfuric acid and at least one tertiary amine. The process further comprises the step of contacting the process stream with ammonia to form a waste stream and a product stream. The waste stream comprises water, tertiary amine, and ammonia and the product stream comprises a first amount of ammonium salt. The process further comprises the step of deriving from the waste stream an off gas stream comprising a preliminary amount of ammonia. The process also comprises the step of contacting the off gas stream with an acid to form an ammonium salt stream and a purge stream. The ammonium salt stream comprises a second amount of ammonium salt and the purge stream comprises a reduced amount of ammonia, which is less than the preliminary amount.

    Abstract translation: 本发明涉及一种生产铵盐组合物的方法。 该方法包括提供包含硫酸和至少一种叔胺的工艺流的步骤。 该方法还包括使工艺流与氨接触以形成废物流和产物流的步骤。 废物流包含水，叔胺和氨，产物流包含第一量的铵盐。 该方法还包括从废物流中导出包含初步量的氨的废气流的步骤。 该方法还包括使废气流与酸接触以形成铵盐流和吹扫流的步骤。 铵盐料流包含第二量的铵盐，并且吹扫流包含少量的氨，其小于初步量。

    Method for the Manufacture of an Ammonium Sulfate Composition
    4.
    发明申请
    Method for the Manufacture of an Ammonium Sulfate Composition 有权
    制造硫酸铵组合物的方法

    公开(公告)号：US20130064755A1

    公开(公告)日：2013-03-14

    申请号：US13640330

    申请日：2011-04-13

    Applicant: Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf

    Inventor： Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf

    IPC: C01C1/242 ,  C01C1/24

    CPC classification number: C01C1/242 ,  C01B17/905 ,  C01B17/92 ,  C01C1/24 ,  C07C209/86 ,  C07C211/05

    Abstract: The present invention describes a method manufacture of an ammonium sulfate composition having a total organic carbon (TOC) content of 1% by weight or less than 1% by weight, based on the total weight of the composition, comprising the following steps: a) reacting i) waste sulfuric acid comprising an organic tertiary amines with ii) ammonia in an amount sufficient to obtain a pH of 9.5 or higher b) separating the organic tertiary amine from the reaction mixture obtained in step a) wherein during the separation the pH of the reaction mixture is maintained at a pH higher than 10 and c) optionally reducing the content of water and/or other volatile components from the aqueous solution comprising the ammonium sulfate.

    Abstract translation: 本发明描述了基于组合物的总重量，总有机碳（TOC）含量为1重量％或小于1重量％的硫酸铵组合物的方法制备方法，包括以下步骤：a） 使i）将含有有机叔胺的硫酸废物与ii）足以获得pH值为9.5或更高的量的氨b）从步骤a）中获得的反应混合物中分离出有机叔胺，其中在分离过程中， 反应混合物保持在高于10的pH，并且c）任选地从包含硫酸铵的水溶液中降低水和/或其它挥发性组分的含量。

    Method for the manufacture of an ammonium sulfate composition
    5.
    发明授权
    Method for the manufacture of an ammonium sulfate composition 有权
    硫酸铵组合物的制造方法

    公开(公告)号：US08496905B2

    公开(公告)日：2013-07-30

    申请号：US13640330

    申请日：2011-04-13

    Applicant: Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf

    Inventor： Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf

    IPC: C01C1/242

    CPC classification number: C01C1/242 ,  C01B17/905 ,  C01B17/92 ,  C01C1/24 ,  C07C209/86 ,  C07C211/05

    Abstract: The present invention describes a method manufacture of an ammonium sulfate composition having a total organic carbon (TOC) content of 1% by weight or less than 1% by weight, based on the total weight of the composition, comprising the following steps: a) reacting i) waste sulfuric acid comprising an organic tertiary amines with ii) ammonia in an amount sufficient to obtain a pH of 9.5 or higher b) separating the organic tertiary amine from the reaction mixture obtained in step a) wherein during the separation the pH of the reaction mixture is maintained at a pH higher than 10 and c) optionally reducing the content of water and/or other volatile components from the aqueous solution comprising the ammonium sulfate.

    Abstract translation: 本发明描述了基于组合物的总重量，总有机碳（TOC）含量为1重量％或小于1重量％的硫酸铵组合物的方法制备方法，包括以下步骤：a） 使i）将含有有机叔胺的硫酸废物与ii）足以获得pH值为9.5或更高的量的氨b）从步骤a）中获得的反应混合物中分离出有机叔胺，其中在分离过程中， 反应混合物保持在高于10的pH，并且c）任选地从包含硫酸铵的水溶液中降低水和/或其它挥发性组分的含量。

    Method for the production of a sweetener salt based on aspartame and acesulfame
    6.
    发明申请
    Method for the production of a sweetener salt based on aspartame and acesulfame 审中-公开
    基于阿斯巴甜和乙酰磺胺酸盐生产甜味剂盐的方法

    公开(公告)号：US20070054022A1

    公开(公告)日：2007-03-08

    申请号：US10563155

    申请日：2004-06-26

    Applicant: Peter Groer ,  Gerhard Merkt

    Inventor： Peter Groer ,  Gerhard Merkt

    IPC: A23L1/236

    CPC classification number: C07D291/06 ,  A23L27/30 ,  A23L27/32

    Abstract: This invention relates to a method for producing a sweetener salt of formula APMH+Ace−, according to which aspartame or an aspartame derivative is reacted with acesulfamic acid in a solvent selected among one or several of the following: liquid SO2; halogenated aliphatic hydrocarbons; carbonic acid esters comprising low, aliphatic alcohols; nitroalkanes; alkyl-substituted pyridines; and aliphatic sulfones. The invention also relates to the use of said sweetener salts in food, beverages, pharmaceuticals, and cosmetics.

    Abstract translation: 本发明涉及一种制备式APMH +甜味剂甜味剂盐的方法，根据该方法，将阿斯巴甜或阿斯巴甜衍生物与氨磺胺酸在选自以下的溶剂中反应： 以下中的一种或几种：液体SO 2; 卤代脂族烃; 包含低脂肪醇的碳酸酯; 硝基烷烃; 烷基取代的吡啶; 和脂族砜。 本发明还涉及所述甜味剂盐在食品，饮料，药物和化妆品中的用途。

    Process for producing ammonium salts
    7.
    发明授权
    Process for producing ammonium salts 有权
    生产铵盐的方法

    公开(公告)号：US08663595B2

    公开(公告)日：2014-03-04

    申请号：US13333047

    申请日：2011-12-21

    Applicant: Stephan Brietzke ,  Peter Groer ,  Christoph Mollenkopf ,  Michael J. Bayer

    Inventor： Stephan Brietzke ,  Peter Groer ,  Christoph Mollenkopf ,  Michael J. Bayer

    IPC: C01C1/242 ,  C01C1/24

    CPC classification number: C01C1/24 ,  C07C231/24 ,  C07D291/06 ,  Y02P20/127 ,  C07C237/22

    Abstract: In one embodiment, the invention is to a process for purifying a by-product stream. The process comprises the step of providing a by-product stream comprising an ammonium salt, dimerized amide, and optionally water. The process further comprises the step of precipitating at least a portion of the dimerized amide in the by-product stream to form solid dimerized amide. The process further comprises the step of separating the solid dimerized amide from the by-product stream to form a treated by-product stream comprising less than 1 wt. % solid dimerized amide.

    Abstract translation: 在一个实施方案中，本发明涉及纯化副产物流的方法。 该方法包括提供包含铵盐，二聚酰胺和任选的水的副产物流的步骤。 该方法还包括沉淀副产物流中的二聚酰胺的至少一部分以形成固体二聚酰胺的步骤。 该方法还包括将固体二聚酰胺与副产物流分离以形成经处理的副产物流的步骤，其包含小于1wt。 ％固体二聚酰胺。

    PROCESS FOR PRODUCING AMMONIUM SALTS
    8.
    发明申请
    PROCESS FOR PRODUCING AMMONIUM SALTS 有权
    生产氨水的方法

    公开(公告)号：US20110256045A1

    公开(公告)日：2011-10-20

    申请号：US13088734

    申请日：2011-04-18

    Applicant: Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf ,  Michael J. Bayer

    Inventor： Stephan Brietzke ,  Peter Groer ,  Carl Christoph Mollenkopf ,  Michael J. Bayer

    IPC: B01D53/58 ,  C01C1/242

    CPC classification number: C07C209/86 ,  B01D15/00 ,  B01D53/58 ,  B01D2251/50 ,  B01D2257/406 ,  C01C1/242 ,  C07D291/06 ,  C07C211/05

    Abstract: In one embodiment, the invention is to a process of producing an ammonium salt composition. The process comprises the step of providing a process stream comprising sulfuric acid and at least one tertiary amine. The process further comprises the step of contacting the process stream with ammonia under conditions effective to form a waste stream and a product stream. The waste stream comprises water, the tertiary amine, and ammonia and the product stream comprises a first amount of ammonium salt. The process further comprises the step of deriving from the waste stream an off gas stream comprising a preliminary amount of ammonia. The process also comprises the step of contacting the off gas stream with an acid under conditions effective to form an ammonium salt stream and a purge stream. The ammonium salt stream comprises a second amount of ammonium salt and the purge stream comprises a reduced amount of ammonia, which is less than the preliminary amount.

    Abstract translation: 在一个实施方案中，本发明涉及一种生产铵盐组合物的方法。 该方法包括提供包含硫酸和至少一种叔胺的工艺流的步骤。 该方法还包括在有效形成废物流和产物流的条件下使工艺流与氨接触的步骤。 废物流包含水，叔胺和氨，产物流包含第一量的铵盐。 该方法还包括从废物流中导出包含初步量的氨的废气流的步骤。 该方法还包括在有效形成铵盐流和净化流的条件下使废气流与酸接触的步骤。 铵盐料流包含第二量的铵盐，并且吹扫流包含少量的氨，其小于初步量。

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