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公开(公告)号：US20120149545A1
公开(公告)日：2012-06-14
申请号：US13377198
申请日：2009-06-10
CPC分类号： H01M4/92 , H01M4/8817 , H01M4/926 , H01M8/1004
摘要： An object of the present invention is to provide a platinum catalyst for a fuel cell, the platinum catalyst having platinum particles with a fine particle size which are supported on carbon carriers in a highly dispersed manner. To achieve the above object, the present invention provides a method for producing an electrode catalyst for a fuel cell, the method comprising: an ammonia treatment step of heat-treating carbon carriers in an ammonia gas atmosphere; a platinum salt contact step of mixing the carbon carriers treated with ammonia with a solution prepared by dissolving a platinum salt in a solvent and bringing the platinum salt coming into contact with the carbon carriers in the mixture that has been formed; a recovery step of recovering the carbon carriers by removing the solvent from the mixture; and a heat treatment step of heat-treating the recovered carbon carriers in an inert gas atmosphere.
摘要翻译： 本发明的目的是提供一种用于燃料电池的铂催化剂，铂催化剂具有以高度分散的方式负载在碳载体上的具有细颗粒尺寸的铂颗粒。 为了实现上述目的，本发明提供一种燃料电池用电极催化剂的制造方法，该方法包括：氨气处理工序，对氨载气中的碳载体进行热处理; 将用氨处理的碳载体与通过将铂盐溶解在溶剂中制备的溶液并使铂盐与形成的混合物中的碳载体接触的铂盐接触步骤; 通过从混合物中除去溶剂来回收碳载体的回收步骤; 以及在惰性气体气氛中对回收的碳载体进行热处理的热处理工序。
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2.发明申请METHOD FOR PREPARING FUEL CELL ELECTRODE CATALYST AND SOLID POLYMER FUEL CELL 有权制备燃料电池催化剂和固体聚合物燃料电池的方法公开(公告)号：US20110130270A1
公开(公告)日：2011-06-02
申请号：US13056362
申请日：2008-07-29
申请人： Naoko Iwata , Hiroaki Takahashi , Peter Bogdanoff , Sebastian Fiechter , Iris Herrmann-Geppert , Ulrike Kramm
发明人： Naoko Iwata , Hiroaki Takahashi , Peter Bogdanoff , Sebastian Fiechter , Iris Herrmann-Geppert , Ulrike Kramm
IPC分类号： H01M4/88
CPC分类号： H01M4/9008 , H01M4/8605 , H01M4/8882 , H01M4/9083 , H01M4/923 , H01M4/926 , H01M2008/1095
摘要： According to the present invention, the catalyst performance of a chelate catalyst comprising a complex of a macrocyclic compound such as a porphyrin derivative is improved. Also, the following method is provided: a method for preparing a fuel cell electrode catalyst comprising a nitrogen-containing metal complex in which a metallic element is coordinated with a macrocyclic organic compound, such method comprising the steps of: adding tin oxalate to the nitrogen-containing metal complex; and baking a mixture of the nitrogen-containing metal complex and tin oxalate in an inert gas atmosphere, wherein elution of metal tin is carried out via acid treatment.
摘要翻译： 根据本发明，提高了包含卟啉衍生物等大环化合物的络合物的螯合催化剂的催化剂性能。 另外，提供了以下方法：一种制备燃料电池电极催化剂的方法，该催化剂包含金属元素与大环有机化合物配位的含氮金属络合物，该方法包括以下步骤：向氮中加入草酸锡 含金属络合物; 并在惰性气体气氛中焙烧含氮金属络合物和草酸锡的混合物，其中通过酸处理进行金属锡的洗脱。
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3.发明授权Platinum-free chelate-catalyst material for the selective reduction of oxygen and method for production thereof 失效用于选择性还原氧的无铂螯合催化剂材料及其制备方法公开(公告)号：US07534739B2
公开(公告)日：2009-05-19
申请号：US10482975
申请日：2002-07-03
申请人： Marcus Hilgendorff , Iris Dorbandt , Hendrik Schulenburg , Michael Bron , Sebastian Fiechter , Peter Bogdanoff , Helmut Tributsch
发明人： Marcus Hilgendorff , Iris Dorbandt , Hendrik Schulenburg , Michael Bron , Sebastian Fiechter , Peter Bogdanoff , Helmut Tributsch
CPC分类号： H01M4/9008 , B01J31/06 , B01J31/183 , B01J31/28 , B01J2531/025 , B01J2531/821 , B01J2531/842 , B01J2531/845 , H01M4/9091
摘要： A platinum-free chelate catalyst material consisting of at least one unsupported transition metal, a nitrogen-containing organo-metallic transition complex, a further transition metal other than the unsupported transition metal and a chalcogenic compound.
摘要翻译： 由至少一种未负载的过渡金属，含氮有机金属过渡络合物，除非负载过渡金属以外的其它过渡金属和硫属化合物组成的无铂螯合催化剂材料。
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4.发明授权Method for preparing fuel cell electrode catalyst and solid polymer fuel cell 有权制备燃料电池电极催化剂和固体聚合物燃料电池的方法公开(公告)号：US08455384B2
公开(公告)日：2013-06-04
申请号：US13056362
申请日：2008-07-29
申请人： Naoko Iwata , Hiroaki Takahashi , Peter Bogdanoff , Sebastian Fiechter , Iris Herrmann-Geppert , Ulrike Kramm
发明人： Naoko Iwata , Hiroaki Takahashi , Peter Bogdanoff , Sebastian Fiechter , Iris Herrmann-Geppert , Ulrike Kramm
IPC分类号： H01M4/88 , B01J23/00 , B01J23/38 , B01J23/40 , B01J23/42 , B01J23/44 , B01J23/46 , B01J23/74
CPC分类号： H01M4/9008 , H01M4/8605 , H01M4/8882 , H01M4/9083 , H01M4/923 , H01M4/926 , H01M2008/1095
摘要： According to the present invention, the catalyst performance of a chelate catalyst comprising a complex of a macrocyclic compound such as a porphyrin derivative is improved. Also, the following method is provided: a method for preparing a fuel cell electrode catalyst comprising a nitrogen-containing metal complex in which a metallic element is coordinated with a macrocyclic organic compound, such method comprising the steps of: adding tin oxalate to the nitrogen-containing metal complex; and baking a mixture of the nitrogen-containing metal complex and tin oxalate in an inert gas atmosphere, wherein elution of metal tin is carried out via acid treatment.
摘要翻译： 根据本发明，提高了包含卟啉衍生物等大环化合物的络合物的螯合催化剂的催化剂性能。 另外，提供了以下方法：一种制备燃料电池电极催化剂的方法，该催化剂包含金属元素与大环有机化合物配位的含氮金属络合物，该方法包括以下步骤：向氮中加入草酸锡 含金属络合物; 并在惰性气体气氛中焙烧含氮金属络合物和草酸锡的混合物，其中通过酸处理进行金属锡的洗脱。
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公开(公告)号：US20120196738A1
公开(公告)日：2012-08-02
申请号：US13501115
申请日：2009-10-16
CPC分类号： H01M4/8882 , H01M4/921 , H01M4/926 , H01M2008/1095
摘要： The present invention provides a method for producing an electrode catalyst for a fuel cell, comprising the steps of: mixing conductive particles loaded with catalyst metal fine particles with an organic compound; and heat treating the mixture formed in the mixing step under an inert gas atmosphere, so as to carbonize the organic compound. According to the present invention, the size increase of catalyst metal fine particles, which lowers catalytic activity, can be suppressed.
摘要翻译： 本发明提供一种燃料电池用电极催化剂的制造方法，其特征在于，包括：将载有催化剂金属微粒的导电粒子与有机化合物混合的工序; 并在惰性气体气氛下对在混合步骤中形成的混合物进行热处理，以使有机化合物碳化。 根据本发明，可以抑制降低催化活性的催化剂金属微粒的尺寸增加。
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6.发明申请Production of a Platinum-Free Chelate Catalyst Material as an Intermediate Product, and Further Processing Thereof to Obtain an Electrocatalytic Coating as a Final Product 审中-公开生产无铂螯合催化剂材料作为中间产品，并进一步加工获得电催化涂层作为最终产品公开(公告)号：US20080286490A1
公开(公告)日：2008-11-20
申请号：US11816688
申请日：2006-02-20
CPC分类号： B01J37/349 , B01J21/18 , B01J31/1805 , B01J35/002 , B01J37/086 , B01J2531/845 , H01M4/9008 , H01M8/1011 , H01M2004/028 , Y02E60/523 , Y02P70/56
摘要： A method for preparing a platinum-free chelate catalyst material as an intermediate product for selective electrocatalytic reduction of oxygen includes performing a low-temperature plasma treatment on a powdery form of the transition-metal chelate in a plasma reactor chamber having an inert plasma gas disposed therein. A plasma power, a plasma gas pressure, a plasma initialization and a treatment time of the low-temperature plasma treatment are selected so that molecules of the transition metal chelate are fragmented in the plasma and cross-link in a subsequent chemical reaction so as to form a carbon matrix and retain a basic chelate structure in a surrounding of the transition metal.
摘要翻译： 制备用于选择性电催化还原氧化的中间产物的无铂螯合催化剂材料的方法包括在具有惰性等离子体气体的等离子体反应器室中对过渡金属螯合物的粉末形式进行低温等离子体处理 其中。 选择等离子体功率，等离子体气体压力，等离子体初始化和低温等离子体处理的处理时间，使得过渡金属螯合物的分子在等离子体中碎裂并在随后的化学反应中交联，从而 形成碳基质并在过渡金属的周围保留碱性螯合物结构。
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