Method of manufacturing silicon sulfide
    1.
    发明授权
    Method of manufacturing silicon sulfide 失效
    硫化硅的制造方法

    公开(公告)号:US5843391A

    公开(公告)日:1998-12-01

    申请号:US839677

    申请日:1997-04-15

    IPC分类号: C01B17/20 C01B33/00 C01B17/00

    CPC分类号: C01B33/00 Y10S423/12

    摘要: Silicon sulfide is manufactured from the fine powder of silicon having a particle size in the range of 60 to 100.mu., covered thoroughly with sulfur at lower temperature less than 700.degree. C. in vacuum. In order to produce the silicon sulfide, silicon should be ground in a non-oxidizing atmosphere to prevent the formation of a silicon oxide layer that remains in the product and degrades the purity of the product. The silicon powder is dispersed sufficiently in the molten sulfur. At this time, the quantity of added sulfur needs more than 1.1 times in comparison with the stoichiometric quantity of silicon sulfide. All surfaces of silicon powder should be covered with sulfur to avoid sintering between silicon particles in the whole process of the reaction.

    摘要翻译: 硫化硅由粒度在60-100微米范围内的硅微粉制成,在真空中低于700℃的较低温度下用硫彻底覆盖。 为了生产硫化硅,应在非氧化性气氛中研磨硅,以防止残留在产品中的氧化硅层的形成并降低产品的纯度。 硅粉充分分散在熔融硫中。 此时,与硫化硅的化学计量量相比,添加硫的量需要1.1倍以上。 硅粉的所有表面均应用硫覆盖,以避免整个反应过程中硅颗粒之间的烧结。

    Separator for Fuel Cell and Process for Producing the Same
    2.
    发明申请
    Separator for Fuel Cell and Process for Producing the Same 审中-公开
    燃料电池分离器及其生产方法

    公开(公告)号:US20100159357A1

    公开(公告)日:2010-06-24

    申请号:US12225368

    申请日:2007-04-03

    IPC分类号: H01M2/14

    摘要: In order to attain excellent electrical conductivity and molding processability, a fuel cell separator to be produced by performing press molding on a preform in which expanded graphite is used as the main raw material is improved so that the preform is produced by a papermaking method, whereby the characteristics of the mechanical strength, the flexibility, and the gas impermeability are improved, and a light and compact configuration that is preferred in the automobile use or the like can be realized. In a fuel cell separator which is to be produced by performing press molding on a preform 14 that is formed into a plate-like shape, with a molding die, therefore, the preform 14 is configured into a sandwich structure where a second sheet 14B in which a phenol resin is applied to graphite is interposed between a pair of first sheets 14A made by impregnating a sheet-like member with a phenol resin, the sheet-like member being obtained by a papermaking process using a raw material in which a fibrous filler is added to expanded graphite.

    摘要翻译: 为了获得优异的导电性和成型加工性,通过对以膨胀石墨为主要原料的预成型体进行加压成型而制造的燃料电池用隔膜得到改善,通过造纸方式制造预成型体,由此 机械强度,柔性和气体不透性的特征得到改善,并且可以实现在汽车用途等中优选的轻且紧凑的构造。 因此,在通过对成形为板状的预成型体14进行加压成形而制造的燃料电池用隔板中,因此,在成形模具中,将预成型体14构成为夹层结构, 将酚醛树脂施加到石墨上的一对第一片材14A插入在通过浸渍片状构件与酚醛树脂制成的一对第一片材14A之间,该片状构件通过造纸工艺获得,使用原料,其中纤维状填料 添加到膨胀石墨中。

    Lithium ion-conductive solid electrolyte and method for producing the
same
    3.
    发明授权
    Lithium ion-conductive solid electrolyte and method for producing the same 失效
    锂离子导电固体电解质及其制造方法

    公开(公告)号:US5958281A

    公开(公告)日:1999-09-28

    申请号:US833208

    申请日:1997-04-14

    摘要: A method for producing an electrochemically advantageous lithium ion-conductive solid electrolyte with high ionic conductivity, low electronic conduction and electrochemical stability is disclosed. The method comprises the steps of synthesizing lithium sulfide by reacting lithium hydroxide with a gaseous sulfur source at a temperature of not less than 130.degree. C. and not more than 445.degree. C., thermally melting plural compounds containing at least silicon sulfide and the synthesized lithium sulfide, and cooling the molten mixture. The silicon sulfide is synthesized by the steps of adding a silicon powder to molten sulfur while stirring to disperse the silicon powder in the molten sulfur and heating the silicon powder-dispersed sulfur in a reaction chamber under reduced pressure.

    摘要翻译: 公开了一种制备具有高离子导电性,低电子传导性和电化学稳定性的电化学有利的锂离子传导性固体电解质的方法。 该方法包括以下步骤:在不低于130℃且不高于445℃的温度下,使氢氧化锂与气态硫源反应合成硫化锂,将至少含有硫化硅的多种化合物热合并合成 硫化锂,并冷却熔融混合物。 硫化硅通过在搅拌下将硅粉加入熔融硫中以将硅粉分散在熔融硫中并在减压下加热反应室中的硅粉分散硫的步骤合成。

    Portable communication terminal and wireless communication system therefore
    4.
    发明申请
    Portable communication terminal and wireless communication system therefore 审中-公开
    便携式通信终端和无线通信系统

    公开(公告)号:US20080004071A1

    公开(公告)日:2008-01-03

    申请号:US11894827

    申请日:2007-08-22

    IPC分类号: H04M1/00

    CPC分类号: H04B1/406 H04B7/2631

    摘要: A portable communication terminal provides multiple transceivers allowing reception and transmission of signals in accordance with multiple wireless communication systems (e.g., cdma2000 1×-EV DO and cdma2000 1× systems). When the predicted future data communication speed becomes lower than the prescribed threshold, the portable communication terminal automatically switches from one system to another. In addition, the portable communication terminal monitors amounts of data that are received by the preset time period (Td) each. That is, if the reception data rate is continuously reduced lower than the prescribed threshold for the prescribed time period (T), the portable communication terminal automatically switches from one system to another. Thus, it is possible to normally provide the user with a good data communication service, regardless of data communication environments.

    摘要翻译: 便携式通信终端提供允许根据多个无线通信系统(例如,cdma2000 1x-EV DO和cdma2000 1x系统)的信号的接收和传输的多个收发器。 当预测的未来数据通信速度变得低于规定的阈值时,便携式通信终端自动地从一个系统切换到另一个系统。 此外,便携式通信终端监视每个接收的预设时间段(Td)的数据量。 也就是说,如果接收数据速率在规定的时间段(T)内持续降低到低于规定的阈值,则便携式通信终端自动地从一个系统切换到另一个系统。 因此,无论数据通信环境如何,通常可以向用户提供良好的数据通信服务。

    Separator for fuel cell and process for producing the same
    5.
    发明申请
    Separator for fuel cell and process for producing the same 审中-公开
    燃料电池分离器及其制造方法

    公开(公告)号:US20090130534A1

    公开(公告)日:2009-05-21

    申请号:US12227363

    申请日:2007-04-13

    IPC分类号: H01M8/02 H01M8/10 B29C43/02

    摘要: In order to attain excellent electrical conductivity and molding processability, a fuel cell separator to be produced by performing press molding on a preform in which expanded graphite is used as the main raw material is improved so that the preform is produced by a papermaking method, whereby the characteristics of the mechanical strength, the flexibility, and the gas impermeability are improved, and the moldability is made excellent so that a light and compact configuration that is preferred in the automobile use or the like can be realized. In a fuel cell separator which is to be produced by performing press molding on a preform 14 that is formed into a plate-like shape, with a molding die, therefore, the preform 14 is configured into a sandwich structure where a first sheet 14A made by impregnating a sheet-like member with a phenol resin, the sheet-like member being obtained by a papermaking process using a raw material in which a fibrous filler is added to expanded graphite, is interposed between a pair of second sheets 14B in which a phenol resin is applied to graphite.

    摘要翻译: 为了获得优异的导电性和成型加工性,通过对以膨胀石墨为主要原料的预成型体进行加压成型而制造的燃料电池用隔膜得到改善,通过造纸方式制造预成型体,由此 提高了机械强度,柔软性和气体不透性的特性,并且成型性优异,从而可以实现在汽车用途等中优选的轻型和紧凑型结构。 因此,在通过对成形为板状的预成型体14进行加压成形而制造的燃料电池用隔板中,因此,在成型模具中,将预成型体14构成为第一片14A 通过用酚醛树脂浸渍片状构件,通过使用其中向膨胀石墨中加入纤维状填料的原料的造纸方法获得的片状构件插入在一对第二片14B之间,其中 将酚醛树脂应用于石墨。