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公开(公告)号：US5955048A
公开(公告)日：1999-09-21
申请号：US534996
申请日：1995-09-27
IPC分类号： B01J20/06 , B01J20/08 , B01J23/00 , B01J35/00 , B01J37/00 , B01J37/08 , C01F7/00 , C01B25/26 , C01B21/48 , C01B31/30 , C01F7/02
CPC分类号： B01J20/06 , B01J20/08 , B01J23/007 , B01J37/08 , C01F7/005 , B01J35/002 , B01J37/0009
摘要： There is provided a flash activated hydrotalcite which, when extruded to sizes of about 1/16 inch or more, has a crush load strength of at least about 7 pounds. The process for making this extrudate includes: (a) providing a hydrotalcite compound; (b) heating said compound for less than two seconds to one or more temperatures above about 482.degree. C. (900.degree. F.); (c) cooling said heated compound; (d) collecting said cooled compound; (e) forming said compound into an extrudate; and (f) reactivating said extrudate by heating to one or more temperatures above about 400.degree. C. (752.degree. F.) for about 20 minutes or more. Further strength improvements are achieved by exposing these extrudates to steam for at least about 8 hours prior to step (f).
摘要翻译： 提供了一种闪光活化的水滑石，其当挤出至约+ E，1/16 + EE英寸或更大的尺寸时，具有至少约7磅的压碎载荷强度。 制造该挤出物的方法包括：（a）提供水滑石化合物; （b）将所述化合物加热至少于两秒钟至高于约482℃（900°F）的一个或多个温度; （c）冷却所述加热的化合物; （d）收集所述冷却的化合物; （e）将所述化合物形成挤出物; 和（f）通过加热至高于约400℃（752°F）的一个或多个温度约20分钟或更长时间来再活化所述挤出物。 通过在步骤（f）之前将这些挤出物暴露于蒸汽至少约8小时来实现进一步的强度改进。
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公开(公告)号：US4375980A
公开(公告)日：1983-03-08
申请号：US21879
申请日：1979-03-19
申请人： Thomas M. Jones , John M. Stinson
发明人： Thomas M. Jones , John M. Stinson
IPC分类号： C05B7/00
CPC分类号： C05B7/00
摘要： An improved process for the production of concentrated, high-grade, nitrogen-phosphate (N--P.sub.2 O.sub.5) base suspension fertilizer from wet-process or other phosphoric acids and ammonia. The process involves addition of small proportions of fluosilicic acid during preparation of the suspension to cause modification of monoammonium phosphate crystals to shapes and sizes that do not settle during vibration such as occurs during shipment.
摘要翻译： 一种从湿法或其他磷酸和氨生产浓缩高品位氮磷（N-P2O5）基悬浮肥料的改进方法。 该方法包括在制备悬浮液期间加入少量氟硅酸，以使磷酸二氢铵晶体改变成在运输过程中发生的振动期间不稳定的形状和尺寸。
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公开(公告)号：UST986001I4
公开(公告)日：1979-09-04
申请号：US947684
申请日：1978-10-02
申请人： Thomas M. Jones , John M. Stinson
发明人： Thomas M. Jones , John M. Stinson
IPC分类号： C05B7/00
CPC分类号： C05B7/00
摘要： an improved process for production of concentrated high-analysis nitrogen-phosphate base suspension fertilizer by ammoniation of wet-process or other orthophosphoric acids in two stages. The process improvement involves the addition of a small amount (0.1-0.5 percent) of a crystal modifier, fluosilicic acid, for prevention of settling of crystals in the suspension during vibration such as that which occurs during shipment. With use of the crystal modifier, the monoammonium phosphate crystals formed are small and needlelike, and suspension fertilizers with excellent shipping, storage, and handling properties are produced with an N:P.sub.2 O.sub.5 weight ratio in the range of highest solubility, about 0.27 to 0.33.
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公开(公告)号：US5407702A
公开(公告)日：1995-04-18
申请号：US057743
申请日：1993-05-05
申请人： David A. Smith , Susan A. Stanton , Gary J. DiFranco , Roy B. Steidley , John M. Stinson , Thomas L. Levendusky , Vincent J. Downard , William F. Forster , John R. McAllister
发明人： David A. Smith , Susan A. Stanton , Gary J. DiFranco , Roy B. Steidley , John M. Stinson , Thomas L. Levendusky , Vincent J. Downard , William F. Forster , John R. McAllister
IPC分类号： B05D1/00 , B05D1/26 , B05D1/28 , B05D3/02 , B05D7/14 , B29C35/16 , B29C71/00 , B29D7/01 , B32B37/15
CPC分类号： B32B37/153 , B05D1/265 , B05D1/28 , B05D3/02 , B05D7/14 , B05D2252/04 , B05D2252/10 , B29C2035/1616 , B29C71/0063 , B29K2067/00 , B29K2705/02
摘要： A method for extrusion coating both sides of a metal strip. A metal strip, such as aluminum alloy strip, is moved through a pre-conditioner, two extrusion dies, a post heater and a cooling system. Both sides of the strip are coated with thin coatings of polyester material. The coated metal strip is useful for containers, such as cans and can ends, as well as for automobiles, appliances, aerospace, construction and electrical devices.
摘要翻译： 一种用于挤出涂覆金属带的两侧的方法。 诸如铝合金带的金属条移动通过预调节器，两个挤出模具，后加热器和冷却系统。 带材的两面均涂有聚酯材料的薄涂层。 涂覆的金属条可用于容器，例如罐和罐端，以及汽车，电器，航空航天，建筑和电气设备。
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公开(公告)号：US4292067A
公开(公告)日：1981-09-29
申请号：US120949
申请日：1980-02-12
申请人： John M. Stinson , James R. Burnell
发明人： John M. Stinson , James R. Burnell
CPC分类号： C05B13/06
摘要： Crystalline urea phosphate mixed with sufficient quantities of previously produced urea-ammonium polyphosphate liquid to provide fluidity is pyrolyzed batchwise in one stage to give molten urea ammonium polyphosphate containing up to 50 percent of the phosphate as polyphosphate. Water or aqua ammonia can be substituted for the polyphosphate liquid if certain prescribed steps in proper sequence are followed. Heat from ammoniation of the urea phosphate provides all of the heat for pyroloysis. The molten urea-ammonium polyphosphate is then processed into high-analysis liquid fertilizer.
摘要翻译： 与足量的先前生产的尿素 - 聚磷酸铵液体混合以提供流动性的结晶尿素磷酸盐在一个阶段间歇地热解，得到含多达50％磷酸盐的多磷酸盐的熔融尿素铵多磷酸盐作为多磷酸盐。 如果遵循适当顺序的某些规定步骤，则可以用水或氨水代替多磷酸盐液体。 尿素磷的氨化的热量提供了用于热解的所有热量。 然后将熔融的尿素 - 多磷酸铵加工成高分析液体肥料。
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公开(公告)号：US2131498A
公开(公告)日：1938-09-27
申请号：US5605935
申请日：1935-12-24
申请人： JOHN M STINSON
发明人： CHANDLER WILLIAM W
IPC分类号： B26B21/44
CPC分类号： B26B21/446
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7.发明授权Two powder synthesis of hydrotalcite and hydrotalcite-like compounds with monovalent organic anions 失效两种粉末合成水滑石和类水滑石化合物与一价有机阴离子
公开(公告)号：US5728366A
公开(公告)日：1998-03-17
申请号：US645666
申请日：1996-05-14
IPC分类号： B01J23/00 , C01B19/00 , C01B33/38 , C01F7/00 , C01G31/00 , C01G39/00 , C01G41/00 , C07C51/41 , C07F11/00 , C07F13/00
CPC分类号： C07C51/412 , B01J23/007 , C01B19/002 , C01B33/38 , C01F7/00 , C01F7/002 , C01F7/005 , C01G31/006 , C01G39/006 , C01G41/006 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2002/78 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： There is provided a method for making monovalent organic anion-intercalated hydrotalcite-like materials by first reacting a magnesium-containing powder and a transition alumina powder in a carboxylic acid-free, aqueous suspension to form a meixnerite intermediate. This intermediate is then contacted with a monovalent organic anion to form a hydrotalcite-like material. The latter is then separated from the suspension. Representative materials include a stearate-, acetate- or benzoate-intercalated hydrotalcite-like material.
摘要翻译： 提供了通过首先使含镁粉末和过渡氧化铝粉末在不含羧酸的水悬浮液中反应以形成中间体的方法来制备单价有机阴离子 - 插层的类水滑石材料。 然后将该中间体与一价有机阴离子接触以形成类水滑石材料。 然后将后者与悬浮液分离。 代表性的材料包括硬脂酸酯，乙酸酯或苯甲酸酯插层的类水滑石材料。
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公开(公告)号：US5728364A
公开(公告)日：1998-03-17
申请号：US629717
申请日：1996-04-09
IPC分类号： B01J23/00 , C01B13/36 , C01B19/00 , C01B33/38 , C01F7/00 , C01G31/00 , C01G39/00 , C01G41/00 , C07C51/41 , C07F11/00 , C07F13/00
CPC分类号： C07C51/412 , B01J23/007 , C01B13/363 , C01B19/002 , C01B33/38 , C01F7/00 , C01F7/002 , C01F7/005 , C01G31/006 , C01G39/006 , C01G41/006 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2002/78 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： There is provided an improved method for making synthetic hydrotalcite by first reacting a divalent metal compound with a trivalent metal oxide powder in a carboxylic acid-free, aqueous solution or suspension to form an intermediate. This intermediate is then contacted with an anion source such as carbon dioxide; a carbonate-containing compound; an acid or an ammonium salt to form a layered double hydroxide having the formula: A.sub.1-x B.sub.x (OH).sub.2 C.sub.z.mH.sub.2 O, where A represents a divalent metal cation, B represents a trivalent metal cation, C represents a mono- to polyvalent anion, and x, z and m satisfy the following conditions: 0.09 m>0.5. Said layered double hydroxide is typically separated from the suspension by filtering, centrifugation, vacuum dehydration or other known means.
摘要翻译： 提供一种通过首先在无羧酸的水溶液或悬浮液中使二价金属化合物与三价金属氧化物粉末反应形成中间体来制备合成水滑石的改进方法。 然后将该中间体与阴离子源例如二氧化碳接触; 含碳酸盐的化合物; 酸或铵盐形成具有下式的Al-xBx（OH）2Cz.mH2O的层状双氢氧化物，其中A表示二价金属阳离子，B表示三价金属阳离子，C表示一价至多价阴离子， x，z和m满足以下条件：0.09
m> 0.5。 所述层状双氢氧化物通常通过过滤，离心，真空脱水或其它已知方法与悬浮液分离。 -
9.发明授权Two powder synthesis of hydrotalcite-like compounds with divalent or polyvalent organic anions 失效两种具有二价或多价有机阴离子的类水滑石化合物的粉末合成
公开(公告)号：US5578286A
公开(公告)日：1996-11-26
申请号：US482390
申请日：1995-06-07
IPC分类号： B01J23/00 , C01B13/36 , C01B19/00 , C01B33/38 , C01F7/00 , C01G1/00 , C01G3/00 , C01G9/00 , C01G31/00 , C01G39/00 , C01G41/00 , C01G45/00 , C01G49/00 , C01G53/00 , C07C51/41 , C07F11/00 , C07F13/00
CPC分类号： B01J23/007 , B82Y30/00 , C01B13/363 , C01B19/002 , C01B33/38 , C01F7/00 , C01F7/002 , C01F7/005 , C01G1/00 , C01G3/006 , C01G31/006 , C01G39/006 , C01G41/006 , C01G45/006 , C01G49/009 , C01G53/006 , C01G9/006 , C07C51/412 , C01P2002/02 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2002/78 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： There is provided a method for making a divalent or polyvalent organic anion-intercalated hydrotalcite-like materials by first reacting a magnesium-containing powder and a transition alumina powder in an aqueous suspension to form a meixnerite intermediate. This intermediate is then contacted with a dicarboxylate or polycarboxylate anion to form a hydrotalcite-like material. The latter is then separated from the suspension. Representative materials include an oxalate-, succinate- or terephthalate-intercalated hydrotalcite-like material.
摘要翻译： 提供了制备二价或多价有机阴离子插层的类水滑石材料的方法，首先使含水粉末和过渡氧化铝粉末在水性悬浮液中反应形成中间体。 然后将该中间体与二羧酸盐或多羧酸盐阴离子接触以形成类水滑石材料。 然后将后者与悬浮液分离。 代表性材料包括草酸盐，琥珀酸盐或对苯二甲酸盐插层的类水滑石材料。
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公开(公告)号：UST973004I4
公开(公告)日：1978-08-01
申请号：US838503
申请日：1977-10-03
IPC分类号： C05B13/06
摘要： a process for the production of high-purity urea-ammonium polyphosphate fertilizers from crystalline urea orthophosphate derived from the reaction of wet-process acid and urea. Initially, urea phosphate was pyrolyzed in one stage to give molten urea-ammonium polyphosphates that contained up to 95 percent of the phosphate as polyphosphate, dependent upon the reaction conditions used. Heat to effect condensation of orthophosphate with urea to form polyphosphate was provided by steam. Reaction conditions ranging from a retention time of 1 minute at 350.degree. F to 30 minutes at 260.degree. F were satisfactory. The pyrolyzate contained mixtures of urea, ammonium orthophosphate, and ammonium polyphosphates and was dissolved in aqua ammonia to yield clear liquid fertilizers containing 12 to 15 percent nitrogen and 18 to 29 percent P.sub.2 O.sub.5. Addition of either urea to the process to maintain a urea:biuret ratio of at least 16, or about 2 pounds NH.sub.3 per unit P.sub.2 O.sub.5 to the pyrolysis reactor prevented biuret precipitation in the liquid fertilizers. Granulation of urea-ammonium polyphosphate melt by conventional means gave solids containing 19 to 21 percent N and 45 to 47 percent P.sub.2 O.sub.5. Supplementary, secondary, or micronutrient-containing materials may be incorporated in the liquid or solid products.
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