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1.发明授权Two powder synthesis of hydrotalcite and hydrotalcite-like compounds with divalent inorganic anions 失效两种粉末合成水滑石和类水滑石化合物与二价无机阴离子
公开(公告)号：US5728365A
公开(公告)日：1998-03-17
申请号：US645665
申请日：1996-05-14
IPC分类号： B01J23/00 , C01B13/36 , C01B19/00 , C01B33/38 , C01F7/00 , C01G31/00 , C01G39/00 , C01G41/00 , C07F11/00 , C07F13/00
CPC分类号： C01B19/002 , B01J23/007 , C01B13/363 , C01B33/38 , C01F7/00 , C01F7/002 , C01F7/005 , C01G31/006 , C01G39/006 , C01G41/006 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2002/78 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： There is provided a method for making a divalent inorganic anion-intercalated hydrotalcite-like material by first reacting a magnesium-containing powder and a transition alumina powder in a carboxylic acid-free aqueous suspension to form a meixnerite intermediate. This intermediate is then contacted with a divalent inorganic anion, in its acid, acid salt or ammonium salt form, to make a hydrotalcite-like material. The latter is then separated from the suspension. Representative materials include a sulfate- and metavanadate-intercalated hydrotalcite-like material.
摘要翻译： 提供了通过首先使含镁粉末和过渡型氧化铝粉末在不含羧酸的水性悬浮液中反应形成二氯甲烷中间体的方法来制备二价无机阴离子插层的类水滑石材料。 然后将该中间体与其酸，酸盐或铵盐形式的二价无机阴离子接触，以制备类似水滑石的材料。 然后将后者与悬浮液分离。 代表性材料包括硫酸盐和偏钒酸盐插层的类水滑石材料。
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2.发明授权Two powder synthesis of hydrotalcite and hydrotalcite-like compounds with monovalen inorganic anions 失效两种粉末合成水滑石和类水滑石化合物与单价无机阴离子
公开(公告)号：US5776424A
公开(公告)日：1998-07-07
申请号：US629713
申请日：1996-04-09
IPC分类号： B01J23/00 , C01B19/00 , C01B33/38 , C01F7/00 , C01G31/00 , C01G39/00 , C01G41/00 , C07C51/41 , C07F11/00 , C07F13/00
CPC分类号： C07C51/412 , B01J23/007 , C01B19/002 , C01B33/38 , C01F7/00 , C01F7/002 , C01F7/005 , C01G31/006 , C01G39/006 , C01G41/006 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2002/78 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： There is provided a method for making a monovalent inorganic anion-intercalated hydrotalcite-like material by first reacting a magnesium-containing powder and a transition alumina powder in a carboxylic acid-free, aqueous suspension to form a meixnerite intermediate. This intermediate is then contacted with a monovalent inorganic anion, in its acid or soluble salt form, to make a hydrotalcite-like material. The latter is then separated from the suspension. Representative materials include a bromide-, chloride-, nitrate- or vanadate-intercalated, hydrotalcite-like material.
摘要翻译： 提供了通过首先使含镁粉末和过渡氧化铝粉末在不含羧酸的水性悬浮液中反应以形成中间体的方法来制备单价无机阴离子插层的类水滑石材料。 然后将该中间体以其酸或可溶性盐形式与一价无机阴离子接触，以制备类水滑石材料。 然后将后者与悬浮液分离。 代表性材料包括溴化物，氯化物，硝酸盐或钒酸盐插层的类水滑石材料。
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3.发明授权
公开(公告)号：US5750453A
公开(公告)日：1998-05-12
申请号：US771461
申请日：1996-12-20
摘要： A method for making a synthetic mixed metal oxide or meixnerite which, when activated, has a high B.E.T. surface area, typically about 290 m.sup.2 /g or greater. The method comprises activating hydrotalcite, then cooling and hydrating such activated material with a metal salt solution in a carbon dioxide-free environment. Such hydration can produce a material that absorbs more than 100% of its weight in water. Following hydration, this material is activated a second time in a virtually carbon dioxide-free environment. Such reactivation decomposes the salt and leaves a supported metal oxide readily available to be used for catalyst reactions.
摘要翻译： 一种制造合成的混合金属氧化物或镁石的方法，其在活化时具有高B.E.T. 通常约290m 2 / g或更大。 该方法包括活化水滑石，然后在无二氧化碳的环境中用金属盐溶液冷却和水合这种活化的材料。 这种水合可以产生在水中吸收超过其重量的100％的材料。 水合后，该物质在几乎无二氧化碳的环境中再次被激活。 这种再活化使盐分解并留下易于用于催化剂反应的负载金属氧化物。
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4.发明授权Two powder synthesis of hydrotalcite and hydrotalcite-like compounds with polyvalent inorganic anions 失效两种粉末合成水滑石和类水滑石化合物与多价无机阴离子
公开(公告)号：US5730951A
公开(公告)日：1998-03-24
申请号：US647509
申请日：1996-05-14
IPC分类号： B01J23/00 , C01B13/36 , C01F7/00 , C01G31/00 , C01G39/00 , C01G41/00 , C07F11/00 , C07F13/00
CPC分类号： C01F7/00 , B01J23/007 , C01B13/363 , C01F7/002 , C01F7/005 , C01G31/006 , C01G39/006 , C01G41/006 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2002/78 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： There is provided a method for making a polyvalent inorganic anion-intercalated hydrotalcite-like material by first reacting a magnesium-containing powder and a transition alumina powder in a carboxylic acid-free, aqueous suspension to form a meixnerite intermediate. This intermediate is then contacted with a polyvalent inorganic anion, in its acid, acid salt or ammonium salt form, to make a hydrotalcite-like material. The latter is then separated from the suspension. Representative materials include a borate- metatungstate- and paramolybdate-intercalated hydrotalcite-like material.
摘要翻译： 提供了一种制备多价无机阴离子插层类水滑石材料的方法，首先使含镁粉末和过渡氧化铝粉末在不含羧酸的水悬浮液中反应形成中间体。 然后将该中间体与其酸，酸盐或铵盐形式的多价无机阴离子接触，以制备类似水滑石的材料。 然后将后者与悬浮液分离。 代表性材料包括硼酸盐 - 偏钨酸盐和仲钼酸盐 - 插层的类水滑石材料。
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公开(公告)号：US5728363A
公开(公告)日：1998-03-17
申请号：US625584
申请日：1996-03-28
IPC分类号： B01J23/00 , C01B13/36 , C01B19/00 , C01B33/38 , C01F7/00 , C01G1/00 , C01G3/00 , C01G9/00 , C01G31/00 , C01G39/00 , C01G41/00 , C01G45/00 , C01G49/00 , C01G53/00 , C07C51/41 , C07F11/00 , C07F13/00
CPC分类号： B82Y30/00 , B01J23/007 , C01B13/363 , C01B19/002 , C01B33/38 , C01F7/00 , C01F7/002 , C01F7/005 , C01G1/00 , C01G3/006 , C01G31/006 , C01G39/006 , C01G41/006 , C01G45/006 , C01G49/009 , C01G53/006 , C01G9/006 , C07C51/412 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2004/61 , C01P2006/12
摘要： There is provided an improved method for making synthetic hydrotalcite by first reacting powdered magnesium oxide with a high surface area, transition alumina in a solution or suspension to form a meixnerite-like intermediate. This intermediate is then contacted with an anion source such as an acid, and most preferably carbon dioxide, to form the layered double hydroxide which is separated from the suspension by filtering, centrifugation, vacuum dehydration or other known means. On a preferred basis, the transition alumina combined with activated magnesia consists essentially of an rehydratable alumina powder having a surface area of 100 m.sup.2 /g or greater. To make related double hydroxide compounds, still other reactants such as bromides, chlorides, boric acids, or salts thereof, may be substituted for the carbon dioxide gas fed into this suspension.
摘要翻译： 提供了一种通过首先使粉末状氧化镁与高表面积反应制备合成水滑石的改进方法，在溶液或悬浮液中使过渡氧化铝反应形成梅毒石状中间体。 然后将该中间体与阴离子源（例如酸，最优选二氧化碳）接触，形成通过过滤，离心，真空脱水或其它已知方法与悬浮液分离的层状双氢氧化物。 在优选的基础上，与活性氧化镁组合的过渡氧化铝基本上由表面积为100m 2 / g或更大的可再水化的氧化铝粉末组成。 为了制备相关的双氢氧化物化合物，还可以将其它反应物如溴化物，氯化物，硼酸或其盐替代进入该悬浮液的二氧化碳气体。
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公开(公告)号：US5543173A
公开(公告)日：1996-08-06
申请号：US308263
申请日：1994-09-19
CPC分类号： B01J2/30 , C04B35/62655 , C04B35/628 , C04B35/63448 , C04B2235/3217 , C04B2235/3222 , C04B2235/3232 , C04B2235/3236 , C04B2235/3241 , C04B2235/3244 , C04B2235/3248 , C04B2235/3445 , C04B2235/3463 , C04B2235/3481 , C04B2235/5436 , C04B2235/608 , Y10T428/2995
摘要： A method of reducing the agglomeration of inorganic powdered material, the method comprising: (a) providing an inorganic powdered material comprising ceramic particles; (b) coating the ceramic particles with a solution containing from 0.05-0.5 wt. % of a polysiloxanol oligomer of a trialkoxysiloxane monomer having the structure Si(OR').sub.3 wherein R' represents a C.sub.1 -C.sub.4 alkoxy group selected from the group consisting of methyl, ethyl, isopropyl and n-butyl and wherein the oligomer has chains having a number average distribution with a number average degree of polymerization X.sub.n in the range above 2 but below the gel point; and (c) drying the inorganic powdered material.
摘要翻译： 一种减少无机粉末材料附聚的方法，所述方法包括：（a）提供包含陶瓷颗粒的无机粉末材料; （b）用含有0.05-0.5wt。％的溶液涂覆陶瓷颗粒。 具有Si（OR'）3结构的三烷氧基硅氧烷单体的聚硅氧烷低聚物的％，其中R'表示选自甲基，乙基，异丙基和正丁基的C1-C4烷氧基，其中低聚物具有链具有 具有数均聚合度Xn在2以上但低于凝胶点的数均分布; 和（c）干燥无机粉末材料。
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7.发明授权Two powder synthesis of hydrotalcite and hydrotalcite-like compounds with monovalent organic anions 失效两种粉末合成水滑石和类水滑石化合物与一价有机阴离子
公开(公告)号：US5728366A
公开(公告)日：1998-03-17
申请号：US645666
申请日：1996-05-14
IPC分类号： B01J23/00 , C01B19/00 , C01B33/38 , C01F7/00 , C01G31/00 , C01G39/00 , C01G41/00 , C07C51/41 , C07F11/00 , C07F13/00
CPC分类号： C07C51/412 , B01J23/007 , C01B19/002 , C01B33/38 , C01F7/00 , C01F7/002 , C01F7/005 , C01G31/006 , C01G39/006 , C01G41/006 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2002/78 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： There is provided a method for making monovalent organic anion-intercalated hydrotalcite-like materials by first reacting a magnesium-containing powder and a transition alumina powder in a carboxylic acid-free, aqueous suspension to form a meixnerite intermediate. This intermediate is then contacted with a monovalent organic anion to form a hydrotalcite-like material. The latter is then separated from the suspension. Representative materials include a stearate-, acetate- or benzoate-intercalated hydrotalcite-like material.
摘要翻译： 提供了通过首先使含镁粉末和过渡氧化铝粉末在不含羧酸的水悬浮液中反应以形成中间体的方法来制备单价有机阴离子 - 插层的类水滑石材料。 然后将该中间体与一价有机阴离子接触以形成类水滑石材料。 然后将后者与悬浮液分离。 代表性的材料包括硬脂酸酯，乙酸酯或苯甲酸酯插层的类水滑石材料。
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公开(公告)号：US5728364A
公开(公告)日：1998-03-17
申请号：US629717
申请日：1996-04-09
IPC分类号： B01J23/00 , C01B13/36 , C01B19/00 , C01B33/38 , C01F7/00 , C01G31/00 , C01G39/00 , C01G41/00 , C07C51/41 , C07F11/00 , C07F13/00
CPC分类号： C07C51/412 , B01J23/007 , C01B13/363 , C01B19/002 , C01B33/38 , C01F7/00 , C01F7/002 , C01F7/005 , C01G31/006 , C01G39/006 , C01G41/006 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2002/78 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： There is provided an improved method for making synthetic hydrotalcite by first reacting a divalent metal compound with a trivalent metal oxide powder in a carboxylic acid-free, aqueous solution or suspension to form an intermediate. This intermediate is then contacted with an anion source such as carbon dioxide; a carbonate-containing compound; an acid or an ammonium salt to form a layered double hydroxide having the formula: A.sub.1-x B.sub.x (OH).sub.2 C.sub.z.mH.sub.2 O, where A represents a divalent metal cation, B represents a trivalent metal cation, C represents a mono- to polyvalent anion, and x, z and m satisfy the following conditions: 0.09 m>0.5. Said layered double hydroxide is typically separated from the suspension by filtering, centrifugation, vacuum dehydration or other known means.
摘要翻译： 提供一种通过首先在无羧酸的水溶液或悬浮液中使二价金属化合物与三价金属氧化物粉末反应形成中间体来制备合成水滑石的改进方法。 然后将该中间体与阴离子源例如二氧化碳接触; 含碳酸盐的化合物; 酸或铵盐形成具有下式的Al-xBx（OH）2Cz.mH2O的层状双氢氧化物，其中A表示二价金属阳离子，B表示三价金属阳离子，C表示一价至多价阴离子， x，z和m满足以下条件：0.09
m> 0.5。 所述层状双氢氧化物通常通过过滤，离心，真空脱水或其它已知方法与悬浮液分离。 -
9.发明授权Two powder synthesis of hydrotalcite-like compounds with divalent or polyvalent organic anions 失效两种具有二价或多价有机阴离子的类水滑石化合物的粉末合成
公开(公告)号：US5578286A
公开(公告)日：1996-11-26
申请号：US482390
申请日：1995-06-07
IPC分类号： B01J23/00 , C01B13/36 , C01B19/00 , C01B33/38 , C01F7/00 , C01G1/00 , C01G3/00 , C01G9/00 , C01G31/00 , C01G39/00 , C01G41/00 , C01G45/00 , C01G49/00 , C01G53/00 , C07C51/41 , C07F11/00 , C07F13/00
CPC分类号： B01J23/007 , B82Y30/00 , C01B13/363 , C01B19/002 , C01B33/38 , C01F7/00 , C01F7/002 , C01F7/005 , C01G1/00 , C01G3/006 , C01G31/006 , C01G39/006 , C01G41/006 , C01G45/006 , C01G49/009 , C01G53/006 , C01G9/006 , C07C51/412 , C01P2002/02 , C01P2002/22 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2002/78 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/80 , C01P2006/82
摘要： There is provided a method for making a divalent or polyvalent organic anion-intercalated hydrotalcite-like materials by first reacting a magnesium-containing powder and a transition alumina powder in an aqueous suspension to form a meixnerite intermediate. This intermediate is then contacted with a dicarboxylate or polycarboxylate anion to form a hydrotalcite-like material. The latter is then separated from the suspension. Representative materials include an oxalate-, succinate- or terephthalate-intercalated hydrotalcite-like material.
摘要翻译： 提供了制备二价或多价有机阴离子插层的类水滑石材料的方法，首先使含水粉末和过渡氧化铝粉末在水性悬浮液中反应形成中间体。 然后将该中间体与二羧酸盐或多羧酸盐阴离子接触以形成类水滑石材料。 然后将后者与悬浮液分离。 代表性材料包括草酸盐，琥珀酸盐或对苯二甲酸盐插层的类水滑石材料。
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公开(公告)号：US4385145A
公开(公告)日：1983-05-24
申请号：US322506
申请日：1981-11-18
申请人： William E. Horn, Jr.
发明人： William E. Horn, Jr.
CPC分类号： C08K5/527
摘要： Poly(alkylene terephthalate) compositions containing a stabilizing proportion of a pentaerythritol diphosphite ester. The compositions are relatively stable under usual processing conditions which include high temperatures. Color formation, molecular degradation and acetaldehyde contamination are inhibited significantly.
摘要翻译： 含有稳定化比例的季戊四醇二亚磷酸酯的聚（对苯二甲酸亚烷基酯）组合物。 组合物在包括高温的通常加工条件下相对稳定。 颜色形成，分子降解和乙醛污染受到显着抑制。
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