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    Separation of plant oil triglyceride mixtures by solid bed adsorption
    4.
    发明授权
    Separation of plant oil triglyceride mixtures by solid bed adsorption 有权
    通过固体床吸附分离植物油甘油三酯混合物

    公开(公告)号：US07097770B2

    公开(公告)日：2006-08-29

    申请号：US10471875

    申请日：2002-03-21

    申请人： Zenon Lysenko ,  Sanjeev Katti ,  Richard Stringfield ,  Thomas Gregory ,  George J. Quarderer, Jr.

    发明人： Zenon Lysenko ,  Sanjeev Katti ,  Richard Stringfield ,  Thomas Gregory ,  George J. Quarderer, Jr.

    IPC分类号： B01D15/08 ,  C11B7/00

    CPC分类号： C11B7/0008 ,  C11B7/0058

    摘要： A solid bed adsorptive process for separating a seed oil into two substantially pure triglyceride fractions. The process involves contacting a seed oil, such as castor oil, preferably as a concentrate, with an adsorbent in a bed, the adsorbent having a particle size greater than about 40 microns, and thereafter contacting the adsorbent with a desorbent material, preferably under minimal flow conditions, to obtain a raffinate output stream containing predominantly a second triglyceride and an extract output stream containing predominantly a first triglyceride. Purified fatty acid triglyceride esters obtainable from castor, vernonia, and lesquerella plant oils provide renewable, non-petroleum-based sources of chemical feedstocks.

    摘要翻译： 用于将种子油分离成两个基本上纯的甘油三酯馏分的固体床吸附方法。 该方法包括使诸如蓖麻油（优选浓缩物）的种子油与床中的吸附剂接触，吸附剂具有大于约40微米的粒度，然后使吸附剂与解吸材料接触，优选地在最小程度上 流动条件，以获得主要含有第二甘油三酯和主要含有第一甘油三酸酯的提取物输出流的萃余液输出流。 从蓖麻，弗兰诺瓦和莱斯特雷拉植物油获得的纯化脂肪酸甘油三酯可提供可再生的非石油基化学原料来源。

    Process of preparing an olefin oxide from olefin and organic hydroperoxide
    5.
    发明授权
    Process of preparing an olefin oxide from olefin and organic hydroperoxide 有权
    从烯烃和有机氢过氧化物制备烯烃氧化物的方法

    公开(公告)号：US07273941B2

    公开(公告)日：2007-09-25

    申请号：US10495001

    申请日：2002-12-04

    申请人： Gary R. Strickler ,  George J. Quarderer, Jr. ,  Joerg P. Lindner

    发明人： Gary R. Strickler ,  George J. Quarderer, Jr. ,  Joerg P. Lindner

    IPC分类号： C07D301/14 ,  C07D301/03 ,  C07D301/19

    CPC分类号： C07D301/19 ,  B01J19/006 ,  B01J19/2415 ,  B01J19/242 ,  B01J2219/00083 ,  B01J2219/00768 ,  B01J2219/182 ,  C07C29/132 ,  C07C31/10 ,  C07C33/22 ,  C07C31/205

    摘要： A process of preparing an olefin oxide, preferably propylene oxide, and an alcohol, such as α-ethylphenyl alcohol, the process involving contacting an olefin, such as propylene, and an organic hydroperoxide, such as ethylbenzene hydroperoxide, in the presence of an epoxidation catalyst, preferably, a homogeneous molybdenum catalyst, in a single reactor system or in a multi-reactor system containing a plurality of sequentially interconnected reactors. Each reactor in the single or multi-reactor system is preferably divided into a plurality of reaction zones designed to facilitate plug flow behavior. The olefin is fed to a first reaction zone in the single reactor system or to a first reactor in the multi-reactor system. The organic hydroperoxide feed is split into a plurality of split organic hydroperoxide feedstreams, and the split feedstreams are distributed throughout the reaction zones, or the reactors, or both.

    摘要翻译： 一种制备烯烃氧化物，优选环氧丙烷和醇如α-乙基苯醇的方法，该方法包括使烯烃如丙烯与有机氢过氧化物如乙苯氢过氧化物在环氧化物存在下接触 催化剂，优选均匀的钼催化剂，在单个反应器系统中或在包含多个顺序相互连接的反应器的多反应器系统中。 单反应器或多反应器系统中的每个反应器优选分成多个设计成促进活塞流动性能的反应区域。 将烯烃加入单反应器系统中的第一反应区或多反应器系统中的第一反应器。 有机氢过氧化物进料分成多个裂解的有机氢过氧化物进料流，并且分离的进料流分布在整个反应区或反应器中，或两者均分布。

    Method for producing epoxides
    6.
    发明授权
    Method for producing epoxides 失效
    环氧化物生产方法

    公开(公告)号：US5486627A

    公开(公告)日：1996-01-23

    申请号：US348639

    申请日：1994-12-02

    申请人： George J. Quarderer, Jr. ,  Curtis N. Swisher ,  David L. Trent

    发明人： George J. Quarderer, Jr. ,  Curtis N. Swisher ,  David L. Trent

    IPC分类号： C07D301/26 ,  C07D303/04 ,  C07D303/08 ,  C07D303/14

    CPC分类号： C07D301/26

    摘要： Described herein is a method for producing epoxides which is continuous, inhibits formation of chlorinated byproducts, and eliminates or substantially reduces waste water discharge. The method includes:(a) forming a low chlorides aqueous hypochlorous acid solution;(b) contacting the low chlorides aqueous hypochlorous acid solution with at least one unsaturated organic compound to form an aqueous organic product comprising at least olefin chlorohydrin;(c) contacting at least the olefin chlorohydrin with an aqueous alkali metal hydroxide to form an aqueous salt solution product containing at least epoxide; and(d) isolating the epoxide from the aqueous salt solution;wherein water is recovered from the product of at least Step (b) and recycled into Step (a) for use in forming the low chlorides aqueous hypochlorous acid solution. In this process, not only is the water internally recycled after Step (b), but a concentrated brine solution is generated in both Steps (a) and (d) which is useful in other processes such as electrochemical production of chlorine and caustic. The chlorine and caustic, in turn, may then be recycled back to the method of this invention.

    摘要翻译： 本文描述了一种连续生产环氧化物的方法，抑制氯化副产物的形成，并且消除或显着减少废水排放。 该方法包括：（a）形成低氯化物次氯酸水溶液; （b）将低氯化物次氯酸水溶液与至少一种不饱和有机化合物接触以形成至少含有氯代醇的含水有机产物; （c）至少使烯丙基氯醇与碱金属氢氧化物水溶液接触以形成至少含有环氧化物的盐水溶液产物; 和（d）从盐水溶液中分离环氧化物; 其中从至少步骤（b）的产物中回收水并再循环到步骤（a）中，以用于形成低氯酸盐次氯酸水溶液。 在这个过程中，不仅在步骤（b）之后内部循环的水，而且在步骤（a）和（d）中产生浓缩的盐水溶液，其可用于其它方法如氯和苛性碱的电化学生产。 然后将氯和苛性碱又可循环回本发明的方法。