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    BIDIRECTIONAL SHAPE-MEMORY POLYMER, METHOD OF ITS PRODUCTION AND ITS USE
    62.
    发明申请
    BIDIRECTIONAL SHAPE-MEMORY POLYMER, METHOD OF ITS PRODUCTION AND ITS USE 审中-公开
    双向形状记忆聚合物，其生产方法及其用途

    公开(公告)号：US20150344600A1

    公开(公告)日：2015-12-03

    申请号：US14653941

    申请日：2013-12-20

    Applicant: HELMOHOLTZ-ZENTRUM GEESTHACHT ZENTRUM FÜR MATERIAL UNDKÜSTENFORSCHUNG GMBH

    Inventor： Marc Behl ,  Karl Kratz ,  Ulrich Noechel ,  Tilman Sauter ,  Joerg Zotzmann ,  Srinivasa Reddy Chaganti ,  Andreas Lendlein

    IPC: C08F210/02 ,  H01F1/42 ,  C08G63/91 ,  C08G18/42 ,  C08G81/02

    CPC classification number: C08F210/02 ,  B29C61/003 ,  B29C61/06 ,  C08G18/4277 ,  C08G63/91 ,  C08G81/021 ,  C08G81/027 ,  C08G2280/00 ,  C08J3/248 ,  H01F1/42

    Abstract: The present invention relates to an article consisting of or comprising a bidirectional shape-memory polymer (bSMP), the bSMP comprising: first phase-segregated domains (AD) having a first transition temperature (Tt,AD) corresponding to a crystallization transition or glass transition of the first domains (AD), second phase-segregated domains (SD) having a second transition temperature (Tt,AD) corresponding to a crystallization transition or glass transition of the second domains (SD), the second transition temperature (Tt,SD) being higher than the first transition temperature (Tt,AD), and covalent or physical bonds cross-linking the polymer chains of the bSMP, and in this way interconnecting the first and second domains (AD, SD), wherein the second phase-separated domains (SD) form a skeleton which is at least partially embedded in the first phase-segregated domains (AD), and wherein polymer chain segments of the bSMP forming the first domains (AD) are substantially orientated in a common direction, such that the bSMP is able to undergo a reversible shape-shift between a first shape (A) at a first temperature (Thigh) and a second shape (B) at a second temperature (Tlow) upon variation of temperature between the first and second temperature (Thigh, Tlow) driven by the crystallization and melting or vitrification and melting of the first phase-separated domains (AD) and without application of an external stress, with Tlow

    Abstract translation: 本发明涉及由双向形状记忆聚合物（bSMP）组成或包含双边形状记忆聚合物（bSMP）的物品，所述bSMP包括：具有对应于结晶转变的第一转变温度（Tt，AD）的第一分相畴（AD）或玻璃 具有对应于第二结构域（SD）的结晶转变或玻璃化转变的第二转变温度（Tt，AD）的第一结构域（AD），第二分相畴（SD）的转变，第二转变温度（Tt， SD）高于第一转变温度（Tt，AD），并且共价或物理键交联bSMP的聚合物链，并且以这种方式互连第一和第二结构域（AD，SD），其中第二相 分离结构域（SD）形成至少部分地嵌入第一分相结构域（AD）中的骨架，并且其中形成第一结构域（AD）的bSMP的聚合物链段基本上定向于共 使得bSMP在第一温度（Thigh）的第一形状（A）和第二温度（Tlow）的第二形状（B）之间能够在第二温度（Tlow）之间经历可逆形状位移 第一和第二温度（Thigh，Tlow）由第一相分离结构域（AD）的结晶和熔化或玻璃化和熔化而驱动并且不施加外部应力，Tlow

    Water absorbent material, method for production of surface cross-linked water absorbent resin, and method for evaluation of water absorbent material
    64.
    发明授权
    Water absorbent material, method for production of surface cross-linked water absorbent resin, and method for evaluation of water absorbent material 有权
    吸水材料，表面交联吸水性树脂的制造方法以及吸水材料的评价方法

    公开(公告)号：US08501873B2

    公开(公告)日：2013-08-06

    申请号：US11660758

    申请日：2005-08-31

    Applicant: Masazumi Sasabe ,  Kenji Kadonaga ,  Shigeru Sakamoto ,  Motohiro Imura ,  Tsunemasa Ueno ,  Hiroko Ueda ,  Yoshifumi Adachi

    Inventor： Masazumi Sasabe ,  Kenji Kadonaga ,  Shigeru Sakamoto ,  Motohiro Imura ,  Tsunemasa Ueno ,  Hiroko Ueda ,  Yoshifumi Adachi

    IPC: C08F8/42 ,  C08F8/12 ,  C08F6/02

    CPC classification number: C08J3/248 ,  C08J3/243 ,  C08J2300/14 ,  Y10T428/254 ,  Y10T428/2982

    Abstract: A homogeneously surface cross-linked water absorbent resin and a method for the production thereof are provided.The water absorbent material is formed of a surface cross-linked water absorbent resin resulting from granular irregularly pulverized shaped surface cross-linking the product of partial neutralization or whole neutralization of a water absorbent resin having acrylic acid or a metal salt thereof as a main component, which water absorbent material shows a metal atom concentration on the surface of the water absorbent material in the range of 0-10% within 0 second of polishing and 2-35% at 10 seconds value of polishing as determined by subjecting the water absorbent material to Ar ion discharge polishing under a voltage of 500 Å. The surface cross-linked water absorbent resin to be used herein can be produced by surface cross-linking a water absorbent resin having a specific particle diameter with a surface cross-linking agent having a water concentration in a specific range.

    Abstract translation: 提供均匀的表面交联型吸水性树脂及其制造方法。 吸水材料由表面交联的吸水性树脂形成，该表面交联的吸水性树脂是由具有丙烯酸或其金属盐作为主要成分的吸水性树脂的部分中和或全部中和产生的颗粒不规则粉碎的表面交联而成的 该吸水材料在抛光的0秒内在吸水材料的表面上表现出0-10％的范围内的金属原子浓度，在10秒的抛光时间为2-35％，通过使吸水材料 在500的电压下进行Ar离子放电研磨。 这里使用的表面交联型吸水性树脂可以通过将具有特定粒径的吸水性树脂与具有特定范围的水分浓度的表面交联剂进行表面交联来制造。

    Polyolefin treatment process for uniform crosslinking
    65.
    发明申请
    Polyolefin treatment process for uniform crosslinking 审中-公开
    聚烯烃处理工艺均匀交联

    公开(公告)号：US20120178843A1

    公开(公告)日：2012-07-12

    申请号：US12986163

    申请日：2011-01-06

    Applicant: Dehchuan Sun

    Inventor： Dehchuan Sun

    IPC: C08F110/02 ,  C08F2/46

    CPC classification number: C08J3/247 ,  C08F8/50 ,  C08J3/248 ,  C08J7/08 ,  C08J7/123 ,  C08J2323/02 ,  C08F110/02

    Abstract: A process produces a block of polyolefin material with uniform crosslinking, which may be uniform between and within polymer chains in the polyolefin material. Steps include: providing an oven; placing the block into the oven; preheating the block to a uniform temperature above the melting point; further heating the block to a temperature at least 30 degrees Centigrade above the melting point; cooling the block to room temperature under an inert gas; and removing oxidized material from surface of the block. Optional steps include: subjecting the block to radiation before placing the block into the oven; removing the gases from the oven on a continuous or stepwise basis; controlling the purge gas flow out of the oven; and determining a heating time period for the block by subjecting control blocks to the same process and analyzing them after various heating times.

    Abstract translation: 一种方法产生具有均匀交联的聚烯烃材料块，其在聚烯烃材料中的聚合物链之间和聚合物链之间可以是均匀的。 步骤包括：提供烤箱; 将块放入烤箱中; 将块体预热至高于熔点的均匀温度; 进一步将块体加热至高于熔点至少30摄氏度的温度; 在惰性气体下将块体冷却至室温; 并从块的表面除去氧化的材料。 可选步骤包括：在将块放入烘箱之前对块进行辐射; 以连续或逐步的方式从烤箱中取出气体; 控制吹扫气体流出烘箱; 以及通过对控制块进行相同的处理并在各种加热时间之后对其进行分析来确定块的加热时间段。

    Method for estimating state of ultraviolet curing resin material
    68.
    发明申请
    Method for estimating state of ultraviolet curing resin material 有权
    用于估计紫外线固化树脂材料的状态的方法

    公开(公告)号：US20070216069A1

    公开(公告)日：2007-09-20

    申请号：US11717785

    申请日：2007-03-14

    Applicant: Kiyoshi Imai ,  Hiroyuki Inoue ,  Tadashi Senga ,  Kenichi Nakamune ,  Yoji Hasebe

    Inventor： Kiyoshi Imai ,  Hiroyuki Inoue ,  Tadashi Senga ,  Kenichi Nakamune ,  Yoji Hasebe

    IPC: B29C35/08

    CPC classification number: G01N21/6408 ,  C08J3/248 ,  G01N33/442

    Abstract: A CPU provides a fluorescent light detecting head with an irradiation instruction, in response to which the fluorescent light detecting head irradiates an ultraviolet ray for detection on an ultraviolet curing resin material to be examined. The CPU then acquires from the fluorescent light detecting head an intensity of a fluorescent light emitted from a photo polymerization initiator included in the ultraviolet curing resin material when receiving the ultraviolet ray for detection. The CPU retrieves a predetermined number of past data of the intensity of the fluorescent light from a storage unit and performs a (moving) average calculation processing to calculate the intensity of the fluorescent light at the current time. The CPU performs an estimation processing of a state of the ultraviolet curing resin material based on the calculated intensity of the fluorescent light.

    Abstract translation: CPU提供具有照射指示的荧光检测头，响应于此，荧光检测头照射用于检测的紫外线固化树脂材料的紫外线。 然后，CPU在接收到用于检测的紫外线时，从荧光检测头获取从包含在紫外线固化树脂材料中的光聚合引发剂发射的荧光的强度。 CPU从存储单元检索预定数量的荧光强度的过去数据，并执行（移动）平均计算处理以计算当前时间的荧光强度。 CPU根据计算出的荧光强度对紫外线固化树脂材料的状态进行估计处理。

    Method for determining cure in a polycarboxylic acid bindered material
    69.
    发明授权
    Method for determining cure in a polycarboxylic acid bindered material 有权

    公开(公告)号：US07063983B2

    公开(公告)日：2006-06-20

    申请号：US10160775

    申请日：2002-05-31

    Applicant: Liang Chen

    Inventor： Liang Chen

    IPC: G01N33/00

    CPC classification number: C08J3/248 ,  G01N31/22 ,  Y10T436/201666

    Abstract: By utilizing a pH indicator having known color change characteristics, an accurate determination of the pH of a binder surface, and hence the amount of cure of a polycarboxylic acid based binder on the fiberglass fibers, can be easily determined for polycarboxylic binder based fiberglass materials used in insulation and composite applications. Based on these results, the manufacturing line used to make these bindered materials may be adjusted to ensure adequate curing at maximum efficiency while minimizing operating costs and reducing waste.

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