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    CARRIER TREATMENT TO IMPROVE CATALYTIC PERFORMANCE OF AN ETHYLENE OXIDE CATALYST
    13.
    发明申请
    CARRIER TREATMENT TO IMPROVE CATALYTIC PERFORMANCE OF AN ETHYLENE OXIDE CATALYST 审中-公开
    载体处理提高乙烯氧化物催化剂的催化性能

    公开(公告)号：US20150329510A1

    公开(公告)日：2015-11-19

    申请号：US14811309

    申请日：2015-07-28

    Applicant: Scientific Design Company, Inc.

    Inventor： Nabil Rizkalla ,  Andrzej Rokicki

    IPC: C07D301/10 ,  C01F7/02 ,  B01J37/02 ,  B01J21/04 ,  B01J23/66

    CPC classification number: C07D301/10 ,  B01J21/04 ,  B01J23/50 ,  B01J23/66 ,  B01J23/688 ,  B01J37/0201 ,  B01J37/0207 ,  B01J37/06 ,  C01F7/02

    Abstract: A method for lowering the sodium content of different carriers which may have different physical properties as well as varying degrees of sodium is provided. The method, which lowers the sodium content from the surface, subsurface as well as the binding layer of the carrier, includes contacting a carrier with water. A rinse solution is recovered from the contacting. The rinse solution includes leached sodium from the carrier. The sodium content in the rinse solution is then determined. The contacting, recovering and determining are repeated until a steady state in the sodium content is achieved.

    Abstract translation: 提供了降低可能具有不同物理性质以及不同程度的钠的不同载体的钠含量的方法。 降低表面，地下以及载体结合层的钠含量的方法包括使载体与水接触。 从接触中回收漂洗溶液。 冲洗溶液包括从载体中浸出的钠。 然后确定冲洗溶液中的钠含量。 重复接触，回收和测定，直到达到钠含量的稳定状态。

    Carrier treatment to improve catalytic performance of an ethylene oxide catalyst
    14.
    发明授权
    Carrier treatment to improve catalytic performance of an ethylene oxide catalyst 有权
    载体处理以改善环氧乙烷催化剂的催化性能

    公开(公告)号：US09095843B2

    公开(公告)日：2015-08-04

    申请号：US14279534

    申请日：2014-05-16

    Applicant: Scientific Design Company, Inc.

    Inventor： Nabil Rizkalla ,  Andrzej Rokicki

    IPC: B01J21/04 ,  B01J23/50 ,  C07D301/10

    CPC classification number: C07D301/10 ,  B01J21/04 ,  B01J23/50 ,  B01J23/66 ,  B01J23/688 ,  B01J37/0201 ,  B01J37/0207 ,  B01J37/06 ,  C01F7/02

    Abstract: A method for lowering the sodium content of different carriers which may have different physical properties as well as varying degrees of sodium is provided. The method, which lowers the sodium content from the surface, subsurface as well as the binding layer of the carrier, includes contacting a carrier with water. A rinse solution is recovered from the contacting. The rinse solution includes leached sodium from the carrier. The sodium content in the rinse solution is then determined. The contacting, recovering and determining are repeated until a steady state in the sodium content is achieved.

    Abstract translation: 提供了降低可能具有不同物理性质以及不同程度的钠的不同载体的钠含量的方法。 降低表面，地下以及载体结合层的钠含量的方法包括使载体与水接触。 从接触中回收漂洗溶液。 冲洗溶液包括从载体中浸出的钠。 然后确定冲洗溶液中的钠含量。 重复接触，回收和测定，直到达到钠含量的稳定状态。

    CARRIER FOR ETHYLENE OXIDE CATALYSTS
    16.
    发明申请
    CARRIER FOR ETHYLENE OXIDE CATALYSTS 有权
    乙烯氧化物催化剂载体

    公开(公告)号：US20140343307A1

    公开(公告)日：2014-11-20

    申请号：US14279570

    申请日：2014-05-16

    Applicant: Scientific Design Company, Inc.

    Inventor： Nabil Rizkalla ,  Andrzej Rokicki

    IPC: B01J23/68 ,  B01J23/50 ,  C07D301/10 ,  B01J21/06

    CPC classification number: B01J23/685 ,  B01J21/04 ,  B01J21/063 ,  B01J23/26 ,  B01J23/50 ,  B01J23/688 ,  B01J37/0207 ,  C07D301/10 ,  Y02P20/52

    Abstract: A carrier for an ethylene epoxidation catalyst is provided that includes an alumina first component and a mixed metal oxide of alumina second component. The mixed metal oxide of alumina second component comprises a corundum lattice structure having a plurality of O—Al—O bonds, wherein an Al atom of at least one O—Al—O bond of the plurality of O—Al—O bonds, but not all of the plurality of O—Al—O bonds, is replaced with a divalent or trivalent transition metal selected from the group consisting of scandium (Sc), titanium (Ti), vanadium (V), chromium (Cr), manganese (Mn), iron (Fe), cobalt (Co), nickel (Ni) copper (Cu), and zinc (Zn). A catalyst containing the carrier, as well as a process for the epoxidation of ethylene using the catalyst are also disclosed.

    Abstract translation: 提供了一种用于乙烯环氧化催化剂的载体，其包括氧化铝第一组分和氧化铝第二组分的混合金属氧化物。 氧化铝第二成分的混合金属氧化物包括具有多个O-Al-O键的刚玉晶格结构，其中多个O-Al-O键中的至少一个O-Al-O键的Al原子，但是 不是所有的多个O-Al-O键都被选自钪（Sc），钛（Ti），钒（V），铬（Cr），锰（ Mn），铁（Fe），钴（Co），镍（Ni）铜（Cu）和锌（Zn）。 还公开了含有载体的催化剂以及使用该催化剂对乙烯进行环氧化的方法。

    HIGH CONCENTRATION SILVER SOLUTIONS FOR ETHYLENE OXIDE CATALYST PREPARATION
    19.
    发明申请
    HIGH CONCENTRATION SILVER SOLUTIONS FOR ETHYLENE OXIDE CATALYST PREPARATION 审中-公开
    用于乙烯氧化物催化剂制备的高浓度银溶液

    公开(公告)号：US20150174554A1

    公开(公告)日：2015-06-25

    申请号：US14575035

    申请日：2014-12-18

    Applicant: Scientific Design Company, Inc.

    Inventor： Lixin Cao ,  Andrzej Rokicki

    IPC: B01J23/68

    CPC classification number: B01J23/688 ,  B01J23/50 ,  B01J31/00 ,  B01J35/1009 ,  B01J37/0203 ,  B01J37/0207 ,  B01J37/0213 ,  B01J37/06

    Abstract: A silver impregnation solution comprising: (i) silver ions, (ii) a silver concentration enhancer selected from at least one ammonium salt having an anionic component that is thermally decomposable; or at least one amino acid, or a combination thereof, (iii) at least one organic amine; and (iv) water; wherein said components (i)-(iii) are dissolved in said impregnation solution, and oxalic acid may or may not be included. The silver impregnation solution can achieve significantly higher silver concentrations, including at least or above 33, 34, or 35 wt %. Methods for producing a silver catalyst by silver impregnation of a refractory support followed by calcination are also described. The resulting silver catalysts possess high silver loadings of typically at least 17, 18, or 19 wt %.

    Abstract translation: 一种银浸渍溶液，其包含：（i）银离子，（ii）选自至少一种具有可分解阴离子组分的铵盐的银浓度增强剂; 或至少一种氨基酸，或其组合，（iii）至少一种有机胺; 和（iv）水; 其中所述组分（i） - （iii）溶解在所述浸渍溶液中，并且可以不包括草酸。 银浸渍溶液可以获得显着更高的银浓度，包括至少或高于33,34或35重量％。 还描述了通过浸渍耐火载体然后煅烧来生产银催化剂的方法。 所得到的银催化剂具有通常至少17,18或19重量％的高银负载量。

    CARRIER TREATMENT TO IMPROVE CATALYTIC PERFORMANCE OF AN ETHYLENE OXIDE CATALYST
    20.
    发明申请
    CARRIER TREATMENT TO IMPROVE CATALYTIC PERFORMANCE OF AN ETHYLENE OXIDE CATALYST 有权
    载体处理提高乙烯氧化物催化剂的催化性能

    公开(公告)号：US20140343306A1

    公开(公告)日：2014-11-20

    申请号：US14279534

    申请日：2014-05-16

    Applicant: SCIENTIFIC DESIGN COMPANY, INC.

    Inventor： Nabil Rizkalla ,  Andrzej Rokicki

    IPC: B01J23/50 ,  C07D301/10 ,  B01J21/04

    CPC classification number: C07D301/10 ,  B01J21/04 ,  B01J23/50 ,  B01J23/66 ,  B01J23/688 ,  B01J37/0201 ,  B01J37/0207 ,  B01J37/06 ,  C01F7/02

    Abstract: A method for lowering the sodium content of different carriers which may have different physical properties as well as varying degrees of sodium is provided. The method, which lowers the sodium content from the surface, subsurface as well as the binding layer of the carrier, includes contacting a carrier with water. A rinse solution is recovered from the contacting. The rinse solution includes leached sodium from the carrier. The sodium content in the rinse solution is then determined. The contacting, recovering and determining are repeated until a steady state in the sodium content is achieved.

    Abstract translation: 提供了降低可能具有不同物理性质以及不同程度的钠的不同载体的钠含量的方法。 降低表面，地下以及载体结合层的钠含量的方法包括使载体与水接触。 从接触中回收漂洗溶液。 冲洗溶液包括从载体中浸出的钠。 然后确定冲洗溶液中的钠含量。 重复接触，回收和测定，直到达到钠含量的稳定状态。

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