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    PROCESS OF MAKING DIFLUOROTHIENOTHIOPHENE BASED CONJUGATED POLYMERS
    11.
    发明申请
    PROCESS OF MAKING DIFLUOROTHIENOTHIOPHENE BASED CONJUGATED POLYMERS 审中-公开
    制备基于二氢苯并噻二唑的共聚聚合物的方法

    公开(公告)号：US20150344495A1

    公开(公告)日：2015-12-03

    申请号：US14722919

    申请日：2015-05-27

    Applicant: PHILLIPS 66 COMPANY ,  SOLARMER ENERGY, INC.

    Inventor： Wei Wang ,  Jun Yang ,  Chenjun Shi ,  Christopher Daeffler ,  Janice Hawkins ,  Yue Wu ,  Ting He ,  Hui Huang ,  Amit Palkar ,  Kathy Woody ,  Joe Bullock

    IPC: C07D495/04

    CPC classification number: C07D495/04

    Abstract: A method of producing a monomer wherein the method begins by dissolving 3-fluoro-4,6 dihydrothieno[3,4-b]thiophene in a solvent to create a solution. An initiator is then added to the solution to produce an initiated solution. This is followed by adding a fluorinated chemical to the initiated solution to produce 2,3-difluoro-4,6-dihydrothieno[3,4-b]thiophene. 2,3-difluoro-4,6-dihydrothieno[3,4-b]thiophene is then oxidized with an oxidant to produce 2,3-difluorothieno[3,4-b]thiophene. 2,3-difluorothieno[3,4-b]thiophene is then bromoated to produce 4,6-dibromo-2,3-difluorothieno[2,3-c]thiophene. The final step involves debrominating 4,6-dibromo-2,3-difluorothieno[2,3-c]thiophene and adding an aryl group to produce the monomer

    Abstract translation: 制备单体的方法，其中该方法开始于将3-氟-4,6-二氢噻吩并[3,4-b]噻吩溶于溶剂中以产生溶液。 然后将引发剂加入到溶液中以产生引发的溶液。 然后在引发的溶液中加入氟化物，生成2,3-二氟-4,6-二氢噻吩并[3,4-b]噻吩。 然后用氧化剂氧化2,3-二氟-4,6-二氢噻吩并[3,4-b]噻吩，得到2,3-二氟噻吩并[3,4-b]噻吩。 然后将2,3-二氟噻吩并[3,4-b]噻吩溴化，得到4,6-二溴-2,3-二氟噻吩并[2,3-c]噻吩。 最后一步涉及脱溴4,6-二溴-2,3-二氟噻吩并[2,3-c]噻吩并加入芳基来制备单体

    ANTHRADITHIOPHENE-BASED SEMICONDUCTING POLYMERS AND METHODS THEREOF
    13.
    发明申请
    ANTHRADITHIOPHENE-BASED SEMICONDUCTING POLYMERS AND METHODS THEREOF 有权
    基于十二烷基的半导体聚合物及其方法

    公开(公告)号：US20150136224A1

    公开(公告)日：2015-05-21

    申请号：US14532229

    申请日：2014-11-04

    Applicant: Phillips 66 Company ,  Solarmer Energy, Inc.

    Inventor： Chenjun Shi ,  Ruby Chen ,  Jun Yang ,  Christopher S. Daeffler ,  Janice Hawkins ,  Yue Wu ,  Wei Wang ,  Kathy Woody ,  Joe Bullock ,  Hui Huang ,  Amit Palkar ,  Ting He

    IPC: H01L51/00 ,  H01L51/44 ,  H01L51/42 ,  C08G61/12

    CPC classification number: H01L51/0036 ,  C08G61/126 ,  C08G2261/12 ,  C08G2261/18 ,  C08G2261/3243 ,  C08G2261/91 ,  C09K11/06 ,  C09K2211/1458 ,  H01L51/0043 ,  H01L51/0074 ,  H01L51/4253 ,  H01L2251/308 ,  Y02E10/549

    Abstract: Compositions, synthesis and applications for benzene, furan, thiophene, selenophene, pyrole, pyran, pyridine, oxazole, thiazole and imidazole derivatized anthra[2,3-b:6,7-b′]dithiophene (ADT) based polymers, namely, poly{5,11-bis(5-(2-ethylhexyl)thiophen-2-yl)anthra[2,3-b:6,7-b′]dithiophene-2,8-diyl-alt-2-ethyl-1-(thieno[3,4-b]thiophen-2-yl)hexan-1-one-4,6-diyl}, poly{5,11-bis(5-(2-ethylhexyl)furan-2-yl)anthra[2,3-b:6,7-b′]dithiophene-2,8-diyl-alt-2-ethyl-1-(thieno[3,4-b]thiophen-2-yl)hexan-1-one-4,6-diyl and poly{5,11-bis(5-(2-ethylhexyl)selenophen-2-yl)anthra[2,3-b:6,7-b′]dithiophene-2,8-diyl-alt-2-ethyl-1-(thieno[3,4-b]thiophen-2-yl)hexan-1-one-4,6-diyl} are disclosed. Further, an organic solar cell constructed of a derivatized anthra[2,3-b:6,7-b′]dithiophene (ADT) based polymer is discussed.

    Abstract translation: 苯，呋喃，噻吩，硒吩，吡咯，吡喃，吡啶，恶唑，噻唑和咪唑衍生化的蒽[2,3-b：6,7-b']二噻吩（ADT）基聚合物的组合物，合成和应用， 聚[5,11-双（5-（2-乙基己基）噻吩-2-基）蒽[2,3-b：6,7-b']二噻吩-2,8-二基-2-乙基-2-乙基 - 1-（噻吩并[3,4-b]噻吩-2-基）己-1-酮-4,6-二基}，聚{5,11-双（5-（2-乙基己基）呋喃-2-基 ）噻吩[2,3-b：6,7-b']二噻吩-2,8-二基-2-乙基-1-（噻吩并[3,4-b]噻吩-2-基）己烷-1 - 酮-4,6-二基和聚{5,11-双（5-（2-乙基己基）硒吩-2-基）蒽[2,3-b：6,7-b']二噻吩-2,8 - 二基-2-乙基-1-（噻吩并[3,4-b]噻吩-2-基）己-1-酮-4,6-二基}。 此外，讨论了由衍生的蒽[2,3-b：6,7-b']二噻吩（ADT）基聚合物构成的有机太阳能电池。

    Process of making difluorothienothiophene based conjugated polymers
    17.
    发明授权
    Process of making difluorothienothiophene based conjugated polymers 有权
    制备二氟噻吩并噻吩基共轭聚合物的方法

    公开(公告)号：US09278980B2

    公开(公告)日：2016-03-08

    申请号：US14722919

    申请日：2015-05-27

    Applicant: PHILLIPS 66 COMPANY ,  SOLARMER ENERGY, INC.

    Inventor： Wei Wang ,  Jun Yang ,  Chenjun Shi ,  Christopher Daeffler ,  Janice Hawkins ,  Yue Wu ,  Ting He ,  Hui Huang ,  Amit Palkar ,  Kathy Woody ,  Joe Bullock

    IPC: C07D495/04

    CPC classification number: C07D495/04

    Abstract: A method of producing a monomer wherein the method begins by dissolving 3-fluoro-4,6 dihydrothieno[3,4-b]thiophene in a solvent to create a solution. An initiator is then added to the solution to produce an initiated solution. This is followed by adding a fluorinated chemical to the initiated solution to produce 2,3-difluoro-4,6-dihydrothieno[3,4-b]thiophene. 2,3-difluoro-4,6-dihydrothieno[3,4-b]thiophene is then oxidized with an oxidant to produce 2,3-difluorothieno[3,4-b]thiophene. 2,3-difluorothieno[3,4-b]thiophene is then bromoated to produce 4,6-dibromo-2,3-difluorothieno[2,3-c]thiophene. The final step involves debrominating 4,6-dibromo-2,3-difluorothieno[2,3-c]thiophene and adding an aryl group to produce the monomer

    Abstract translation: 制备单体的方法，其中该方法开始于将3-氟-4,6-二氢噻吩并[3,4-b]噻吩溶于溶剂中以产生溶液。 然后将引发剂加入到溶液中以产生引发的溶液。 然后在引发的溶液中加入氟化物，生成2,3-二氟-4,6-二氢噻吩并[3,4-b]噻吩。 然后用氧化剂氧化2,3-二氟-4,6-二氢噻吩并[3,4-b]噻吩，得到2,3-二氟噻吩并[3,4-b]噻吩。 然后将2,3-二氟噻吩并[3,4-b]噻吩溴化，得到4,6-二溴-2,3-二氟噻吩并[2,3-c]噻吩。 最后一步涉及脱溴4,6-二溴-2,3-二氟噻吩并[2,3-c]噻吩并加入芳基来制备单体

    Anthradithiophene-based semiconducting polymers and methods thereof
    18.
    发明授权
    Anthradithiophene-based semiconducting polymers and methods thereof 有权
    基于蒽并噻吩的半导体聚合物及其方法

    公开(公告)号：US09214635B2

    公开(公告)日：2015-12-15

    申请号：US14532229

    申请日：2014-11-04

    Applicant: Phillips 66 Company ,  Solarmer Energy, Inc.

    Inventor： Chenjun Shi ,  Ruby Chen ,  Jun Yang ,  Christopher S. Daeffler ,  Janice Hawkins ,  Yue Wu ,  Wei Wang ,  Kathy Woody ,  Joe Bullock ,  Hui Huang ,  Amit Palkar ,  Ting He

    IPC: C08G61/12 ,  H01L51/00 ,  H01L51/42

    CPC classification number: H01L51/0036 ,  C08G61/126 ,  C08G2261/12 ,  C08G2261/18 ,  C08G2261/3243 ,  C08G2261/91 ,  C09K11/06 ,  C09K2211/1458 ,  H01L51/0043 ,  H01L51/0074 ,  H01L51/4253 ,  H01L2251/308 ,  Y02E10/549

    Abstract: Compositions, synthesis and applications for benzene, furan, thiophene, selenophene, pyrole, pyran, pyridine, oxazole, thiazole and imidazole derivatized anthra[2,3-b:6,7-b′]dithiophene (ADT) based polymers, namely, poly{5,11-bis(5-(2-ethylhexyl)thiophen-2-yl)anthra[2,3-b:6,7-b′]dithiophene-2,8-diyl-alt-2-ethyl-1-(thieno[3,4-b]thiophen-2-yl)hexan-1-one-4,6-diyl}, poly{5,11-bis(5-(2-ethylhexyl)furan-2-yl)anthra[2,3-b:6,7-b′]dithiophene-2,8-diyl-alt-2-ethyl-1-(thieno[3,4-b]thiophen-2-yl)hexan-1-one-4,6-diyl and poly{5,11-bis(5-(2-ethylhexyl)selenophen-2-yl)anthra[2,3-b:6,7-b′]dithiophene-2,8-diyl-alt-2-ethyl-1-(thieno[3,4-b]thiophen-2-yl)hexan-1-one-4,6-diyl} are disclosed. Further, an organic solar cell constructed of a derivatized anthra[2,3-b:6,7-b′]dithiophene (ADT) based polymer is discussed.

    Abstract translation: 苯，呋喃，噻吩，硒吩，吡咯，吡喃，吡啶，恶唑，噻唑和咪唑衍生化的蒽[2,3-b：6,7-b']二噻吩（ADT）基聚合物的组合物，合成和应用， 聚[5,11-双（5-（2-乙基己基）噻吩-2-基）蒽[2,3-b：6,7-b']二噻吩-2,8-二基-2-乙基-2-乙基 - 1-（噻吩并[3,4-b]噻吩-2-基）己-1-酮-4,6-二基}，聚{5,11-双（5-（2-乙基己基）呋喃-2-基 ）噻吩[2,3-b：6,7-b']二噻吩-2,8-二基-2-乙基-1-（噻吩并[3,4-b]噻吩-2-基）己烷-1 - 酮-4,6-二基和聚{5,11-双（5-（2-乙基己基）硒吩-2-基）蒽[2,3-b：6,7-b']二噻吩-2,8 - 二基-2-乙基-1-（噻吩并[3,4-b]噻吩-2-基）己-1-酮-4,6-二基}。 此外，讨论了由衍生的蒽[2,3-b：6,7-b']二噻吩（ADT）基聚合物构成的有机太阳能电池。

    COMPOSITIONS AND APPLICATIONS OF A MULTI-COMPONENT BENZO[1,2-B:4,5-B] DITHIOPHENE-THIENOTHIOPHENE RANDOMLY SUBSTITUTED POLYMERS FOR ORGANIC SOLAR CELLS
    19.
    发明申请
    COMPOSITIONS AND APPLICATIONS OF A MULTI-COMPONENT BENZO[1,2-B:4,5-B] DITHIOPHENE-THIENOTHIOPHENE RANDOMLY SUBSTITUTED POLYMERS FOR ORGANIC SOLAR CELLS 有权
    多组分苯并[1,2-B：4,5-B]二氢苯并噻喃的组合物和应用随机取代的有机太阳能电池聚合物

    公开(公告)号：US20150349260A1

    公开(公告)日：2015-12-03

    申请号：US14722573

    申请日：2015-05-27

    Applicant: PHILLIPS 66 COMPANY ,  SOLARMER ENERGY, INC.

    Inventor： Kathy Woody ,  Hui Huang ,  Ting He ,  Wei Wang ,  Chenjun Shi ,  Yue Wu

    IPC: H01L51/00 ,  C08G75/06

    CPC classification number: H01L51/0036 ,  H01L51/0043 ,  H01L51/0047 ,  H01L51/4253 ,  Y02E10/549

    Abstract: A polymer having at least four different repeat units comprising: In this polymer R1, R2, R3 and R4 can be independently selected from the group consisting of alkyl group, alkoxy group, aryl groups and combinations thereof and where the combination of R1, R2, R3 and R4 are not all identical. Additionally, in this polymer, m, n, o and p can be greater than 1. x and y are different from each other and can be independently selected from the group consisting of: of alkyl group, alkoxy group, aryl groups, where y=1-3, where y=0-12, where R5 is selected from the group consisting of H, of alkyl group, alkoxy group, aryl groups, where R6 is selected from the group consisting of H, alkyl, substituted alkyls, aryls and substituted aryls, where R7 and R8 are independently selected from the group consisting of H, of alkyl group, alkoxy group, aryl groups, —NR9R10 where R9 and R10 are independently selected from the group consisting of H, of alkyl group, alkoxy group, aryl groups.

    Abstract translation: 具有至少四个不同重复单元的聚合物包括：在该聚合物R1中，R2，R3和R4可以独立地选自烷基，烷氧基，芳基及其组合，并且其中R1，R2， R3和R4不完全相同。 另外，在该聚合物中，m，n，o和p可以大于1.x和y彼此不同，并且可以独立地选自：烷基，烷氧基，芳基，其中y = 1-3，其中y = 0-12，其中R 5选自H，烷基，烷氧基，芳基，其中R 6选自H，烷基，取代的烷基，芳基 和取代的芳基，其中R 7和R 8独立地选自H，烷基，烷氧基，芳基，-NR 9 R 10，其中R 9和R 10独立地选自H，烷基，烷氧基 ，芳基。

    PROCESS OF PRODUCING AND APPLICATIONS OF A MULTI-COMPONENT BENZO[1,2-B:4,5-B] DIFLUOROTHIENOTHIOPHENE RANDOMLY SUBSTITUTED POLYMERS FOR ORGANIC SOLAR CELLS
    20.
    发明申请
    PROCESS OF PRODUCING AND APPLICATIONS OF A MULTI-COMPONENT BENZO[1,2-B:4,5-B] DIFLUOROTHIENOTHIOPHENE RANDOMLY SUBSTITUTED POLYMERS FOR ORGANIC SOLAR CELLS 有权
    多组分苯并[1,2-B：4,5-B]衍生物的制备及应用方法有机太阳能电池的随机取代的聚合物

    公开(公告)号：US20150344630A1

    公开(公告)日：2015-12-03

    申请号：US14722650

    申请日：2015-05-27

    Applicant: PHILLIPS 66 COMPANY ,  SOLARMER ENERGY, INC.

    Inventor： Wei Wang ,  Jun Yang ,  Chenjun Shi ,  Christopher Daeffler ,  Janice Hawkins ,  Yue Wu ,  Ting He ,  Hui Huang ,  Amit Palkar ,  Kathy Woody ,  Joe Bullock

    IPC: C08G75/06

    CPC classification number: C08G75/06 ,  A61K31/4162 ,  C07B59/002 ,  C07D495/04 ,  C08G61/123

    Abstract: A process of dissolving 3-fluoro-4,6-dihydrothieno[3,4-b]thiophene in a solvent to create a solution. An initiator is then added to the solution to produce an initiated solution followed by adding a fluorinated chemical to the initiated solution to produce 2,3-difluoro-4,6-dihydrothieno[3,4-b]thiophene. 2,3-difluoro-4,6-dihydrothieno[3,4-b]thiophene is then oxidized with an oxidant to produce 2,3-difluorothieno[3,4-b]thiophene. A brominating step then occurs to the 2,3-difluorothieno[3,4-b]thiophene to produce 4,6-dibromo-2,3-difluorothieno[2,3-c]thiophene. 4,6-dibromo-2,3-difluorothieno[2,3-c]thiophene is then debrominated and polymerized to The stoichiometric ratio of (f+g)≈h and f, g and h are not equal to 0. Additionally, in this embodiment R1, R2, R3 and R4 are independently selected from the group consisting of alkyl group, alkoxy group, aryl groups and combinations thereof and where the combination of R1, R2, R3 and R4 are not all identical.

    Abstract translation: 将3-氟-4,6-二氢噻吩并[3,4-b]噻吩溶解在溶剂中以产生溶液的方法。 然后将引发剂加入到溶液中以产生引发的溶液，然后向引发的溶液中加入氟化物，得到2,3-二氟-4,6-二氢噻吩并[3,4-b]噻吩。 然后用氧化剂氧化2,3-二氟-4,6-二氢噻吩并[3,4-b]噻吩，得到2,3-二氟噻吩并[3,4-b]噻吩。 然后在2,3-二氟噻吩并[3,4-b]噻吩中发生溴化步骤，生成4,6-二溴-2,3-二氟噻吩并[2,3-c]噻吩。 然后将4,6-二溴-2,3-二氟噻吩并[2,3-c]噻吩脱溴并聚合成（f + g）≈h的化学计量比，f，g和h不等于0.另外， 在该实施方案中，R 1，R 2，R 3和R 4独立地选自烷基，烷氧基，芳基及其组合，并且其中R 1，R 2，R 3和R 4的组合不完全相同。

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