Method for Analysis of Residual Lithium Compounds in Positive Electrode Active Material

    公开(公告)号:US20240151697A1

    公开(公告)日:2024-05-09

    申请号:US18284354

    申请日:2022-11-15

    申请人: LG Chem, Ltd.

    IPC分类号: G01N31/12 G01N31/16 H01M10/42

    摘要: A method for analysis of residual lithium compounds in a positive electrode active material for a lithium secondary battery comprises the steps of: analyzing a sample of a positive electrode active material using an oxygen/nitrogen/hydrogen analyzer (ONH analyzer) and a Karl Fischer analyzer to determine the amount of the H component; analyzing the sample using a carbon/sulfur analyzer (CS analyzer) to determine the amount of the C component and the S component; analyzing the sample using an inductively coupled plasma optical emission spectrometer (ICP-OES) to determine the amount of the Li component; and calculating the amount of each of LiOH, Li2CO3, and Li2SO4 in the sample using the quantification results of the H, C, and S components, and calculating the amount of Li2O in the sample using the quantification result of the Li component.

    Measuring cell for chemical analyses

    公开(公告)号:US11860144B2

    公开(公告)日:2024-01-02

    申请号:US17464257

    申请日:2021-09-01

    摘要: The present disclosure relates to a measuring cell for carrying out chemical analyses, having a vessel, in which at least one liquid to be analyzed is located; a heating wire, which is guided at least partially around an outer wall of the vessel, so that the liquid inside the vessel can be heated in a uniform and controlled manner; and a first temperature sensor, which determines and/or monitors a first temperature of the liquid. The measuring cell furthermore comprises a magnetic stirrer with a stir bar and a cover for closing the vessel, wherein the cover has a plurality of ducts, wherein at least one first duct is provided for at least one first analysis sensor, which determines and/or monitors at least one chemical and/or physical variable of the liquid of the vessel and wherein at least one second duct is provided for a liquid line.

    Methods for colorimetric endpoint detection and multiple analyte titration systems

    公开(公告)号:US11454619B2

    公开(公告)日:2022-09-27

    申请号:US16378714

    申请日:2019-04-09

    申请人: Ecolab USA Inc.

    IPC分类号: G01N31/16 G01N21/79 G01N21/75

    摘要: Systems for quantifying one or more target analyte concentrations in a process solution are provided and can be used, for example, in methods for quantifying a target analyte concentration. These systems and methods include continuous and batchwise automated titration methods that use titration chemistries to measure the target analyte concentration in the process solution using a multiwavelength detector. The methods provide for efficient and robust automated titration methods for a variety of target analytes and can include methods that analyze more than one analyte and that provide for a dynamic range for measurement of more than one target analyte concentration.

    Analysis of silver ion and complexing agent in tin-silver electrodeposition solution

    公开(公告)号:US10920336B2

    公开(公告)日:2021-02-16

    申请号:US16519973

    申请日:2019-07-23

    摘要: The present disclosure relates to methods of monitoring the concentrations of silver ion and complexing agent in tin-silver (SnAg) electrodeposition solutions, and analysis and process control using such methods. Methods can include adding a precipitating agent to an electrodeposition solution including at least tin ions, silver ions, and complexing agent to cause a reaction between at least a portion of the precipitating agent and substantially all of the silver ions (to precipitate silver ions as a precipitant); adding a metallic salt to the electrodeposition solution to cause a reaction with substantially all of the remaining precipitating agent; measuring the endpoint of the silver ion back titration; further adding metallic salt to cause a further reaction with the complexing agent; and measuring the endpoint of the complexing agent titration.

    Real-Time Monitor And Control Of Active Clay In Water-Based Drilling Fluids

    公开(公告)号:US20200378252A1

    公开(公告)日:2020-12-03

    申请号:US16613786

    申请日:2018-12-27

    摘要: Systems and methods for this disclosure describe systems and methods that are directed to monitoring active clay in water-based drilling fluid may be provided. A method for monitoring active clay concentration while drilling may be provided. The method may include providing a sample of water-based drilling fluid. The method may further include adding methylene blue to the sample in a methylene blue titration. The method may further include performing an impedance measurement on the sample during the methylene blue titration. The method may further include determining an endpoint of the methylene blue titration using a phase angle measurement from the impedance measurement. The method may further include correlating the endpoint to the active clay concentration of the sample. The method may further include determining a treatment for the water-based drilling fluid based on the active clay concentration.

    Oven insulation arrangement
    7.
    发明授权

    公开(公告)号:US10809238B2

    公开(公告)日:2020-10-20

    申请号:US16059520

    申请日:2018-08-09

    发明人: Christian Forrer

    摘要: An analytical device has an oven arrangement (1) with an oven (2), an insulation system, a ventilation system and a housing. The ventilation system has a first convection system that uses natural convection, arranged to keep the housing cool, as well as a second convection system that uses forced convection, arranged to reduce the temperature in the oven (2). In particular, the analytical device is a component of a Karl Fischer titration instrument.

    ADAPTIVE RANGE TITRATION SYSTEMS AND METHODS

    公开(公告)号:US20190317063A1

    公开(公告)日:2019-10-17

    申请号:US16385588

    申请日:2019-04-16

    申请人: Ecolab USA Inc.

    IPC分类号: G01N31/16 G01N35/00

    摘要: Systems for quantifying a target analyte concentration in a process solution are provided and can be used, for example, in methods for quantifying a target analyte concentration. These systems and methods include continuous automated titration methods that use titration chemistries to measure the target analyte concentration in the process solution. The method steps provide for efficient and robust automated titration methods for a variety of target analytes and can include methods that provide for methods that provide a dynamic range for measurement of target analyte concentrations.