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    Polymerization of olefins
    4.
    发明授权
    Polymerization of olefins 有权
    烯烃聚合

    公开(公告)号：US06444763B1

    公开(公告)日：2002-09-03

    申请号：US09517457

    申请日：2000-03-02

    Applicant: Takehiro Sagae ,  Yumito Uehara

    Inventor： Takehiro Sagae ,  Yumito Uehara

    IPC: C08F402

    CPC classification number: B01J31/14 ,  B01J21/16 ,  B01J31/143 ,  B01J31/1616 ,  B01J31/2295 ,  B01J2531/30 ,  B01J2531/40 ,  B01J2531/46 ,  B01J2531/48 ,  B01J2531/49 ,  B01J2531/50 ,  B01J2531/60 ,  B01J2540/22 ,  C08F4/025 ,  C08F4/65912 ,  C08F10/00 ,  C08F110/02 ,  C08F210/16 ,  Y10S526/943 ,  C08F4/65916 ,  C08F2500/18 ,  C08F2500/24 ,  C08F210/08 ,  C08F2500/12 ,  C08F210/14

    Abstract: A particulate phyllosilicate mixture comprising a mixture containing a phyllosilicte belonging to the smectite group and a phyllosilicate belonging to the mica group, the phyllosilicate particle having a content of the phyllosilicate belonging to the smectite group of 0.1 to 50% by weight and optionally satisfying the following requirements (a) to (c): (a): the average particle diameter is 20 to 1000 &mgr;m with not more than 20% of the total number of particles being accounted for by particles having a particle diameter of not more than 10 &mgr;m; (b): the crushing strength of the particle is not less than 0.5 MPa as measured with a microcompression tester and (c): the bulk density of the particle of not less than 0.6 g/cm3. Polymerization of olefins with catalyst comprising the particulate phyllosilicate mixture as a carrier or support for the catalysts is also disclosed

    Abstract translation: 一种颗粒状页硅酸盐混合物，其包含含有属于蒙脱石组的页硅酸盐和属于云母族的页硅酸盐的混合物，具有属于蒙皂石组的页硅酸盐含量为0.1-50重量％的页硅酸盐颗粒，并且任选地满足以下 要求（a）〜（c）:( a）平均粒径为20〜1000μm，不超过粒径为10μm以下的颗粒占总粒数的20％以下; （b）：使用微压缩试验机测定，颗粒的抗碎强度不小于0.5MPa，（c）颗粒的堆积密度不小于0.6g / cm 3。烯烃与包含颗粒的催化剂的聚合 还公开了页硅酸盐混合物作为催化剂的载体或载体

    Catalysts for polyethylene production and use thereof
    5.
    发明授权
    Catalysts for polyethylene production and use thereof 有权
    用于聚乙烯生产和使用的催化剂

    公开(公告)号：US06300272B1

    公开(公告)日：2001-10-09

    申请号：US09325924

    申请日：1999-06-04

    Applicant: Philippe Bodart

    Inventor： Philippe Bodart

    IPC: C08F402

    CPC classification number: C08F10/02 ,  C08F110/02 ,  C08F210/16 ,  C08F4/025 ,  C08F4/24 ,  C08F2500/12 ,  C08F210/14 ,  C08F2500/07 ,  C08F2500/04

    Abstract: A process for producing a chromium-based catalyst for the production of polyethylene, the process comprising providing a silica support having a surface area of at least 380 m2/g and a pore volume of at least 1.5 ml/g; impregnating the silica support with a liquid including a source of aluminum ions and a source of phosphate ions; neutralizing the resultant impregnated support with a neutralizing agent to provide a pH greater than 7 for the resultant neutralized support whereby aluminum phosphate forms in pores of the silica support; and, at any stage in the method, impregnating the silica support with a chromium component.

    Abstract translation: 一种制备用于生产聚乙烯的铬基催化剂的方法，该方法包括提供表面积至少为380m 2 / g，孔体积至少为1.5ml / g的二氧化硅载体; 用包含铝离子源和磷酸根离子源的液体浸渍二氧化硅载体; 用中和剂中和所得浸渍的载体以提供所得中和载体的pH大于7，由此在二氧化硅载体的孔中形成磷酸铝; 并且在该方法的任何阶段，用铬组分浸渍二氧化硅载体。

    Supported polymerisation catalyst
    7.
    发明授权
    Supported polymerisation catalyst 失效
    负载型聚合催化剂

    公开(公告)号：US06664350B1

    公开(公告)日：2003-12-16

    申请号：US09555145

    申请日：2000-08-14

    Applicant: David M. Haddleton ,  Arnaud Radigue ,  Dax Kukulj ,  David Duncalf

    Inventor： David M. Haddleton ,  Arnaud Radigue ,  Dax Kukulj ,  David Duncalf

    IPC: C08F402

    CPC classification number: C08F4/02 ,  C08F4/26 ,  Y10S526/904

    Abstract: The invention relates to supported ligands and catalysts for use in the polymerization of olefinically unsaturated monomers such as vinylic monomers, comprising the use of a compound attached to support, the compound being capable of complexing with a transitional metal. Preferably the compound capable of complexing with a transition metal is a diimine such as a 1,4-diaza-1,3-butadiene, a 2-pyridinecarbaldehyde imine, an oxazolidone or a quinoline carbaldeyde. Preferably the catalysts are used in conjunction with an initiator comprising a homolytically cleavable bond with a halogen atom. The application also discloses processes for attaching ligands to supports, and processes for using the catalysts disclosed in the application.

    Abstract translation: 本发明涉及用于聚合烯属不饱和单体如乙烯基单体的载体配体和催化剂，其包括使用连接于载体上的化合物，该化合物能够与过渡金属络合。 优选地，能够与过渡金属络合的化合物是二亚胺，例如1,4-二氮杂-1,3-丁二烯，2-吡啶甲醛亚胺，恶唑烷酮或喹啉碳链。 优选地，催化剂与包含与卤素原子的均可切割键的引发剂结合使用。 本申请还公开了将配体连接到载体上的方法，以及使用本申请中公开的催化剂的方法。

    Olefin polymerization process using fatty amine additives and boron-modified supported catalyst
    8.
    发明授权
    Olefin polymerization process using fatty amine additives and boron-modified supported catalyst 失效
    使用脂肪胺添加剂和硼改性负载催化剂的烯烃聚合方法

    公开(公告)号：US06476165B1

    公开(公告)日：2002-11-05

    申请号：US09521166

    申请日：2000-03-08

    Applicant: Shaotian Wang

    Inventor： Shaotian Wang

    IPC: C08F402

    CPC classification number: C08F210/16 ,  C08F4/65908 ,  C08F4/65916 ,  C08F4/6592 ,  C08F10/02 ,  C08F110/02 ,  Y10S526/904 ,  C08F2/14 ,  C08F4/6495 ,  C08F4/65912 ,  C08F210/14

    Abstract: An olefin polymerization process is described. The process comprises polymerizing an olefin in the presence of a support, a single-site catalyst, an optional activator, and a fatty amine. The support is chemically treated with an organoboron compound. The single-site catalyst contains a polymerization-stable, heteroatomic ligand. The fatty amine is added directly to the reactor. The combination of pre-treating the support with an organoboron compound and the addition of fatty amine to the process unexpectedly increases catalyst activity.

    Abstract translation: 描述烯烃聚合方法。 该方法包括在载体，单中心催化剂，任选的活化剂和脂肪胺的存在下聚合烯烃。 载体用有机硼化合物进行化学处理。 单中心催化剂含有聚合稳定的杂原子配位体。 将脂肪胺直接加入到反应器中。 将载体与有机硼化合物预处理和向该方法中加入脂肪胺的组合意外地增加了催化剂活性。

    Preparation of polymers of alkenes by suspension polymerization
    10.
    发明授权
    Preparation of polymers of alkenes by suspension polymerization 失效
    通过悬浮聚合制备烯烃聚合物

    公开(公告)号：US06326444B2

    公开(公告)日：2001-12-04

    申请号：US09117657

    申请日：1998-08-04

    Applicant: John Lynch ,  David Fischer ,  Hans-Helmut Görtz ,  Günther Schweier

    Inventor： John Lynch ,  David Fischer ,  Hans-Helmut Görtz ,  Günther Schweier

    IPC: C08F402

    CPC classification number: C08F10/00 ,  C08F4/65908 ,  C08F4/65912 ,  C08F4/65916 ,  C08F4/65922 ,  C08F110/02 ,  Y10S526/943 ,  C08F2/14 ,  C08F2500/17

    Abstract: Polymers of alkenes are prepared by suspension polymerization in the presence of catalyst systems by a process in which the catalyst systems used are supported catalyst systems obtainable by A) reaction of an inorganic carrier with a metal compound of the general formula I M1(R1)r(R2)s(R3 )t(R4 )u  I where M1 is an alkali metal, an alkaline earth metal or a metal of main group III or IV of the Periodic Table, R1 to R7 are variously halogen, alkoxy, dialkylamino, hydrogen, C1-C10-alkyl, C6-C15-aryl, alkylaryl or arylalkyl each having 1 to 10 carbon atoms in the alkyl radical and 6 to 20 carbon atoms in the aryl radical, r, s, t and u are integers from 1 to 4 the sum r+s+t+u corresponding to the valency of M1, B) reaction of the material obtained according to A) with a metallocene complex in its metal dihalide form and a compound forming metallocenium ions and C) subsequent reaction with a metal compound of the general formula II M2(R5)o(R6)p(R7)q  II.

    Abstract translation: 烯烃的聚合物通过在催化剂体系存在下通过悬浮聚合制备，其中使用的催化剂体系是负载的催化剂体系可通过以下方法获得：A）无机载体与通式I的金属化合物的反应，其中M 1是碱金属， 碱土金属或元素周期表主要III或IV族金属，R 1至R 7各自为卤素，烷氧基，二烷基氨基，氢，C 1 -C 10 - 烷基，C 6 -C 15 - 芳基，烷基芳基或芳烷基，各自具有1至10个 烷基中的碳原子和芳基中的6至20个碳原子，r，s，t和u是1至4的整数，对应于M1的化合价的和r + s + t + u，B）反应 根据A）获得的材料与金属二卤化物形式的茂金属络合物和形成金属茂离子的化合物，C）随后与通式II的金属化合物反应

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