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    Process for producing carbonyl sulfide
    1.
    发明授权
    Process for producing carbonyl sulfide 有权
    生产硫化羰的方法

    公开(公告)号：US09115000B2

    公开(公告)日：2015-08-25

    申请号：US14112477

    申请日：2012-04-13

    申请人： Hiromoto Ohno ,  Hidejiro Yokoo ,  Shiho Irie

    发明人： Hiromoto Ohno ,  Hidejiro Yokoo ,  Shiho Irie

    IPC分类号： C01B31/26

    CPC分类号： C01B31/26 ,  B01J31/0239 ,  B01J31/0247 ,  B01J31/0251 ,  B01J31/0265 ,  C01B32/70

    摘要： An efficient process is provided in which sulfur is reacted with carbon monoxide in a liquid phase to produce carbonyl sulfide. In the presence of a base catalyst, carbon monoxide is continuously introduced into a reactor in which a liquid reaction mixture obtained by dissolving or suspending sulfur in an organic solvent is held, and the sulfur is reacted with the carbon monoxide at a pressure of 0.2-3.0 MPa and a temperature of 40-120° C. to yield carbonyl sulfide. The gaseous-phase part is withdrawn from the reactor, and the withdrawn gaseous-phase part is cooled with a cooler to condense the carbonyl sulfide contained in the gaseous-phase part. The condensed carbonyl sulfide is continuously withdrawn, and the gas that has not been condensed with the cooler is returned to the reactor. Thus, carbonyl sulfide is continuously produced.

    摘要翻译： 提供了一种有效的方法，其中硫与液相中的一氧化碳反应以产生羰基硫化物。 在碱催化剂的存在下，将一氧化碳连续引入反应器，其中通过将硫溶解或悬浮在有机溶剂中而获得的液体反应混合物保持在其中，硫与一氧化碳在0.2- 3.0MPa，温度为40-120℃，得到羰基硫化物。 将气相部分从反应器中取出，并将抽出的气相部分用冷却器冷却以冷凝气相部分中所含的羰基硫化物。 连续抽出冷凝的硫化羰，并且未与冷却器冷凝的气体返回反应器。 因此，连续生产硫化羰。

    LIGANDS AND CATALYST SYSTEMS THEREOF FOR THE CATALYTIC OLIGOMERIZATION OF OLEFINIC MONOMERS
    4.
    发明申请
    LIGANDS AND CATALYST SYSTEMS THEREOF FOR THE CATALYTIC OLIGOMERIZATION OF OLEFINIC MONOMERS 审中-公开
    烯烃单体催化低级化合物的配体和催化剂体系

    公开(公告)号：US20100311932A1

    公开(公告)日：2010-12-09

    申请号：US12859337

    申请日：2010-08-19

    申请人： Eric Johannes Maria DE BOER ,  Harry Van Der Heijden ,  Quoc An On ,  Johan Paul Smit ,  Arie Van Zon

    发明人： Eric Johannes Maria DE BOER ,  Harry Van Der Heijden ,  Quoc An On ,  Johan Paul Smit ,  Arie Van Zon

    IPC分类号： C08F4/22 ,  C07F9/08 ,  B01J31/12

    CPC分类号： C07C2/34 ,  B01J31/0265 ,  B01J31/189 ,  B01J2231/14 ,  B01J2231/20 ,  B01J2531/62 ,  B01J2531/64 ,  B01J2531/66 ,  C07F9/5355 ,  C07F9/6571 ,  C07F9/657154 ,  C07F11/005 ,  C08F110/02

    摘要： The present invention relates to a ligand and its use in a catalyst for the oligomerization of olefinic monomers, the ligand having the general formula (VI); (R9)(R10)P—N(R3)—P(R4)  (VI) wherein: the R9 and R10 groups are independently selected from optionally substituted alkyl or heteroalkyl groups; the R3 group is selected from hydrogen, a hydrocarbyl group, a substituted hydrocarbyl group, a heterohydrocarbyl group, a substituted heterohydrocarbyl group, a silyl group or derivative thereof; the R4 group is an optionally substituted alkylenedioxy, alkylenedimercapto or alkylenediamino structure which is bound to the phosphorus atom through the two oxygen, sulphur or nitrogen atoms of the alkylenedioxy, alkylenedimercapto or alkylenediamino structure or an optionally substituted arylenedioxy, arylenedimercapto or arylenediamino structure which is bound to the phosphorus atom through the two oxygen, sulphur or nitrogen atoms of the arylenedioxy, arylenedimercapto or arylenediamino structure.

    摘要翻译： 本发明涉及一种配体及其在烯烃单体低聚催化剂中的应用，具有通式（VI）的配体; （R 9）（R 10）P-N（R 3）-P（R 4）（VI）其中：R 9和R 10基团独立地选自任选取代的烷基或杂烷基; R 3基团选自氢，烃基，取代的烃基，杂烃基，取代的杂烃基，甲硅烷基或其衍生物; R 4基团是任选取代的亚烷基二氧基，亚烷基二巯基或亚烷基二氨基结构，其通过亚烷基二氧基，亚烷基二巯基或亚烷基二氨基结构的两个氧，硫或氮原子或与被结合的任选取代的亚芳基二氧基，亚芳基二巯基或亚芳基二氨基结构与磷原子结合 通过亚芳基二氧基，亚芳基二巯基或亚芳基二氨基结构的两个氧，硫或氮原子到磷原子。

    Phoshazenium salt phase transfer catalysts
    6.
    发明申请
    Phoshazenium salt phase transfer catalysts 失效
    磷酸盐相转移催化剂

    公开(公告)号：US20070112223A1

    公开(公告)日：2007-05-17

    申请号：US11651167

    申请日：2007-01-09

    申请人： Daniel Brunelle

    发明人： Daniel Brunelle

    IPC分类号： C07C43/20 ,  C07D209/02

    CPC分类号： B01J31/0239 ,  B01J31/0265 ,  B01J31/0268 ,  B01J2231/14 ,  B01J2231/40 ,  B01J2531/98 ,  C07C41/16 ,  C07C315/04 ,  C07F9/067 ,  C08G65/4087 ,  C08G79/025 ,  C07C317/22 ,  C07C43/29

    摘要： A method for carrying out a chemical reaction between at least two reactants occupying separate phases within a multiphase reaction mixture has been discovered in which at least one phosphazenium salt is employed as a phase transfer catalyst. The remarkable utility of phosphazenium salts as phase transfer catalysts is illustrated by the preparation of aromatic ethers. The phosphazenium salt phase transfer catalysts are shown to be especially useful in the preparation of aromatic polyethers such as polyether sulfones.

    摘要翻译： 已经发现在多相反应混合物中在至少两种占据分离相的反应物之间进行化学反应的方法，其中使用至少一种磷氮烯基鏻盐作为相转移催化剂。 通过制备芳族醚来说明磷氮烯基鏻盐作为相转移催化剂的显着效用。 显示磷氮烯基鏻盐相转移催化剂特别可用于制备芳族聚醚如聚醚砜。

    Phosphazenium salt phase transfer catalysts
    7.
    发明申请
    Phosphazenium salt phase transfer catalysts 审中-公开
    磷腈鎓盐相转移催化剂

    公开(公告)号：US20060069291A1

    公开(公告)日：2006-03-30

    申请号：US10950874

    申请日：2004-09-24

    申请人： Daniel Brunelle

    发明人： Daniel Brunelle

    IPC分类号： C07C43/02 ,  C07C43/20

    CPC分类号： B01J31/0239 ,  B01J31/0265 ,  B01J31/0268 ,  B01J2231/14 ,  B01J2231/40 ,  B01J2531/98 ,  C07C41/16 ,  C07C315/04 ,  C07F9/067 ,  C08G65/4087 ,  C08G79/025 ,  C07C317/22 ,  C07C43/29

    摘要： A method for carrying out a chemical reaction between at least two reactants occupying separate phases within a multiphase reaction mixture has been discovered in which at least one phosphazenium salt is employed as a phase transfer catalyst. The remarkable utility of phosphazenium salts as phase transfer catalysts is illustrated by the preparation of aromatic ethers. The phosphazenium salt phase transfer catalysts are shown to be especially useful in the preparation of aromatic polyethers such as polyether sulfones.

    摘要翻译： 已经发现在多相反应混合物中在至少两种占据分离相的反应物之间进行化学反应的方法，其中使用至少一种磷氮烯基鏻盐作为相转移催化剂。 通过制备芳族醚来说明磷氮烯基鏻盐作为相转移催化剂的显着用途。 显示磷氮烯基鏻盐相转移催化剂特别可用于制备芳族聚醚如聚醚砜。