Trace detector and analytical method for trace detector
    1.
    发明授权
    Trace detector and analytical method for trace detector 有权
    痕量检测器和痕量探测器的分析方法

    公开(公告)号:US08309918B2

    公开(公告)日:2012-11-13

    申请号:US12747243

    申请日:2009-12-30

    CPC classification number: G01N27/62 G01N1/2202 G01N1/40

    Abstract: A trace detector is disclosed. The trace detector comprises: a desorption chamber defining a desorption region, and the desorption chamber has a housing. The housing has a sample feeding port for introducing a substance to be detected into the desorption chamber and a gas discharge port for discharging gas entraining the sample from the desorption chamber. A controller is used for controlling the trace detector in such a manner that the sample feeding port and the gas discharge port are in fluid communication with the desorption chamber during pre-concentration process of the trace detector, thereby continuously feeding and collecting the sample. With the above manner, data collecting, processing and analyzing processes may be performed by the trace detector throughout the sample feeding process and the gas pre-concentrating process. The trace detector has an excellent detecting period of time whether the substance to be detected in the gas is in a high concentration state or a low concentration state, and the trace detector can perform continuous sampling for a long time, thereby improving a ratio of the amount of trapped substance to the amount of the substance entrained in the gas to be detected and the amount of the cumulated trapped substance, decreasing the probability of failing to detect the substance, and increasing detection sensitivity. In addition, the detection efficiency of the detector is increased during the gas pre-concentration process.

    Abstract translation: 公开了一种跟踪检测器。 痕量检测器包括:解吸室,其限定解吸区域,并且解吸室具有壳体。 壳体具有用于将待检测物质引入解吸室的样品供给口和用于排出从解吸室夹带样品的气体的气体排出口。 控制器用于控制跟踪检测器,使得样品供给口和排气口在迹线检测器的预浓缩过程期间与解吸室流体连通,从而连续地进料和收集样品。 通过上述方式,数据收集,处理和分析过程可以在整个采样过程和气体预浓缩过程中由迹线检测器执行。 痕量检测器在气体中被检测物质是处于高浓度状态还是低浓度状态下具有优异的检测时间段,并且痕量检测器可以长时间进行连续取样,从而提高 捕获的物质的量与被检测气体中夹带的物质的量和累积的捕获物质的量的量,降低检测不到物质的可能性,并提高检测灵敏度。 此外,在气体预浓缩过程中检测器的检测效率增加。

    DOPANT GAS GENERATING DEVICE
    2.
    发明申请
    DOPANT GAS GENERATING DEVICE 有权
    氘代气体发生装置

    公开(公告)号:US20110114210A1

    公开(公告)日:2011-05-19

    申请号:US12743926

    申请日:2009-12-30

    Abstract: The present invention relates to a dopant gas generating device for supplying the dopant gas to the ion mobility spectrometry instrument, comprising: a doping container; an air inlet having an inlet end connecting with an upstream side of a carrier gas passage and an outlet end connecting with the doping container; an air outlet having an entrance end connecting with the doping container and an exit end connecting with an downstream side of the carrier gas passage; a dopant gas generating unit for releasing the dopant gas, wherein the dopant gas generating unit is disposed within the doping container. Through disposing the dopant gas generating unit, which is used for releasing the dopant gas, within the doping container, the dopant gas in the present invention is applicable with not only a solid state dopant, but also a liquid state dopant.

    Abstract translation: 本发明涉及一种用于将掺杂剂气体供给到离子迁移率光谱仪器的掺杂剂气体产生装置,包括:掺杂容器; 空气入口,其具有与载气通道的上游侧连接的入口端和与所述掺杂容器连接的出口端; 具有与所述掺杂容器连接的入口端的出气口和与所述载气通道的下游侧连接的出口端; 用于释放掺杂气体的掺杂剂气体发生单元,其中所述掺杂剂气体发生单元设置在所述掺杂容器内。 通过在掺杂容器内设置用于释放掺杂剂气体的掺杂剂气体发生单元,本发明中的掺杂气体不仅可以应用于固态掺杂剂,而且也可应用于液态掺杂剂。

    Electrode structure for drift tube in ion mobility spectrometer
    3.
    发明授权
    Electrode structure for drift tube in ion mobility spectrometer 有权
    离子迁移谱仪中漂移管的电极结构

    公开(公告)号:US07851747B2

    公开(公告)日:2010-12-14

    申请号:US12455029

    申请日:2009-05-27

    CPC classification number: G01N27/622

    Abstract: Disclosed is an electrode structure for a drift tube in IMS comprising a ring electrode, for each of two surfaces of the ring electrode, at least a part adjacent to the inner radius is formed into a cone, and the angles formed between the cones and the axis of the ring electrode are different from each other. The electrode structure of the present invention can alleviate, even eliminate, the accumulation of space charges in the drift tube. Such structure is particularly suitable when the electric field in the drift tube is low in strength or a great number of ions pass through. Meanwhile, the structure allows a significant decrease in the size of the outer radius of the electrode, while the inner radius remains constant. In this way, it is possible to effectively reduce the outline size of the drift tube and thus make the IMS compact.

    Abstract translation: 公开了一种用于IMS中的漂移管的电极结构,包括环形电极,对于环形电极的两个表面中的每一个,至少与内半径相邻的部分形成为锥体,并且在锥体和 环电极的轴线彼此不同。 本发明的电极结构可以减轻甚至消除漂移管中空间电荷的累积。 当漂移管中的电场强度低或大量离子通过时,这种结构特别合适。 同时,结构允许电极的外半径的大小显着减小,而内半径保持恒定。 以这种方式,可以有效地减小漂移管的轮廓尺寸,从而使得IMS紧凑。

    Sampling component, sampling device and ion mobility spectrometer
    4.
    发明授权
    Sampling component, sampling device and ion mobility spectrometer 有权
    采样部件,取样装置和离子迁移谱仪

    公开(公告)号:US08528425B2

    公开(公告)日:2013-09-10

    申请号:US12737341

    申请日:2010-12-01

    CPC classification number: G01N27/622 G01N1/4022

    Abstract: A sampling component including a sampling body that can be electrically heated and an outer surface of which has a wiping sampling area to receive a sample; and an insulated handle that is connected to one longitudinal end of the sampling body. The sampling component contacts directly electrical contacts of an external power supply after being positioned in a analysis chamber, the power supply is turned on to vaporize the sample, and the power is turned off immediately after the sampling component removed from the chamber. The power consumption and a malfunction caused by long-term use of the sampling device under a high temperature can be avoided. A sampling device having the sampling component and an ion mobility spectrometer having the sampling device are also provided.

    Abstract translation: 一种采样部件,包括可被电加热并且其外表面具有用于接收样品的擦拭采样区域的采样体; 以及连接到采样体的一个纵向端的绝缘手柄。 采样部件定位在分析室中后,直接与外部电源的电接点接触,电源接通以使样品汽化,并且在从腔室中取出取样部件后立即关闭电源。 功耗降低,并且可以避免在高温下长期使用取样装置引起的故障。 还提供了具有取样分量的采样装置和具有采样装置的离子迁移谱仪。

    Ion gate for dual ion mobility spectrometer and method thereof
    5.
    发明授权
    Ion gate for dual ion mobility spectrometer and method thereof 有权
    双离子迁移谱仪的离子门及其方法

    公开(公告)号:US08013297B2

    公开(公告)日:2011-09-06

    申请号:US12579719

    申请日:2009-10-15

    CPC classification number: H01J3/04 H01J49/004 H01J49/061

    Abstract: Disclosed is an ion gate for a dual IMS and method. The ion gate includes an ion source, a first gate electrode placed on one side of the ion source, a second gate electrode placed on the other side of the ion source, a third gate electrode placed on the side of the first gate electrode away from the ion source, a fourth gate electrode placed on the side of the second gate electrode away from the ion source, wherein during the ion storage, the potential at the position on the tube axis of the ion gate corresponding to the first gate electrode is different from the potentials at the positions on the tube axis corresponding to the ion source and the third gate electrode, and the potential at the position on the tube axis corresponding to the second gate electrode is different from the potentials at the positions on the tube axis corresponding to the ion source and the fourth gate electrode. According to the present invention, after sample gas enters the ion gates, charge exchange with reaction ions occurs between the first gate electrode and the second electrode, and positive and negative ions are continuously stored into the storage regions for the positive and negative ions. This leads to an improvement of utility rate of ions. Then, the ions are educed in a step-wise manner from the storage regions for the positive and negative ions by a simple control of a combination of the electrodes.

    Abstract translation: 公开了一种用于双重IMS和方法的离子门。 离子浇口包括离子源,位于离子源一侧的第一栅电极,位于离子源另一侧的第二栅电极,位于第一栅电极侧的第三栅电极, 离子源,第四栅极放置在远离离子源的第二栅电极侧,其中在离子存储期间,对应于第一栅电极的离子门的管轴上的位置的电位不同 从对应于离子源和第三栅电极的管轴上的位置的电位和对应于第二栅电极的管轴上的位置的电位与管轴对应的位置的电位不同 到离子源和第四栅电极。 根据本发明,在样品气体进入离子浇口之后,在第一栅电极和第二电极之间产生与反应离子的电荷交换,正离子和负离子被连续地存储在正离子和负离子的存储区中。 这导致了离子的利用率的提高。 然后,通过简单地控制电极的组合,从正离子和负离子的存储区域逐步地排出离子。

    Gas filtering-buffering device
    6.
    发明授权
    Gas filtering-buffering device 有权
    气体过滤缓冲装置

    公开(公告)号:US07815721B2

    公开(公告)日:2010-10-19

    申请号:US11964384

    申请日:2007-12-26

    Abstract: The present invention relates to a gas filtering-buffering device, which comprises at least one gas filtering unit; a gas inlet, the gas to be processed flows into the at least one gas filtering unit from the gas inlet; and a gas outlet, the gas processed by the at least one gas filtering unit is discharged out of the at least one gas filtering unit via the gas outlet, wherein the at least one gas filtering unit comprising: a gas buffering cavity for performing buffering function for the gas, and a gas filtering part for performing filtering function for the gas. In the present invention, it is not only provided with a gas filtering part which is able to filter the moisture and organic substance in the gas, but also provided with a gas buffering cavity, which integrate the filtering and buffering functions together. The buffering cavity may expand the capacity and stabilize the pressure of the gas, and balance the concentration, pressure and flow rate of the gas, it is advantageous to reduce the on-way pressure lost and partially pressure lost, decrease fluctuation of the flow current and the pressure thus, the detecting performance of the detector is improved.

    Abstract translation: 本发明涉及一种气体过滤缓冲装置,其包括至少一个气体过滤单元; 气体入口,待处理气体从气体入口流入至少一个气体过滤单元; 和气体出口,由所述至少一个气体过滤单元处理的气体经由所述气体出口排出所述至少一个气体过滤单元,其中所述至少一个气体过滤单元包括:气体缓冲腔,用于执行缓冲功能 用于气体,以及用于对气体进行过滤功能的气体过滤部。 在本发明中,不仅设置能够对气体中的水分和有机物质进行过滤的气体过滤部,还设置有将过滤和缓冲功能集成在一起的气体缓冲腔。 缓冲腔可以扩大容量并稳定气体的压力,平衡气体的浓度,压力和流量,有利于减少接通压力损失和部分压力损失,减少流量的波动 从而提高了检测器的检测性能。

    Gas Filtering-Buffering Device
    7.
    发明申请
    Gas Filtering-Buffering Device 有权
    气体过滤缓冲装置

    公开(公告)号:US20080155946A1

    公开(公告)日:2008-07-03

    申请号:US11964384

    申请日:2007-12-26

    Abstract: The present invention relates to a gas filtering-buffering device, which comprises at least one gas filtering unit; a gas inlet, the gas to be processed flows into the at least one gas filtering unit from the gas inlet; and a gas outlet, the gas processed by the at least one gas filtering unit is discharged out of the at least one gas filtering unit via the gas outlet, wherein the at least one gas filtering unit comprising: a gas buffering cavity for performing buffering function for the gas, and a gas filtering part for performing filtering function for the gas. In the present invention, it is not only provided with a gas filtering part which is able to filter the moisture and organic substance in the gas, but also provided with a gas buffering cavity, which integrate the filtering and buffering functions together. The buffering cavity may expand the capacity and stabilize the pressure of the gas, and balance the concentration, pressure and flow rate of the gas, it is advantageous to reduce the on-way pressure lost and partially pressure lost, decrease fluctuation of the flow current and the pressure thus, the detecting performance of the detector is improved.

    Abstract translation: 本发明涉及一种气体过滤缓冲装置,其包括至少一个气体过滤单元; 气体入口,待处理气体从气体入口流入至少一个气体过滤单元; 和气体出口,由所述至少一个气体过滤单元处理的气体经由所述气体出口排出所述至少一个气体过滤单元,其中所述至少一个气体过滤单元包括:用于执行缓冲功能的气体缓冲腔 用于气体,以及用于对气体进行过滤功能的气体过滤部。 在本发明中,不仅设置能够对气体中的水分和有机物质进行过滤的气体过滤部,还设置有将过滤和缓冲功能集成在一起的气体缓冲腔。 缓冲腔可以扩大容量并稳定气体的压力,平衡气体的浓度,压力和流量,有利于减少接通压力损失和部分压力损失,减少流量的波动 从而提高了检测器的检测性能。

    Sampling method and sampling device
    8.
    发明授权
    Sampling method and sampling device 有权
    采样方式及取样装置

    公开(公告)号:US08646340B2

    公开(公告)日:2014-02-11

    申请号:US12746825

    申请日:2009-12-30

    CPC classification number: G01N1/22 G01N1/24 G01N2001/022 G01N2001/028

    Abstract: Disclosed is a sampling method which comprises the steps of: blowing airflow towards a center portion of a sampling surface through a blowing port; and sucking the blown airflow from periphery of the sampling surface through a sucking port, or a sampling method which comprises the steps of: providing a sampling device on a sampling surface, the sampling device being shaped to form a sampling space together with the sampling surface, and the sampling device including a blowing port arranged at the center portion of the sampling device and a sucking port arranged at periphery of the sampling device; blowing airflow towards the sampling surface through the blowing port; and sucking the airflow blown towards the sampling surface through the sucking port so as to collect samples.

    Abstract translation: 公开了一种采样方法,包括以下步骤:通过吹风口朝向采样表面的中心部分吹送气流; 以及通过抽吸口从所述取样表面周边抽吸吹出的气流或采样方法,所述取样方法包括以下步骤:在采样表面上提供取样装置,所述采样装置被成形为与取样表面一起形成取样空间 并且所述取样装置包括布置在所述取样装置的中心部分处的吹出口和布置在所述取样装置的周边的抽吸口; 通过吹气口向采样表面吹送气流; 并且通过吸入口抽吸朝向采样表面吹送的气流以收集样品。

    Dopant gas generating device
    9.
    发明授权
    Dopant gas generating device 有权
    掺杂气体发生装置

    公开(公告)号:US08640727B2

    公开(公告)日:2014-02-04

    申请号:US12743926

    申请日:2009-12-30

    Abstract: The present invention relates to a dopant gas generating device for supplying the dopant gas to the ion mobility spectrometry instrument, comprising: a doping container; an air inlet having an inlet end connecting with an upstream side of a carrier gas passage and an outlet end connecting with the doping container; an air outlet having an entrance end connecting with the doping container and an exit end connecting with an downstream side of the carrier gas passage; a dopant gas generating unit for releasing the dopant gas, wherein the dopant gas generating unit is disposed within the doping container. Through disposing the dopant gas generating unit, which is used for releasing the dopant gas, within the doping container, the dopant gas in the present invention is applicable with not only a solid state dopant, but also a liquid state dopant.

    Abstract translation: 本发明涉及一种用于将掺杂剂气体供给到离子迁移率光谱仪器的掺杂剂气体产生装置,包括:掺杂容器; 空气入口,其具有与载气通道的上游侧连接的入口端和与所述掺杂容器连接的出口端; 具有与所述掺杂容器连接的入口端的出气口和与所述载气通道的下游侧连接的出口端; 用于释放掺杂气体的掺杂剂气体发生单元,其中所述掺杂剂气体发生单元设置在所述掺杂容器内。 通过在掺杂容器内设置用于释放掺杂剂气体的掺杂剂气体发生单元,本发明中的掺杂气体不仅可以应用于固态掺杂剂,而且也可应用于液态掺杂剂。

    Detection Method for an Ion Migration Spectrum and an Ion Migration Spectrometer Using the Same Method
    10.
    发明申请
    Detection Method for an Ion Migration Spectrum and an Ion Migration Spectrometer Using the Same Method 有权
    使用相同方法的离子迁移谱和离子迁移光谱仪的检测方法

    公开(公告)号:US20120326024A1

    公开(公告)日:2012-12-27

    申请号:US13560440

    申请日:2012-07-27

    CPC classification number: G01N27/622

    Abstract: A detection apparatus and method for an ion migration spectrum include acquiring an ion migration spectrum of pure carrier gas and an ion migration spectrum of carrier gas containing a test substance sample and performing differential process on the ion migration spectrum of the pure carrier gas and the ion migration spectrum of the carrier gas containing the test substance sample to acquire a differential spectrum. The value of a characteristic peak of the differential spectrum represents properties of the sample of substances. The method avoids interferences on the migration spectrum from interference sources of the apparatus itself, thereby improving detection sensitivity and accuracy of the ion migration spectrum, and migration spectrum shift caused by variations in the environmental conditions can be found and corrected through the differential process on the migration spectrum of the pure carrier gas, thereby achieving self-stableness and self-correction of the ion migration spectrometer.

    Abstract translation: 用于离子迁移谱的检测装置和方法包括获得纯载体的离子迁移谱和含有测试物质样品的载气的离子迁移谱,并对纯载体和离子的离子迁移谱进行差别过程 含有测试物质样品的载气的迁移谱,以获得差示谱。 差分光谱特征​​峰值代表物质样品的特性。 该方法避免了对设备本身的干扰源的迁移谱的干扰,从而提高了离子迁移谱的检测灵敏度和精度,并且通过差分过程可以发现和纠正由环境条件变化引起的迁移频谱偏移 纯载体的迁移谱,从而实现离子迁移光谱仪的自稳定和自校正。

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