公开(公告)号：US09562328B2

公开(公告)日：2017-02-07

申请号：US14441268

申请日：2013-11-06

Applicant: Stora Enso Oyj

Inventor： Lars Axrup ,  Heidi Saxell ,  Veikko Jokela ,  Henri Kastinen ,  Anna Kauppi ,  Kaj Backfolk ,  Nina Ruohoniemi ,  Risto Laitinen ,  Isto Heiskanen ,  Teija Laukala

IPC: D21H17/67 ,  C08B15/02 ,  D21H11/18 ,  D21H17/64 ,  C08K3/26

CPC classification number: D21H17/675 ,  C08B15/02 ,  C08K3/26 ,  C08K2003/265 ,  C08L2205/16 ,  D21H11/18 ,  D21H17/24 ,  D21H17/64 ,  D21H17/67 ,  C08L1/04

Abstract: A method for the production of a composite material comprising nanofibrillated polysaccharide, the method comprising the following steps: (i) providing a liquid suspension of the nanofibrillated polysaccharide; (ii) bringing said liquid suspension in contact with at least one additive, thereby forming a composite material suspension, wherein the composite comprises the nanofibrillated polysaccharide and the at least one additive, (iii) increasing the solid contents of said composite material suspension, thereby forming a high solid contents composite material suspension.

Abstract translation: 一种制备包含纳米纤维化多糖的复合材料的方法，所述方法包括以下步骤：（i）提供纳米纤维化多糖的液体悬浮液; （ii）使所述液体悬浮液与至少一种添加剂接触，从而形成复合材料悬浮液，其中复合材料包含纳米纤维化多糖和至少一种添加剂，（iii）增加所述复合材料悬浮液的固体含量，从而 形成高固体含量的复合材料悬浮液。

公开(公告)号：US20170107669A1

公开(公告)日：2017-04-20

申请号：US15389482

申请日：2016-12-23

Applicant: Stora Enso Oyj

Inventor： Lars Axrup ,  Heidi Saxell ,  Veikko Jokela ,  Henri Kastinen ,  Anna Kauppi ,  Kaj Backfolk ,  Nina Ruohoniemi ,  Risto Laitinen ,  Isto Heiskanen ,  Teija Laukala

IPC: D21H17/67 ,  C08B15/02 ,  D21H17/24 ,  D21H11/18 ,  D21H17/64

CPC classification number: D21H17/675 ,  C08B15/02 ,  C08K3/26 ,  C08K2003/265 ,  C08L2205/16 ,  D21H11/18 ,  D21H17/24 ,  D21H17/64 ,  D21H17/67 ,  C08L1/04

Abstract: A substantially dry composite material comprising a nanofibrillated polysaccharide and two or more additives, wherein the composite nanofibrillated polysaccharide is a microfibrillated cellulose and wherein the additives are lime milk and carbon dioxide, wherein the additives are allowed to react with each other and forming a precipitated calcium carbonate on the nanofibrillated polysaccharide, thereby forming a composite product comprising precipitated calcium carbonate and nanofibrillated polysaccharide.

公开(公告)号：US20150094464A1

公开(公告)日：2015-04-02

申请号：US14390519

申请日：2013-04-04

Applicant: Stora Enso OYJ

Inventor： Heidi Saxell ,  Isto Heiskanen ,  Lars Axrup ,  Cecilia Land Hensdal ,  Veikko Jokela

IPC: C08B11/12

CPC classification number: C08B11/12 ,  C08B1/08

Abstract: The present invention provides a method for production of cellulose ethers in a high solids process substantially without use of organic solvents as reaction and/or washing medium. In the method of the invention the first alkalization step is carried out by using high solids content cellulose pulp and solid sodium hydroxide. This is followed by an etherification step where the solids content is preferably further increased and the use of solid etherification reactant is preferred. As no organic solvents are used as reaction media the invented method enables production of cellulose ethers directly from never dried pulp with significant savings in energy and investment costs. The method is especially suitable for the production of carboxymethyl cellulose sodium salt (CMC) with low degree of substitution (DS

Abstract translation: 本发明提供了一种基本上不使用有机溶剂作为反应和/或洗涤介质的高固含量方法生产纤维素醚的方法。 在本发明的方法中，通过使用高固含量的纤维素纸浆和固体氢氧化钠来进行第一碱化步骤。 之后是醚化步骤，其中固体含量优选进一步增加，并且优选使用固体醚化反应物。 由于不使用有机溶剂作为反应介质，本发明的方法可以直接从未干燥的纸浆生产纤维素醚，从而显着节省能源和投资成本。 该方法特别适用于低取代度（DS <0.3）的羧甲基纤维素钠盐（CMC）的生产。 所得到的无水或低水溶性羧甲基化纤维素纤维的使用适用于例如用于生产微纤化纤维素。

公开(公告)号：US20150299959A1

公开(公告)日：2015-10-22

申请号：US14441268

申请日：2013-11-06

Applicant: STORA ENSO OYJ

Inventor： Lars Axrup ,  Heidi Saxell ,  Veikko Jokela ,  Henri Kastinen ,  Anna Kauppi ,  Kaj Backfolk ,  Nina Ruohoniemi ,  Risto Laitinen ,  Isto Heiskanen ,  Teija Laukala

IPC: D21H17/67 ,  D21H11/18

CPC classification number: D21H17/675 ,  C08B15/02 ,  C08K3/26 ,  C08K2003/265 ,  C08L2205/16 ,  D21H11/18 ,  D21H17/24 ,  D21H17/64 ,  D21H17/67 ,  C08L1/04

Abstract: A method for the production of a composite material comprising nanofibrillated polysaccharide, the method comprising the following steps: (i) providing a liquid suspension of the nanofibrillated polysaccharide; (ii) bringing said liquid suspension in contact with at least one additive, thereby forming a composite material suspension, wherein the composite comprises the nanofibrillated polysaccharide and the at least one additive, (iii) increasing the solid contents of said composite material suspension, thereby forming a high solid contents composite material suspension.

Abstract translation: 一种制备包含纳米纤维化多糖的复合材料的方法，所述方法包括以下步骤：（i）提供纳米纤维化多糖的液体悬浮液; （ii）使所述液体悬浮液与至少一种添加剂接触，从而形成复合材料悬浮液，其中复合材料包含纳米纤维化多糖和至少一种添加剂，（iii）增加所述复合材料悬浮液的固体含量，从而 形成高固体含量的复合材料悬浮液。

公开(公告)号：US09926668B2

公开(公告)日：2018-03-27

申请号：US15389482

申请日：2016-12-23

Applicant: Stora Enso Oyj

Inventor： Lars Axrup ,  Heidi Saxell ,  Veikko Jokela ,  Henri Kastinen ,  Anna Kauppi ,  Kaj Backfolk ,  Nina Ruohoniemi ,  Risto Laitinen ,  Isto Heiskanen ,  Teija Laukala

IPC: D21H11/18 ,  D21H17/67 ,  C08B15/02 ,  D21H17/64 ,  C08K3/26 ,  D21H17/24

CPC classification number: D21H17/675 ,  C08B15/02 ,  C08K3/26 ,  C08K2003/265 ,  C08L2205/16 ,  D21H11/18 ,  D21H17/24 ,  D21H17/64 ,  D21H17/67 ,  C08L1/04

Abstract: A substantially dry composite material comprising a nanofibrillated polysaccharide and two or more additives, wherein the composite nanofibrillated polysaccharide is a microfibrillated cellulose and wherein the additives are lime milk and carbon dioxide, wherein the additives are allowed to react with each other and forming a precipitated calcium carbonate on the nanofibrillated polysaccharide, thereby forming a composite product comprising precipitated calcium carbonate and nanofibrillated polysaccharide.

公开(公告)号：US20150308017A1

公开(公告)日：2015-10-29

申请号：US14441263

申请日：2013-10-30

Applicant: Stora Enso Oyj

Inventor： Kaj Backfolk ,  Heidi Saxell ,  Isto Heiskanen ,  Lars Axrup ,  Cecilia Land Hensdal ,  Veikko Jokela ,  Esa Saukkonen ,  Ari Kotilainen ,  Henri Kastinen ,  Anna Kauppi

IPC: D01F2/00

CPC classification number: D01F2/00 ,  C08L1/04 ,  D21C9/007 ,  D21C9/06 ,  D21C9/18 ,  D21H11/18 ,  F26B3/36

Abstract: A method for drying nanofibrillated polysaccharide to obtain a substantially dry nanofibrillated polysaccharide product, comprising the following steps: (i) providing an aqueous suspension of nanofibrillated polysaccharide; (ii) increasing the solid content of said suspension, thereby forming a high solid content microfibrillated cellulose suspension; and (iii) drying said high solid content microfibrillated cellulose suspension, through a simultaneous heating and mixing operation.

Abstract translation: 一种干燥纳米纤维化多糖以获得基本干燥的纳米纤维化多糖产物的方法，包括以下步骤：（i）提供纳米纤维化多糖的水性悬浮液; （ii）增加所述悬浮液的固体含量，从而形成高固体含量的微纤化纤维素悬浮液; 和（iii）通过同时加热和混合操作来干燥所述高固含量微纤化纤维素悬浮液。