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1.发明授权Process and installation for the production of an organic solution of a water-insoluble organic base 失效用于生产水不溶性有机碱的有机溶液的方法和安装
公开(公告)号：US4605771A
公开(公告)日：1986-08-12
申请号：US604365
申请日：1984-04-26
申请人： Leon Ninane , Claude Breton , Constant Guerdon
发明人： Leon Ninane , Claude Breton , Constant Guerdon
IPC分类号： C07C209/86 , C01D7/16 , C07C67/00 , C07C209/00 , C07C211/03 , C07C85/26 , C07C87/06
CPC分类号： C01D7/16
摘要： An organic solution (2) of a water-immiscible chloride of an organic cation is mixed with a basic reagent and with water (3) in a reaction chamber (1), the mixture (6) which has reacted is transferred into a phase separation chamber (5) where the organic solution of the base (8) and an aqueous phase (7) containing a solid residue are separated and at least a part of a sludge (9) formed between the organic solution and the aqueous phase which have separated is recycled into the reaction chamber (1).
摘要翻译： 将有机阳离子的水不混溶氯化物的有机溶液（2）与碱性试剂和反应室（1）中的水（3）混合，将已反应的混合物（6）转移到相分离 （8）的有机溶液和含有固体残余物的水相（7）分离的室（5）和形成在有机溶液和水相之间的污泥（9）的至少一部分已经分离 被再循环到反应室（1）中。
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公开(公告)号：US5290322A
公开(公告)日：1994-03-01
申请号：US522605
申请日：1990-04-24
申请人： Claude Breton , Leon Ninane
发明人： Claude Breton , Leon Ninane
摘要： Process for the manufacture of sodium bicarbonate particles having an ovoid or spherical shape, the process preparing an aqueous solution of sodium bicarbonate, which is supersaturated; circulating the aqueous solution supersaturated in sodium bicarbonate through a bed of crystals in order to cause the bed to be a mobile bed in which the crystals are in continuous motion, and to cause crystallization of the sodium bicarbonate particles and at least partial desupersaturation of the aqueous solution supersaturated in sodium bicarbonate to provide a mother liquor and, withdrawing the sodium bicarbonate particles from the bed.
摘要翻译： 用于制造具有卵球形或球形形状的碳酸氢钠颗粒的方法，该方法制备过饱和的碳酸氢钠水溶液; 使在碳酸氢钠中过饱和的水溶液通过晶体床循环，以使床成为移动床，其中晶体连续运动，并引起碳酸氢钠颗粒的结晶和至少部分去饱和的水溶液 溶液在碳酸氢钠中过饱和以提供母液并从床中取出碳酸氢钠颗粒。
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公开(公告)号：US4797981A
公开(公告)日：1989-01-17
申请号：US940220
申请日：1986-12-08
申请人： Leon Ninane , Claude Breton
发明人： Leon Ninane , Claude Breton
CPC分类号： C01D3/22
摘要： Process for the production of salt in which sodium chloride is crystallized in the form of spheres by evaporation of a sodium chloride brine and the spheres obtained are then broken up. The salt produced by the process is particularly suitable for the food industry.
摘要翻译： 生产氯化钠通过蒸发氯化钠盐水并以球体形式结晶的盐的方法然后分解。 该方法生产的盐特别适用于食品工业。
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公开(公告)号：US5154909A
公开(公告)日：1992-10-13
申请号：US637985
申请日：1991-01-02
申请人： Leon Ninane , Claude Breton
发明人： Leon Ninane , Claude Breton
IPC分类号： C01D3/22
CPC分类号： C01D3/22
摘要： Process for the production of salt in which sodium chloride is crystallized in the form of spheres by evaporation of a sodium chloride brine and the spheres obtained are then broken up. The salt produced by the process is particularly suitable for the food industry.
摘要翻译： 生产氯化钠通过蒸发氯化钠盐水并以球体形式结晶的盐的方法然后分解。 该方法生产的盐特别适用于食品工业。
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5.发明授权
公开(公告)号：US4677229A
公开(公告)日：1987-06-30
申请号：US754972
申请日：1985-07-15
申请人： Leon Ninane , Claude Breton
发明人： Leon Ninane , Claude Breton
IPC分类号： C01D7/16 , C07C67/00 , C07C209/00 , C07C209/86 , C07C211/03 , C07C85/26
CPC分类号： C01D7/16
摘要： Process for the production of a water-insoluble nitrogeneous organic base, from an aqueous solution of alkali metal bicarbonate and the base hydrochloride, according to which the solution (11) is treated with a complement of the base hydrochloride (12), and the resultant liquid (18) is treated with a basic agent (30) capable of decomposing the hydrochloride. The invention is applied to the regeneration of the amine in the process for the manufacture of sodium bicarbonate by the amines method.
摘要翻译： 从碱金属碳酸氢盐和碱式盐酸盐的水溶液中制备不溶于水的无机有机碱的方法，根据该方法，用碱式盐酸盐（12）的互补液处理溶液（11），所得的 液体（18）用能够分解盐酸盐的碱性试剂（30）处理。 本发明适用于通过胺法制备碳酸氢钠的方法中胺的再生。
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6.发明授权
公开(公告)号：US5396863A
公开(公告)日：1995-03-14
申请号：US29423
申请日：1993-03-09
申请人： Leon Ninane , Claude Breton
发明人： Leon Ninane , Claude Breton
CPC分类号： C01D7/42 , B01D9/0013 , C01D7/35 , C30B7/00 , Y10T117/10 , Y10T117/1008 , Y10T117/1016 , Y10T117/1024
摘要： Installation for the crystallization of an inorganic substance in a crystal slurry, by desupersaturation of a supersaturated solution, the installation comprising a crystallization chamber which has a vertical axis and is divided into a central zone (4) and an annular zone (5), a device (9, 10) designed to bring about a vertical translation of the slurry in the central zone (4) and a translation in the opposite direction in the annular zone (5), a device (8) for withdrawing slurry, comprising a tube (23, 24) which opens into one of the abovementioned zones, a member (14) for mechanical shearing of the slurry, comprising, a disc (17) carrying a ring of shearing teeth (19), and a tube (6, 31) passing through the cover (30) and serving to introduce anhydrous sodium carbonate, the tube (31) having a prolongation inside the crystallization chamber, over which prolongation a film of water is caused to circulate.
摘要翻译： 通过过饱和溶液的过饱和来安装结晶浆料中无机物质的结晶，该装置包括具有垂直轴并分成中心区域（4）和环形区域（5）的结晶室， 设备（9,10），其被设计成使得所述浆料在所述中心区域（4）中的垂直平移和在所述环形区域（5）中沿相反方向的平移;用于抽出浆料的装置（8），包括管 （23,24），其通向上述区域之一，用于机械剪切浆料的构件（14），包括：承载剪切齿环（19）的盘（17）和管（6,31 ）通过所述盖（30）并且用于引入无水碳酸钠，所述管（31）在所述结晶室内具有延长部分，从而延长了膜的水循环。
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公开(公告)号：US06692720B1
公开(公告)日：2004-02-17
申请号：US09763638
申请日：2001-08-27
申请人： Leon Ninane , Cédric Humblot , Pascal Gerard
发明人： Leon Ninane , Cédric Humblot , Pascal Gerard
IPC分类号： C01D316
摘要： Process for the production of sodium chloride crystals from a sodium chloride brine contaminated by potassium chloride and sulphate ions, according to which a calcium compound (32) is added to the brine (48) to crystallize glauberite (35), which is isolated, the resulting aqueous solution (36) is subjected to evaporation to crystallize sodium chloride (40), which is collected, and the aqueous mother liquor (41) from the crystallization of the sodium chloride is subjected to cooling (42) to crystallize glaserite (45).
摘要翻译： 由氯化钾和硫酸根离子污染的氯化钠盐水生产氯化钠晶体的方法，根据该方法，将钙化合物（32）加入到盐水（48）中以结晶分离的芒硝（35）， 使得到的水溶液（36）蒸发以结晶收集的氯化钠（40），并将来自氯化钠结晶的母液（41）冷却（42）以结晶闪石（45） 。
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公开(公告)号：US5478447A
公开(公告)日：1995-12-26
申请号：US204261
申请日：1994-04-22
申请人： Leon Ninane , Jean-Francois Adam , Cedric Humblot
发明人： Leon Ninane , Jean-Francois Adam , Cedric Humblot
摘要： Process for the manufacture of an industrial aqueous solution of sodium chloride, according to which an aqueous mixture (12) containing an aqueous solution of sodium chloride and of polyvalent metals is prepared by introducing into water (10) a solid product (8) collected from the dry-route treatment, with sodium bicarbonate (4), of smokes (2) containing hydrogen chloride, and the said aqueous medium (12) is treated in order to remove the polyvalent metals therefrom.
摘要翻译： PCT No.PCT / EP92 / 00944 Sec。 371日期1994年04月22日 102（e）日期1994年4月22日PCT提交1992年8月31日PCT公布。 公开号WO93 / 04983 日本1993年3月18日制造工业氯化钠水溶液的方法，根据该方法，将含有氯化钠水溶液和多价金属的含水混合物（12）通过引入水（10）a 用碳酸氢钠（4），含有氯化氢的烟雾（2）收集干燥路线处理的固体产物（8），并处理所述水性介质（12）以从中除去多价金属。
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公开(公告)号：US5993772A
公开(公告)日：1999-11-30
申请号：US860567
申请日：1997-09-12
申请人： Leon Ninane , Claude Criado , Francis Feys
发明人： Leon Ninane , Claude Criado , Francis Feys
CPC分类号： C01F11/181 , C01D1/22
摘要： Process for the coproduction of calcium carbonate and sodium hydroxide, comprisingcausticizing sodium carbonate with milk of lime;separating the calcium carbonate and the sodium hydroxide formed in the causticizing stage; andcarbonating a mixture of milk of lime and of the calcium carbonate resulting from the causticizing stage.
摘要翻译： PCT No.PCT / EP95 / 05175第 371日期：1997年9月12日 102（e）日期1997年9月12日PCT 1995年12月22日PCT PCT。 公开号WO96 / 21620 PCT 日期1996年7月18日碳酸钙和氢氧化钠共同生产的方法，包括用碳酸钠与石灰酸乳化; 分离在苛化阶段形成的碳酸钙和氢氧化钠; 并且将由酸化阶段产生的石灰和碳酸钙的混合物进行碳酸化。
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公开(公告)号：US3967039A
公开(公告)日：1976-06-29
申请号：US352048
申请日：1973-04-17
申请人： Leon Ninane , Willy Kegelart
发明人： Leon Ninane , Willy Kegelart
CPC分类号： C01B11/10 , Y10T428/2991
摘要： In order to reduce the tendency to decompose of particles or granules of alkali metal chlorites and to enhance their stability, said particles or granules are completely coated with an inorganic salt or a mixture of such salts which are compatible with the chlorite and with each other, e.g. nitrates, carbonates, bicarbonates, phosphates, silicates and chlorides, especially alkali metal salts and alkaline earth metal salts thereof. The coating may be carried out by any conventional coating process, e.g. by contacting the particles with a solution of the stabilizing salts under vaporizing conditions in a rotating inclined disk, a rotary drum, or in a fluidized bed.
摘要翻译： 为了降低碱金属亚氯酸盐的颗粒或颗粒的分解倾向并提高其稳定性，所述颗粒或颗粒完全涂覆有与亚氯酸盐相容的无机盐或这些盐的混合物， 例如 硝酸盐，碳酸盐，碳酸氢盐，磷酸盐，硅酸盐和氯化物，特别是其碱金属盐和碱土金属盐。 涂层可以通过任何常规的涂覆方法进行，例如 通过在旋转的倾斜盘，旋转鼓或流化床中的蒸发条件下将颗粒与稳定盐的溶液接触。
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