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公开(公告)号:US11813552B2
公开(公告)日:2023-11-14
申请号:US16964041
申请日:2019-08-20
Applicant: LG Chem, Ltd.
Inventor: Jung Kee Jang , Jeong Hun Cho , Joon Hee Cho , Ye Hoon Im , Young Soo Song
Abstract: The present invention relates to a dispersion device and a defoamation device comprising the same, which provides a dispersion device comprising a dispersion plate equipped with an inclined surface extended downwards obliquely and raw material inflow nozzles formed on the inclined surface to introduce a raw material into the inclined surface; and a band spaced apart from the inclined surface of the dispersion plate to form a gap from the inclined surface, thereby being configured so that the raw material flows through the gap.
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公开(公告)号:US11427659B2
公开(公告)日:2022-08-30
申请号:US16481395
申请日:2018-09-18
Applicant: LG CHEM, LTD.
Inventor: Chang Hun Kim , Hyun Min Kim , Jeong Hun Cho , Joon Hee Cho
IPC: C08F20/44 , C08F220/46 , D01F9/22 , C08F120/44 , C08F220/48 , C08F120/42 , C08F220/44 , C08F20/42 , C08F2/06 , C08F2/04
Abstract: A method of preparing an acrylonitrile-based copolymer for a carbon fiber. The method includes: preparing a reaction solution including a (meth)acrylonitrile-based monomer and a first reaction solvent; adding a first portion of a radical polymerization initiator to the reaction solution to initiate polymerization; and adding a second portion of the radical polymerization initiator to the reaction solution when a polymerization conversion ratio is between 70 to 80%.
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公开(公告)号:US11286580B2
公开(公告)日:2022-03-29
申请号:US16491476
申请日:2018-09-27
Applicant: LG CHEM, LTD.
Inventor: Sang Jin Kim , Chang Hong Bak , Hye Jin Han , Ki Yeon Jo , Jeong Hun Cho , Joon Hee Cho
IPC: D01D1/02 , D01D10/02 , D01D10/06 , D01F1/10 , C01B32/05 , C08F222/30 , C08J5/00 , D01D5/06 , D01F6/18 , D01F9/22 , D01D5/04 , D01F6/38
Abstract: The present invention relates to a method for producing an acrylonitrile-based fiber, the method including: providing a polymer solution including an acrylonitrile-based copolymer containing a carboxylic acid group; mixing 100 parts by weight of the polymer solution with 1 to 6 parts by weight of a hydrophilization solution containing an organic solvent and ammonia water in a weight ratio of 95:5 to 60:40 to prepare a spinning stock solution; and spinning the spinning stock solution. The method controls the viscosity of the spinning stock solution to improve the stretchability and strength of the acrylonitrile-based fiber, and suppresses the occurrence of gelation.
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公开(公告)号:US20210039021A1
公开(公告)日:2021-02-11
申请号:US16964041
申请日:2019-08-20
Applicant: LG Chem, Ltd.
Inventor: Jung Kee Jang , Jeong Hun Cho , Joon Hee Cho , Ye Hoon Im , Young Soo Song
Abstract: The present invention relates to a dispersion device and a defoamation device comprising the same, which provides a dispersion device comprising a dispersion plate equipped with an inclined surface extended downwards obliquely and raw material inflow nozzles formed on the inclined surface to introduce a raw material into the inclined surface; and a band spaced apart from the inclined surface of the dispersion plate to form a gap from the inclined surface, thereby being configured so that the raw material flows through the gap.
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公开(公告)号:US11535957B2
公开(公告)日:2022-12-27
申请号:US16335076
申请日:2017-11-22
Applicant: LG CHEM, LTD.
Inventor: Jeong Kyu Lee , Chang Hun Kim , In Young Song , Jeong Hun Cho , Jong Soo Do , Sung Joon Oh , Joon Hee Cho
IPC: D01F9/22 , C08F220/04 , C08F220/18 , C08F220/44
Abstract: The present invention relates to a method for producing a polyacrylonitrile-based fiber, wherein the method polymerizes a monomer mixture including an acrylonitrile-based monomer, a carboxylic acid-based comonomer, and an acrylate-based comonomer, wherein the acrylate-based comonomer includes the steps of producing a polyacrylonitrile-based copolymer so as to be included in an amount of 4 to 20 parts by weight based on 100 parts by weight of the monomer mixture, fiberizing the polyacrylonitrile-based copolymer, oxidizing and stabilizing the fiberized polyacrylonitrile-based copolymer, which may control the oxidation stabilization reaction, particularly the cyclization reaction. Accordingly, the energy consumption of the oxidation stabilization reaction may be reduced, economical efficiency of the production of polyacrylonitrile-based fiber may be obtained, and the physical and mechanical properties of the carbon fiber may be improved.
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公开(公告)号:US11905354B2
公开(公告)日:2024-02-20
申请号:US17266078
申请日:2019-11-01
Applicant: LG CHEM, LTD.
Inventor: Jong Gil Kim , Chang Hun Kim , Jeong Hun Cho , Hyun Min Kim , Joon Hee Cho , Hyo Yong Kim
IPC: C08F220/46 , C01B32/05 , D01F9/22
CPC classification number: C08F220/46 , C01B32/05 , D01F9/22 , C08F2800/10
Abstract: Provided is a method of preparing an acrylonitrile-based copolymer for a carbon fiber, which comprises: preparing a reaction solution including a monomer mixture comprising a sulfonate-based monomer represented by Chemical Formula 1, a carboxylic acid-based monomer, and an acrylonitrile-based monomer and an organic solvent; and subjecting the reaction solution to polymerization, wherein the monomer mixture comprises the sulfonate-based monomer represented by Chemical Formula 1 at 0.55 to 1.6 mol %.
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公开(公告)号:US20210230330A1
公开(公告)日:2021-07-29
申请号:US17265462
申请日:2019-11-01
Applicant: LG CHEM, LTD.
Inventor: Chang Hun Kim , Jong Gil Kim , Hyun Min Kim , Yeon Soo Kim , Jeong Hun Cho , Hye Jin Han , Joon Hee Cho
IPC: C08F220/46 , D01F9/22
Abstract: Provided is an acrylonitrile-based copolymer for a carbon fiber which includes a sulfonate-based monomer unit, a carboxylic acid-based monomer unit, and an acrylonitrile-based monomer unit, and the acrylonitrile-based copolymer for a carbon fiber includes the sulfonate-based monomer unit at 0.55 to 1.55 mol %, and the carboxylic acid-based monomer unit at 0.60 to 1.40 mol %.
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公开(公告)号:US11046792B2
公开(公告)日:2021-06-29
申请号:US16469030
申请日:2018-09-14
Applicant: LG CHEM, LTD.
Inventor: Jeong Hun Cho , Young Soo Song , Hyun Min Kim , Chang Hun Kim , Hyo Yong Kim , Joon Hee Cho
Abstract: The present invention relates to a method of preparing a (meth)acrylonitrile-based polymer for preparing a carbon fiber, which comprises adding a reaction solution comprising a (meth)acrylonitrile-based monomer and a reaction solvent to a reactor to perform solution polymerization, performing solution polymerization under a condition in which a power consumption of the reactor is 1 to 5 kW/m3 when the reaction solution in the reactor has a viscosity of 0.1 poise or more and 250 poise or less, and performing solution polymerization under a condition in which a power consumption of the reactor is 8 to 13 kW/m3 when the reaction solution in the reactor has a viscosity of more than 250 poise and 450 poise or less.
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