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1.发明授权
公开(公告)号：US5830964A
公开(公告)日：1998-11-03
申请号：US993908
申请日：1997-12-18
IPC分类号： C08F226/06 , C08F220/04 , C08F220/18 , C08F220/20 , C08F220/56 , C08F222/06 , C08F226/10
CPC分类号： C08F226/06
摘要： This invention relates to substantially colorless and odorless vinyl lactam polymers containing less than 100 ppm residual vinyl pyrrolidone and less than 1000 ppm vinyl caprolactam monomers and to the process for producing said polymers in the above state of purity which comprises contacting a vinyl pyrrolidone and/or vinyl caprolactam polymer containing excessive residual monomer with between about 0.1 and about 9 wt. % of porous resin having a sulfonic and/or carboxylic functionality wherein said resin has a particle size between 5 and 500 mesh.
摘要翻译： 本发明涉及含有小于100ppm残余乙烯基吡咯烷酮和小于1000ppm乙烯基己内酰胺单体的基本上无色无味的乙烯基内酰胺聚合物，以及以上述纯度状态生产所述聚合物的方法，该方法包括使乙烯基吡咯烷酮和/或 含有过量残留单体的乙烯基己内酰胺聚合物的含量为约0.1至约9wt。 ％的具有磺酸和/或羧酸官能团的多孔树脂，其中所述树脂具有5至500目的粒度。
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2.发明授权Low VOC hair spray compositions containing terpolymers of vinyl pyrrolidone, vinyl caprolactam and 3-(N-dimethylaminopropyl) methacrylamide 失效含有乙烯基吡咯烷酮，乙烯基己内酰胺和3-（N-二甲基氨基丙基）甲基丙烯酰胺的三元共聚物的低VOC喷发组合物
公开(公告)号：US5626836A
公开(公告)日：1997-05-06
申请号：US365259
申请日：1994-12-28
CPC分类号： A61K8/8182 , A61K8/046 , A61Q5/06 , Y10S424/01 , Y10S424/02 , Y10S514/957
摘要： Low VOC hair spray resin compositions containing homogeneous terpolymers of vinyl pyrrolidone, vinyl caprolactam and 3-(N-dimethylaminopropyl) methacrylamide are described. The hair spray compositions are made using a solution of the terpolymer which is clear and low in viscosity, and which provides a spray of relative small particle size. The hair spray compositions exhibit an effective high humidity curl retention property.
摘要翻译： 描述了含有乙烯基吡咯烷酮，乙烯基己内酰胺和3-（N-二甲基氨基丙基）甲基丙烯酰胺的均匀三元共聚物的低VOC发胶树脂组合物。 发胶组合物使用透明且粘度低的三元共聚物溶液制成，并提供相对较小粒度的喷雾。 喷发组合物表现出有效的高湿度卷曲保持性能。
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公开(公告)号：US5603919A
公开(公告)日：1997-02-18
申请号：US369013
申请日：1995-01-05
申请人： Kou-Chang Liu , Colleen M. Rocafort
发明人： Kou-Chang Liu , Colleen M. Rocafort
CPC分类号： A61K8/8182 , A61K8/046 , A61Q5/06 , Y10S424/01 , Y10S424/02 , Y10S514/957
摘要： Low VOC hair spray fixative compositions containing a fixative which is a tetramer of vinyl pyrrolidone, vinyl caprolactam, 3-(N-dimethylaminopropyl) methacrylamide and a C.sub.8 -C.sub.18 alkyl acrylamide or acrylate, in predetermined compositional ranges of each monomer, and molecular weight, are described. The hair spray compositions herein are clear and low in viscosity, and form a spray of relatively small particle size which spreads evenly on the hair of the user as clear films which exhibit an effective high humidity curl retention property, good stiffness, and low tack and short drying times.
摘要翻译： 含有在各单体的预定组成范围内的乙烯基吡咯烷酮，乙烯基己内酰胺，3-（N-二甲基氨基丙基）甲基丙烯酰胺和C 8 -C 18烷基丙烯酰胺或丙烯酸酯的四聚物的固定剂的低VOC发胶固定剂组合物和分子量， 被描述。 本发明的喷发组合物是透明且粘度低的，并且形成相对较小粒度的喷雾，其均匀地扩散在使用者的头发上，作为透明膜，其表现出有效的高湿度卷曲保持性，良好的刚度和低粘性， 干燥时间短
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公开(公告)号：US5637296A
公开(公告)日：1997-06-10
申请号：US298738
申请日：1994-08-31
申请人： Colleen M. Rocafort
发明人： Colleen M. Rocafort
CPC分类号： A61Q5/06 , A61K8/046 , A61K8/8182 , Y10S424/01 , Y10S514/957
摘要： This invention relates to a 0.5 to 7 wt. % solids hair fixative composition having superior moisture resistant hold and minimal tack duration which provides a stiff film on artificial or human hair and superior hair combability, which composition essentially contains a resin mixture of (a) a terpolymer derived from about 17 to about 30 wt. % N-vinyl pyrrolidone, from about 60 to about 80 wt. % N-vinyl caprolactam and from about 3 to about 6 wt. % di-C.sub.1 -C.sub.4 alkyl amino-C.sub.1 -C.sub.4 alkyl-acrylate or methacrylate having a number average molecular weight of between about 20,000 and about 200,000 and (b) a N-vinyl pyrrolidone/vinyl acetate copolymer having a number average molecular weight of between about 10,000 and about 100,000; combined in a weight ratio of 1.4-6:1 (a) to (b). In the present composition, the vinyl acetate moiety of the N-vinyl pyrrolidone/vinyl acetate copolymer interacts with resin (a) to reinforce stiffness and holding properties under conditions of extremely high humidity and materially lowers the duration of tackiness during drying.
摘要翻译： 本发明涉及0.5至7wt。 ％固体发丝固定剂组合物具有优异的耐湿保持性和最小的粘着持续时间，其在人造或人发上提供硬膜，并具有优异的头发可梳理性，该组合物基本上含有（a）衍生自约17至约30重量％ 。 ％N-乙烯基吡咯烷酮，约60至约80wt。 ％N-乙烯基己内酰胺和约3至约6wt。 数均分子量为约20,000至约200,000的二（C 1 -C 4）烷基氨基-C 1 -C 4烷基 - 丙烯酸酯或甲基丙烯酸酯和（b）数均分子量在约20000至约200,000之间的N-乙烯基吡咯烷酮/乙酸乙烯酯共聚物 约10,000和约100,000; 组合重量比为1.4-6：1（a）至（b）。 在本发明的组合物中，N-乙烯基吡咯烷酮/乙酸乙烯酯共聚物的乙酸乙烯酯部分与树脂（a）相互作用，以在非常高的湿度条件下增强刚度和保持性能，并且在干燥期间粘性持续时间大大降低。
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公开(公告)号：US5597551A
公开(公告)日：1997-01-28
申请号：US369016
申请日：1995-01-05
CPC分类号： A61Q5/06 , A61K8/046 , A61K8/068 , A61K8/8129 , A61K8/8164 , A61K8/86 , Y10S424/01 , Y10S424/02 , Y10S514/937 , Y10S514/957
摘要： A low volatile organic compound hair spray composition in the form of a stable, clear, single phase microemulsion in which the particles therein have a diameter of less than 1 micron, consisting essentially of by weight,(a) a butyl half-ester of a copolymer of maleic anhydride and ethyl vinyl ether in an amount of about 2-10%, optionally neutralized up to 20 mole %,(b) poly(methyl vinyl ether) as a surface active polymer in an amount of at least 0.75 to 1 part of (a);(c) a secondary surfactant that is a polyethoxylated glyceryl fatty acid ester in an amount of at least 0.1%, and which has a hydrophilic-hydrophobic balance of greater than 10,(d) ethanol in an amount of 20 to 50%, and(e) water to 100%.
摘要翻译： 一种稳定，透明的单相微乳液形式的低挥发性有机化合物发胶组合物，其中颗粒中的颗粒直径小于1微米，基本上由重量计组成，（a） 马来酸酐和乙基乙烯基醚的共聚物，其量为约2-10％，任选中和至多20摩尔％，（b）作为表面活性聚合物的聚（甲基乙烯基醚）的量为至少0.75至1份 的（a）; （c）第二表面活性剂，其为至少0.1％的聚乙氧基化甘油脂肪酸酯，并且其亲水疏水性平衡大于10，（d）乙醇的量为20至50％，和 （e）水至100％。
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6.发明授权Hair spray composition having 80% or less VOC and advantageous physical and performance characteristics 失效具有80％或更低VOC和有利的物理和性能特征的喷发组合物
公开(公告)号：US5614173A
公开(公告)日：1997-03-25
申请号：US569809
申请日：1995-12-08
申请人： Herbert Ulmer , Colleen M. Rocafort
发明人： Herbert Ulmer , Colleen M. Rocafort
CPC分类号： A61Q5/06 , A61K8/046 , A61K8/8164 , Y10S424/01 , Y10S424/02 , Y10S514/957
摘要： A hair spray composition of 80% or less VOC includes a fixative which is the half-ester of a copolymer of maleic anhydride and methyl vinyl ether having advantageous physical and performance properties even at low fixative levels. The copolymer is made by polymerizing the monomers at a selected temperature in the presence of a predetermined amount of a polymerization initiator whose decomposition fragments are soluble in hydroalcoholic solutions containing high levels of water. The composition is clear and without precipitate formation, has a low weight average molecular weight and a narrow molecular weight distribution or polydispersity, affording a low solution viscosity. The composition also forms a spray pattern of small particle size, providing clear, hard fixative films with superior adhesion to the hair of the user, an advantageous high humidity curl retention (hold), and low tack and dry times, in both pump and aerosol products.
摘要翻译： 80％或更低VOC的喷发组合物包括固定剂，其即使在低固定水平下也具有有利的物理和性能特性的马来酸酐和甲基乙烯基醚的共聚物的半酯。 共聚物是通过在预定量的聚合引发剂存在下在选定温度下聚合单体制备的，其分解片段可溶于含有高含量水的水醇溶液。 该组合物是透明的且没有沉淀物形成，具有低重均分子量和窄分子量分布或多分散性，提供低溶液粘度。 该组合物还形成小粒径的喷雾图案，提供清晰，硬的固定膜，具有优于使用者头发的粘附性，在泵和气溶胶中有利的高湿度卷曲保持（保持）和低粘性和干燥时间 产品。
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7.发明申请Hair care formulations comprising UV absorbers and certain silicone derivatives 审中-公开包含UV吸收剂和某些硅氧烷衍生物的护发制剂公开(公告)号：US20100021407A1
公开(公告)日：2010-01-28
申请号：US12286260
申请日：2008-09-29
摘要： This invention relates to hair conditioning formulations comprising at least one aminofunctional polyorganosiloxane. Furthermore, the invention relates to the use of these formulations for the treatment of keratin-containing fibers, preferably human hair.
摘要翻译： 本发明涉及包含至少一种氨基官能聚有机硅氧烷的护发制剂。 此外，本发明涉及这些制剂用于治疗含角蛋白的纤维，优选人类头发的用途。
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公开(公告)号：US5626835A
公开(公告)日：1997-05-06
申请号：US255192
申请日：1994-06-07
CPC分类号： A61K8/068 , A61K8/39 , A61K8/8164 , A61Q5/06 , Y10S424/01 , Y10S424/02 , Y10S514/957
摘要： A low volatile organic compounds hair spray microemulsion in the form of a stable, clear, single phase system in which the particles therein have a diameter of less than 1 micron, consisting essentially of, by weight,(a) an ethyl half-ester of a copolymer of maleic anhydride and an alkyl vinyl ether in an amount of less than 20%, optionally neutralized up to 20 mole %,(b) an ethoxylated glycerol fatty acid ester as the surfactant having a hydrophobic-lipophilic balance of 10-18, in an amount of at least 0.1%,(c) ethanol in an amount of 55% or less, and(d) water to 100%.
摘要翻译： 低挥发性有机化合物发胶微乳液，其形式为稳定，透明的单相体系，其中颗粒中的颗粒直径小于1微米，基本上由（a）（a）的 马来酸酐和烷基乙烯基醚的共聚物，其量小于20％，任选中和至多20摩尔％，（b）作为表面活性剂的乙氧基化甘油脂肪酸酯具有10-18的疏水 - 亲油平衡， 至少0.1％的量，（c）乙醇的含量为55％以下，（d）水至100％。
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9.发明授权Innovative-type hair spray concentrate capable of delivering reduced VOC spray particles 失效创新型喷发浓缩液能够输送降低的VOC喷雾颗粒
公开(公告)号：US5759522A
公开(公告)日：1998-06-02
申请号：US740344
申请日：1996-11-07
申请人： Herbert Ulmer , Colleen M. Rocafort
发明人： Herbert Ulmer , Colleen M. Rocafort
CPC分类号： A61Q5/06 , A61K8/046 , A61K8/8164 , Y10S424/01 , Y10S424/02 , Y10S514/957
摘要： An innovative-type hair spray concentrate of defined Brookfield viscosity and solids content which is capable of delivering reduced VOC spray particles of acceptable quality under the Innovative Product Clause Regulations in combination with a suitable restricter valve and actuator system. The concentrate includes a fixative which is the half-ester of a copolymer of maleic anhydride and methyl vinyl ether having a weight average molecular weight of about 40,000 to about 70,000, which provides advantageous physical and use performance properties.
摘要翻译： 一种创新型发胶浓缩物，具有明确的布鲁克菲尔德粘度和固体含量，可根据“创新产品条款”规定，结合合适的限制阀和执行器系统，将可接受质量的VOC喷雾颗粒降低。 浓缩物包括固定剂，其是重均分子量为约40,000至约70,000的马来酸酐和甲基乙烯基醚的共聚物的半酯，其提供有利的物理和使用性能。
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公开(公告)号：US5686067A
公开(公告)日：1997-11-11
申请号：US539474
申请日：1995-10-05
CPC分类号： A61K8/046 , A61K8/8182 , A61Q5/06 , Y10S424/02
摘要： A low VOC (volatile organic compounds) hair spray composition having a combination of desirable user performance characteristics is described herein. The hair fixative resin in the composition is a terpolymer of 40-75% by weight of a vinyl lactam, preferably vinyl pyrrolidone, 15-40% of a polymerizable carboxylic acid, preferably acrylic acid or methacrylic acid, and 5-25% of a hydrophobic monomer, preferably a long chain alkyl (C.sub.8 -C.sub.24) acrylate, methacrylate, acrylamide or methacrylamide. The terpolymer has a K-value of 30-55, preferably 40-50, which provides compositions having good sprayability in both pump and aerosol form, and small, fine spray particles.
摘要翻译： 本文描述了具有期望的用户性能特征的组合的低VOC（挥发性有机化合物）喷发组合物。 组合物中的头发固定树脂是40-75重量％的乙烯基内酰胺，优选乙烯基吡咯烷酮，15-40％的可聚合羧酸，优选丙烯酸或甲基丙烯酸，和5-25％ 疏水单体，优选长链烷基（C 8 -C 24）丙烯酸酯，甲基丙烯酸酯，丙烯酰胺或甲基丙烯酰胺。 三元共聚物的K值为30-55，优选为40-50，其提供在泵和气溶胶形式以及小的细小喷雾颗粒中具有良好喷雾性的组合物。
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