公开(公告)号：US20160121401A1

公开(公告)日：2016-05-05

申请号：US14563494

申请日：2014-12-08

Applicant: Korea Basic Science Institute

Inventor： Gaehang LEE ,  Yeon Suk CHOI

IPC: B22F9/24 ,  C22B3/00 ,  B22F9/30

CPC classification number: B22F9/24 ,  B22F1/0018 ,  B22F2301/255 ,  C22B11/04 ,  C22C5/06

Abstract: Provided is a method of synthesizing silver nanoparticles including: a) a nucleation step of reacting a composition containing a silver precursor, a heterogeneous metal precursor, and an amine-based compound at 30 to 120° C. to form a nucleus; and b) a growth step of reacting the composition containing the nucleus formed therein at 155 to 350° C. to grow the nucleus. According to the present invention, significantly uniform and fine silver nanoparticles may be synthesized with high reproducibility on a large scale.

Abstract translation: 提供一种合成银纳米颗粒的方法，其包括：a）在30〜120℃下使含有银前体，异质金属前体和胺系化合物的组合物反应以形成核的成核步骤; 和b）生长步骤，使含有其中形成的细胞核的组合物在155-350℃下反应以生长细胞核。 根据本发明，可以大规模地以高再现性合成显着均匀且细小的银纳米颗粒。

公开(公告)号：US20150132595A1

公开(公告)日：2015-05-14

申请号：US14176357

申请日：2014-02-10

Applicant: Korea Basic Science Institute

Inventor： Gaehang LEE ,  Yeon Suk CHOI ,  Doo Ri BAE

IPC: C07F1/00

CPC classification number: C07F1/10 ,  B22F1/0044 ,  B22F1/0048 ,  B22F9/24 ,  Y10T428/12

Abstract: Provided is a preparing method of an Ag nano-particle for mass-producing Ag nano-particles, the method including: performing a first reaction of a reaction solution containing an Ag precursor and oleylamine at a set first temperature T1; performing a second reaction of the reaction solution at a second temperature T2 set so as to be higher than the first temperature; and obtaining a reactant from the reaction solution, wherein at least one of the first and second reactions is performed in a state in which the reaction solution is not stirred.

Abstract translation: 本发明提供一种用于大量生产Ag纳米颗粒的Ag纳米颗粒的制备方法，该方法包括：在设定的第一温度T1下进行含有Ag前体和油胺的反应溶液的第一次反应; 在设定为高于第一温度的第二温度T2下进行反应溶液的第二反应; 从所述反应溶液中获得反应物，其中所述第一反应和所述第二反应中的至少一个在所述反应溶液不被搅拌的状态下进行。