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    Thermosetting aqueous-type emulsion of nadimides
    1.
    发明授权
    Thermosetting aqueous-type emulsion of nadimides 失效
    纳迪霉素的热固性水性乳液

    公开(公告)号：US5663256A

    公开(公告)日：1997-09-02

    申请号：US546713

    申请日：1995-10-23

    申请人： Hideya Ariga ,  Norio Futaesaku ,  Hiromitsu Baba

    发明人： Hideya Ariga ,  Norio Futaesaku ,  Hiromitsu Baba

    IPC分类号： C08F122/40 ,  C07D209/76 ,  C08F12/32 ,  C08F20/52 ,  C08F26/06 ,  C09D4/00 ,  C08F222/40

    CPC分类号： C08F12/32 ,  C07D209/76 ,  C09D4/00

    摘要： A thermosetting aqueous-type emulsion of nadimide is disclosed. The emulsion comprises 1-70% by weight of an alkenyl-substituted nadimide, 0.1-20% by weight of protective colloid and/or surface-active agent and balance water. The emulsion is especially useful for making a paint, a coating material or an adhesive because the emulsion can easily be cured only by heating without forming any undesirable organic pollutants. In the past, various resins have been used together with organic solvents. However, because of the recent worldwide concern over the influence of organic solvents to pollution of the aerospace and underground environments, non-use or reduced-use of organic solvents is actively desired. Accordingly, developments of aqueous solution or aqueous-type emulsion of resins are desired. Until now there is no aqueous-type emulsion of a monomer of highly heat resistant polyimide.

    摘要翻译： 公开了一种纳米二酰亚胺的热固性水性乳液。 乳液包含1-70重量％的链烯基取代的酰亚胺，0.1-20重量％的保护胶体和/或表面活性剂和余量的水。 该乳液特别可用于制备涂料，涂料或粘合剂，因为乳液可以容易地通过加热固化而不形成任何不期望的有机污染物。 以往，各种树脂与有机溶剂一起使用。 然而，由于最近全球对有机溶剂对航空航天和地下环境污染的影响令人担忧，因此积极地期望不使用或减少有机溶剂。 因此，需要开发树脂的水溶液或水性乳液。 到目前为止，还没有高耐热聚酰亚胺单体的水性乳液。

    Alkenyl-substituted bisnadimides, process for manufacturing the same, process for curing the same, and adhesives and coating materials utilizing the same
    2.
    发明授权
    Alkenyl-substituted bisnadimides, process for manufacturing the same, process for curing the same, and adhesives and coating materials utilizing the same 失效
    烯基取代的双茚二酰亚胺，其制造方法，其固化方法，使用其的粘合剂和涂料

    公开(公告)号：US5502207A

    公开(公告)日：1996-03-26

    申请号：US288592

    申请日：1994-08-10

    申请人： Norio Futaesaku ,  Hideo Fukuda ,  Yoshiharu Itou ,  Hiromitsu Baba ,  Isao Maruyama

    发明人： Norio Futaesaku ,  Hideo Fukuda ,  Yoshiharu Itou ,  Hiromitsu Baba ,  Isao Maruyama

    IPC分类号： C07D209/76 ,  C08F4/34 ,  C08F4/42 ,  C08F22/40 ,  C08F226/06 ,  C09D4/00 ,  C08F222/40

    CPC分类号： C08F226/06 ,  C07D209/76 ,  C08F22/40 ,  C09D4/00

    摘要： An alkenyl-substituted bisnadimide represented by the following formula 1!: ##STR1## wherein R.sup.1 and R.sup.2 individually represent a hydrogen atom or a methyl group, and E is an alkylene.phenylene group or an alkylene.phenylene.alkylene group represented by the following formula 2!: ##STR2## (wherein a is an integer of 0 or 1, and R.sup.3' individually represent a C.sub.1 -C.sub.4 alkylene group or a C.sub.5 -C.sub.8 cycloalkylene group)!, a process for the preparation of the same and a process for curing the same are disclosed. Further, an adhesive material and a coating material containing the bisnadimide as a curing component are also disclosed. A cured material obtaind from the bisnadimide has excellent heat resistance, mechanical strength, toughness, adhesion property to many kinds of substrates, and so on. The adhesive material shows excellent heat resistance and the coating material shows excellent boiling water resistance.

    摘要翻译： 由下式[1]表示的烯基取代的双酰亚胺：其中R 1和R 2各自表示氢原子或甲基，E是亚烷基亚苯基或亚烷基亚苯基亚烷基 由下式[2]表示的基团： [2]（其中a是0或1的整数，并且R 3'个别地表示C 1 -C 4亚烷基或C 5 -C 8亚环烷基）]， 公开了其制备方法和固化方法。 此外，还公开了粘合剂材料和含有双酰亚胺作为固化组分的涂料。 从bisnadimide获得的固化物具有优异的耐热性，机械强度，韧性，对多种基材的粘附性等。 粘合剂材料具有优异的耐热性，并且涂料显示出优异的耐沸水性。

    Alkenyl-substituted bisnadimides, process for manufacturing the same, process for curing the same, and adhesives and coating materials utilizing the same
    3.
    发明授权
    Alkenyl-substituted bisnadimides, process for manufacturing the same, process for curing the same, and adhesives and coating materials utilizing the same 失效
    烯基取代的双茚二酰亚胺，其制造方法，其固化方法，使用其的粘合剂和涂料

    公开(公告)号：US5663257A

    公开(公告)日：1997-09-02

    申请号：US566863

    申请日：1995-12-04

    申请人： Norio Futaesaku ,  Hideo Fukuda ,  Yoshiharu Itou ,  Hiromitsu Baba ,  Isao Maruyama

    发明人： Norio Futaesaku ,  Hideo Fukuda ,  Yoshiharu Itou ,  Hiromitsu Baba ,  Isao Maruyama

    IPC分类号： C07D209/76 ,  C08F4/34 ,  C08F4/42 ,  C08F22/40 ,  C08F226/06 ,  C09D4/00

    CPC分类号： C08F226/06 ,  C07D209/76 ,  C08F22/40 ,  C09D4/00

    摘要： An alkenyl-substituted bisnadimide represented by the following formula [1]: ##STR1## [wherein R.sup.1 and R.sup.2 individually represent a hydrogen atom or a methyl group, and E is an alkylene.multidot.phenylene group or an alkylene.multidot.phenylene.multidot.alkylene group represented by the following formula [2]: ##STR2## (wherein a is an integer of 0 or 1, and R.sup.3 and R.sup.3' individually represent a C.sub.1 -C.sub.4 alkylene group or a C.sub.5 -C.sub.8 cycloalkylene group)], a process for the preparation of the same and a process for curing the same are disclosed. Further, an adhesive material and a coating material containing the bisnadimide as a curing component are also disclosed. A cured material obtaind from the bisnadimide has excellent heat resistance, mechanical strength, toughness, adhesion property to many kinds of substrates, and so on. The adhesive material shows excellent heat resistance and the coating material shows excellent boiling water resistance.

    摘要翻译： 由下式[1]表示的烯基取代双酰亚胺：其中，R 1和R 2分别表示氢原子或甲基，E表示亚烷基亚苯基或亚甲基亚苯基亚烷基亚烷基， [2]： [2]（其中a为0或1的整数，R 3和R 3'分别表示C 1 -C 4亚烷基或C 5 -C 8亚环烷基）]， 公开了相同的固化方法和固化方法。 此外，还公开了粘合剂材料和含有双酰亚胺作为固化组分的涂料。 从bisnadimide获得的固化物具有优异的耐热性，机械强度，韧性，对多种基材的粘附性等。 粘合剂材料具有优异的耐热性，并且涂料显示出优异的耐沸水性。

    Thermosetting resin composition
    4.
    发明授权
    Thermosetting resin composition 失效
    热固性树脂组合物

    公开(公告)号：US5521260A

    公开(公告)日：1996-05-28

    申请号：US346907

    申请日：1994-11-30

    申请人： Norio Futaesaku ,  Hideo Fukuda ,  Yoshie Ito ,  Isao Maruyama

    发明人： Norio Futaesaku ,  Hideo Fukuda ,  Yoshie Ito ,  Isao Maruyama

    IPC分类号： C08K5/01 ,  C08F2/44 ,  C08F22/36 ,  C08F222/40 ,  C08F283/00 ,  C08K5/3415 ,  C08L61/04 ,  C08L61/06 ,  C08L61/10

    CPC分类号： C08F283/00

    摘要： A thermosetting resin composition comprising compounds (A) an alkenyl-substituted nadimide, (B) a compound having at least one vinyl group or cyclic olefin, or both and (C) a phenol resin, and optionally (D) at least one polymerization catalyst selected from the group consisting of organic peroxides, onium salts, and cationic catalysts is disclosed. The components contained in the composition exhibit excellent compatibility among them. The cured product obtained from the thermosetting resin composition has superior anti-hygroscopicity and toughness, without impairing excellent heat resistance, electrical characteristics, mechanical strength, and small molding shrinkage inherently possessed by alkenyl-substituted nadimide resin. The composition is useful not only as a laminating material, a casting material, a molding material, a coating material, a paint, an adhesive, a sealing material, etc., but also as a matrix resin for composite materials.

    摘要翻译： 一种热固性树脂组合物，其包含化合物（A），烯基取代的纳二酰亚胺，（B）具有至少一个乙烯基或环烯烃的化合物或两者，（C）酚醛树脂和任选的（D）至少一种聚合催化剂 公开了选自有机过氧化物，鎓盐和阳离子催化剂的组。 组合物中所含的组分表现出优异的相容性。 由热固性树脂组合物获得的固化产物具有优异的抗吸湿性和韧性，而不损害烯基取代的酰亚胺树脂固有地具有的优异的耐热性，电特性，机械强度和小的成型收缩。 该组合物不仅用作层压材料，浇铸材料，成型材料，涂料，涂料，粘合剂，密封材料等，而且用作复合材料的基质树脂。