公开(公告)号：US20150141689A1

公开(公告)日：2015-05-21

申请号：US14368899

申请日：2012-12-25

Applicant: Dow Corning Toray Co., Ltd.

Inventor： Yasushi Sugiura ,  Yoshinori Taniguchi

IPC: C07F7/18

CPC classification number: C07F7/1876 ,  C07B49/00 ,  C07F7/0827 ,  C07F7/122

Abstract: A method of producing an organic silicon compound includes a step of reaction of the following: (A) a reactive silane compound represented by General Formula (1) below: R1mSiY(4-m) (wherein R1 is a monovalent organic group (except for the group represented by Y) or a hydrogen atom; Y indicates a chlorine atom or a group represented by —OR2; R2 indicates a monovalent hydrocarbon group having 1 to 30 carbon atoms; and m is a number in the range of 0 to 3), (B) a halogenated organic compound represented by General Formula (2) below: R3-X (wherein R3 indicates a monovalent organic group; and X is a halogen atom), and (C) metallic magnesium (Mg) in the presence of (D) an organic solvent containing at least one type of ether type compound.

Abstract translation: 有机硅化合物的制造方法包括以下步骤：（A）由通式（1）表示的反应性硅烷化合物：R1mSiY（4-m）（其中R1是一价有机基团（除 Y表示的基团或氢原子; Y表示氯原子或-OR2表示的基团; R2表示碳原子数1〜30的一价烃基，m表示0〜3的数） ，（B）下述通式（2）表示的卤代有机化合物：R3-X（其中R3表示一价有机基团，X表示卤素原子），（C）金属镁（Mg） （D）含有至少一种醚型化合物的有机溶剂。

公开(公告)号：US09260458B2

公开(公告)日：2016-02-16

申请号：US14368899

申请日：2012-12-25

Applicant: Dow Corning Toray Co., Ltd.

Inventor： Yasushi Sugiura ,  Yoshinori Taniguchi

IPC: C07F7/16 ,  C07F7/18 ,  C07B49/00 ,  C07F7/08 ,  C07F7/12

CPC classification number: C07F7/1876 ,  C07B49/00 ,  C07F7/0827 ,  C07F7/122

Abstract: A method of producing an organic silicon compound includes a step of reaction of the following: (A) a reactive silane compound represented by General Formula (1) below: R1mSiY(4-m) (wherein R1 is a monovalent organic group (except for the group represented by Y) or a hydrogen atom; Y indicates a chlorine atom or a group represented by —OR2; R2 indicates a monovalent hydrocarbon group having 1 to 30 carbon atoms; and m is a number in the range of 0 to 3), (B) a halogenated organic compound represented by General Formula (2) below: R3—X (wherein R3 indicates a monovalent organic group; and X is a halogen atom), and (C) metallic magnesium (Mg) in the presence of (D) an organic solvent containing at least one type of ether type compound.

Abstract translation: 有机硅化合物的制造方法包括以下步骤：（A）由通式（1）表示的反应性硅烷化合物：R1mSiY（4-m）（其中R1是一价有机基团（除 Y表示的基团或氢原子; Y表示氯原子或-OR2表示的基团; R2表示碳原子数1〜30的一价烃基，m表示0〜3的数） ，（B）下述通式（2）表示的卤代有机化合物：R3-X（其中R3表示一价有机基团，X表示卤素原子），（C）金属镁（Mg） （D）含有至少一种醚型化合物的有机溶剂。