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公开(公告)号：US20230092698A1
公开(公告)日：2023-03-23
申请号：US17789476
申请日：2019-12-27
发明人： Lianzhou Chen , Enzhong Zhang , Shaomin Sun , Zhonghai Cai , Shaoqing Gu
IPC分类号： C08L83/04 , C09K3/10 , B32B7/12 , H01M50/231 , H01M50/227 , H01M50/222 , H01M50/229 , H01M50/202
摘要： The two-part composition includes a first part and a second part. The first part includes a vinyl-substituted polysiloxane, a hydrosilylation catalyst, expandable graphite comprising moisture, and first polymeric microspheres having been at least partially coated with inorganic filler. The second part includes a second vinyl-substituted polysiloxane, a hydrosilyl-substituted polysiloxane, and second polymeric microspheres having been at least partially coated with flame-retardant inorganic filler. The two-part composition is useful, for example, for curing into a sealant and making an assembly. The assembly has a first substrate and a second substrate with a cured product of the two-part composition in contact with the first substrate and the second substrate. Methods of making a sealant and an assembly are also described.
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公开(公告)号：US20170362443A1
公开(公告)日：2017-12-21
申请号：US15525350
申请日：2015-12-22
发明人： Lianzhou Chen , Dmitriy Salnikov
IPC分类号： C09D5/00 , C09D163/00 , C08K5/098 , C08K5/544
CPC分类号： C09D5/002 , C08K5/098 , C08K5/544 , C09D163/00 , C08K5/0025 , C08K5/21 , C08K5/3445 , C08K3/36
摘要： A primer composition is presented comprising an aqueous dispersion of a) a thermosetting resin, b) an organosilane containing no hydrolyzable group, and c) a curing agent. In some embodiments, the primer composition additionally comprises d) a rare earth metal containing corrosion inhibitor. In some embodiments, the primer composition comprises no chromium. In some embodiments, the organosilane containing no hydrolyzable group is an aminosilanol. In some embodiments of the primer composition, the thermosetting resin is an epoxy resin and the curing agent is an epoxy curing agent. In some embodiments of the primer composition, the rare earth metal containing corrosion inhibitor is a cerium containing corrosion inhibitor.
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3.发明授权公开(公告)号：US09533935B2
公开(公告)日：2017-01-03
申请号：US14778644
申请日：2014-05-01
摘要： (Meth)acrylates are prepared in a single-step method from a mixture of (meth)acrylic acid and at least one biobased oil and/or its derivative(s), including at least one unsaturation. The (meth)acrylates are made by directly adding the (meth)acrylic acid to the biobased oil by reacting in the presence of an acid catalyst, including an inorganic or organic acid having at least one oxygen atom present thereon and which possesses at least one acid functionality having an ionization constant in water which is not greater than 3.
摘要翻译： （甲基）丙烯酸酯由（甲基）丙烯酸和至少一种生物基油和/或其衍生物的混合物（包括至少一种不饱和键）以单步法制备。 （甲基）丙烯酸酯通过在生物基油中直接加入（甲基）丙烯酸而制备，在酸催化剂存在下反应，所述酸催化剂包括其中存在至少一个氧原子的无机或有机酸，并且具有至少一个 在水中电离常数不大于3的酸官能团。
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公开(公告)号：US11958938B2
公开(公告)日：2024-04-16
申请号：US17918188
申请日：2021-04-09
CPC分类号： C08G59/184 , C08G59/3227 , C08G59/4253 , C08G59/504 , C09J163/00 , C09J2433/00
摘要： Provided is a curative part usable in a two-part curable composition. The curative part includes a liquid amine; a heterogeneous dispersant; and core-shell rubber particles having an elastomeric core and a (meth)acrylic shell. The core-shell rubber particles and the heterogeneous dispersant can be collectively shear-dispersed in the liquid amine such that the core-shell rubber particles are substantially non-aggregated and the curative part is phase-stable over a period of at least 3 months at ambient temperature. Advantageously, large amounts of core-shell rubber particles can thus be incorporated into a cured resin matrix, which can afford significantly enhanced impact performance.
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公开(公告)号：US20230017420A1
公开(公告)日：2023-01-19
申请号：US17781476
申请日：2020-12-11
发明人： Lianzhou Chen
IPC分类号： C09J163/00
摘要： Provided are two-part curable adhesives that can be suitable for use in industrial bonding applications, including aero-space and automotive bonding. The adhesives include a first part that contains an epoxy resin and a first oligomeric toughener. The adhesives further include a second part comprising a curative that is reactive with the epoxy resin at ambient conditions and a second oligomeric toughener. The first and second oligomeric tougheners are immiscible with each other at ambient conditions. Advantageously, the adhesives when cured can simultaneously display both high shear strength and high peel performance at elevated temperatures.
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公开(公告)号：US20220389236A1
公开(公告)日：2022-12-08
申请号：US17776187
申请日：2020-11-20
发明人： Lianzhou Chen
IPC分类号： C09D5/08 , C09D7/20 , C09D7/61 , C09D7/65 , C09D7/40 , C09D183/06 , C09D163/00
摘要： A one-part primer composition is provided. The one-part primer composition includes a first epoxy resin that is a liquid under ambient conditions a particulate corrosion inhibitor present in an amount of from 5 wt % to 30 wt % relative to the overall weight of the composition excluding carrier solvents and water, a curative comprising a primary aromatic amine, a silane coupling agent, a carrier solvent; and water homogeneously mixed with the carrier solvent and present in an amount sufficient to hydrolyze the silane coupling agent while preserving solubility of the first epoxy resin and curative in the carrier solvent/water mixture. The corrosion inhibitor is pre-dispersed in a liquid epoxy to break the agglomeration of the inhibitors, mitigate settling of the pigment and improve primer performance.
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公开(公告)号：US11485881B2
公开(公告)日：2022-11-01
申请号：US16767952
申请日：2018-12-14
发明人： Lianzhou Chen
摘要： Structural adhesive films are presented which comprise branched or networked polymers which are the reaction product of one or more polyether sulfone polymers, which may include amine-terminated polyether sulfone polymers and/or hydroxy-terminated polyether sulfone polymers, with epoxy-functional chemical species including the reaction product of one or more first polyepoxides with an amine-terminated branched polytetrahydrofuran polymer. The structural adhesive films may possess high strength, holding power and durability in high-temperature applications.
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公开(公告)号：US11370908B2
公开(公告)日：2022-06-28
申请号：US17052430
申请日：2019-06-25
发明人： Lianzhou Chen , Dmitriy Salnikov
IPC分类号： C08L63/00 , C09J7/35 , C08G59/24 , C08G59/38 , C08G59/50 , C08G59/60 , C08G75/029 , C08K3/08 , C08K5/18 , C08L81/06 , C08G59/40
摘要： Provided is a curable composition containing a reactive mixture of components including an polyethersulfone having a chemical group reactive with an epoxide, a cycloaliphatic polyepoxide resin, a polyepoxide having a functionality greater than two, a liquid diepoxide resin, a first curative containing 9,9-bis(aminophenyl)fluorene or a derivative therefrom and having a curing onset temperature of from 150° C. to 200° C. The components can further comprise a second curative having a curing onset temperature of from 60° C. to 180° C. When thermally curing this composition, the second epoxy curative starts to cure before the first epoxy curative, thereby inhibiting vertical flow of the adhesive during the curing process.
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公开(公告)号：US11279795B2
公开(公告)日：2022-03-22
申请号：US16492298
申请日：2018-06-26
发明人： Lianzhou Chen , Michael S. Newman
IPC分类号： C08G59/32 , C08G59/50 , C08F110/08 , C08L9/02 , C08L71/02
摘要： Provided are curable compositions including a base part comprising an amine-reactive curable resin and a curative part comprising a polymeric toughener dissolved in an amine. The polymeric toughener, optionally a rubbery polymer or thermoplastic polymer, is solid at ambient conditions with a weight average molecular weight of at least 5,000 g/mol while the amine is a liquid at ambient conditions. The curable composition is cured by mixing the base and curative parts with each other. Hardened compositions obtained thereof can achieve increased toughener loading, resulting in high peel and shear strength performance over a wide range of temperatures, including at temperatures exceeding 180° F. (82° C.).
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公开(公告)号：US20210130535A1
公开(公告)日：2021-05-06
申请号：US16492298
申请日：2018-06-26
发明人： Lianzhou Chen , Michael S. Newman
摘要： Provided are curable compositions including a base part comprising an amine-reactive curable resin and a curative part comprising a polymeric toughener dissolved in an amine. The polymeric toughener, optionally a rubbery polymer or thermoplastic polymer, is solid at ambient conditions with a weight average molecular weight of at least 5,000 g/mol while the amine is a liquid at ambient conditions. The curable composition is cured by mixing the base and curative parts with each other. Hardened compositions obtained thereof can achieve increased toughener loading, resulting in high peel and shear strength performance over a wide range of temperatures, including at temperatures exceeding 180° F. (82° C.).
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