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公开(公告)号：US5035756A
公开(公告)日：1991-07-30
申请号：US296162
申请日：1989-01-10
申请人： Josephine Covino
发明人： Josephine Covino
CPC分类号： C06B33/00 , F42B39/20 , Y10S149/114
摘要： A thermite mixture with a low autoignition temperature for venting ordnancease sidewalls during fuel fire, having increased density, tensile strength and elasticity.
摘要翻译： 具有低自燃温度的铝热混合物，用于在燃料火灾期间排出弹药壳侧壁，具有增加的密度，拉伸强度和弹性。
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公开(公告)号：US5329540A
公开(公告)日：1994-07-12
申请号：US51106
申请日：1993-03-31
摘要： A dye laser comprising a solid styate laser medium and a pumping energy sce, the laser medium comprising a lasing concentration of a water or alcohol soluble organic dye which is incorporated into a hydrolyzed silicon organometallic solution, and forming a gel which is dried to form a transparent silicate glass which is doped with the organic dye.
摘要翻译： 一种染料激光器，其包括固体苯乙烯激光介质和泵送能量源，所述激光介质包含引入水解或硅醇有机金属溶液的水或醇可溶性有机染料的激光浓度，并形成干燥形成 透明硅酸盐玻璃，其掺杂有机染料。
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公开(公告)号：US4637864A
公开(公告)日：1987-01-20
申请号：US846788
申请日：1986-03-28
IPC分类号： C25B1/00
CPC分类号： C25B1/00
摘要： This invention comprises a method of synthesizing ternary phosphide compos of the general formula M(II)M(IV)P.sub.2 by fused salt electrolysis in which a melt powder mixture containing phosphorus compounds is introduced into an electrolytic apparatus containing a liquid group II metal cathode and a group IV metal or semiconductor source. Electrolysis occurs under controlled conditions in which oxygen is excluded as an impurity to produce the desired ternary phosphide compounds.
摘要翻译： 本发明包括通过熔盐电解合成通式M（II）M（Ⅳ）P2的三元磷化合物的方法，其中将含有磷化合物的熔融混合物引入包含液体II族金属阴极的电解装置中， IV族金属或半导体源。 电解发生在控制条件下，其中排除氧作为杂质以产生所需的三元磷化合物。
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公开(公告)号：US6039929A
公开(公告)日：2000-03-21
申请号：US990261
申请日：1997-12-15
申请人： Ilzoo Lee , Josephine Covino
发明人： Ilzoo Lee , Josephine Covino
CPC分类号： C01B33/26
摘要： A process for producing monoclinic celsian comprising the steps of forming a mixture of an alkoxide of silica, an alkoxide of aluminum, and a salt of barium; adding a catalyst of a fluorine containing compound to the mixture; calcining the catalyzed mixture; and, heat treating the calcined mixture. This process uses a sol-gel process to progressively increase the amount of monoclinic phase in relation to the hexagonal celsian. Additionally, a process for producing monoclinic strontium aluminosilicate is disclosed.
摘要翻译： 一种生产单斜晶体的方法，包括以下步骤：形成二氧化硅的醇盐，铝的醇盐和钡盐的混合物; 向混合物中加入含氟化合物的催化剂; 煅烧催化混合物; 并对煅烧的混合物进行热处理。 该方法使用溶胶 - 凝胶法逐渐增加单斜晶相相对于六边形凝胶相的量。 另外，公开了一种生产单斜晶硅酸锶铝硅酸盐的方法。
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5.发明授权
公开(公告)号：US5376594A
公开(公告)日：1994-12-27
申请号：US104955
申请日：1993-08-02
CPC分类号： C04B35/4508 , C01G3/006
摘要： Process for preparing a high temperature superconductor such as yttrium bum copper oxides, by dissolving suitable proportions of hydrolyzable salts, oxides, or organometallic compounds of yttrium, barium and copper in an acid pH-controlled water-containing organic solvent such as methanol, and subjecting the resulting solution to ultrasonic energy or to an oxidation-reduction reaction, preferably while passing oxygen under a positive pressure through the solution, and precipitating a hydrolyzed precursor material. Such precursor material is then heated or annealed at temperatures between about 300.degree. C. and about 600.degree. C., also preferably in the presence of flowing oxygen, to produce the desired high temperature superconductor material.
摘要翻译： 通过将适当比例的可水解盐，氧化物或钇，钡和铜的有机金属化合物溶解在酸性pH控制的含水有机溶剂如甲醇中来制备高温超导体如钇钡铜氧化物的方法， 所得到的超声能量或氧化还原反应的溶液，优选在正压下通过溶液并使水解的前体材料沉淀。 然后将这种前体材料在约300℃至约600℃之间的温度下进行加热或退火，最好在流动的氧气的存在下加热或退火，以产生所需的高温超导体材料。
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公开(公告)号：US5262362A
公开(公告)日：1993-11-16
申请号：US901649
申请日：1992-06-22
CPC分类号： C03C25/107
摘要： A chemical coating consisting of a mixture of tetraethoxysilane (TEOS), AC.sub.4 H.sub.9).sub.3, LiOH, Ti(OC.sub.3 H.sub.7).sub.4, Zr( ).sub.2 C.sub.5 H.sub.7).sub.4, HNO.sub.3 for pH control, and glycerol which produces an environmentally protective barrier resistant to cracking or crazing to a glass fiber to which it is applied by the SOL-GEL process.
摘要翻译： 由四乙氧基硅烷（TEOS），Al（OC4H9）3，LiOH，Ti（OC3H7）4，Zr（）2C5H7）4，用于pH控制的HNO3的混合物组成的化学涂层和产生耐开裂的环境保护屏障的甘油 或者通过SOL-GEL方法对其施加的玻璃纤维进行龟裂。
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公开(公告)号：US5103678A
公开(公告)日：1992-04-14
申请号：US697351
申请日：1991-05-06
CPC分类号： G01N3/26 , G01M11/088 , G01N33/386
摘要： Apparatus for measuring peel force exerted on optical fiber being pulled m a bobbin upon which it is wound, the pull being in the direction of the longitudinal axis of the truncated-conically-shaped bobbin. One end of an elongaged lever arm holds the bobbin cantilevered from the bobbin end opposite that from which the optical fiber is pulled so that the bobbin is positioned generally horizontally over a horizontal base to which the opposite end of the lever arm is pivotally attached. An intermediate point on the arm beneath the bobbin is in contact with a load measuring device so that as the fiber is pulled any reaction by the arm upon the device provides a measure of the peel force upon the fiber.
摘要翻译： 用于测量施加在光纤上的剥离力的装置从被卷绕在其上的线轴上拉出，该拉力沿着截头圆锥形绕线筒的纵轴方向。 伸长的杠杆臂的一端保持从与被拉动的光纤相对的筒管端部悬臂的筒管，使得筒管大致水平地定位在水平底座上，杠杆臂的相对端枢转地附接到水平底座。 线轴下方的臂上的中间点与负载测量装置接触，使得当纤维被拉动时，手臂上的任何反作用力都能提供纤维上的剥离力的量度。
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公开(公告)号：US4728682A
公开(公告)日：1988-03-01
申请号：US781615
申请日：1985-09-30
申请人： Josephine Covino , Marian E. Hills
发明人： Josephine Covino , Marian E. Hills
CPC分类号： C01B17/20 , C01F17/00 , C01F17/0037 , C01G9/006 , C01P2002/70
摘要： Metal ternary sulfides of the general formula MM'.sub.2 S.sub.4 are synthesized by introducing stoichiometric amounts of nitrate precursors in concentrated nitric acid and heating to approximate dryness to yield a homogeneous powder mixture. The mixture is then exposed to a gaseous H.sub.2 S atmosphere under controlled conditions to produce the desired sulfide.
摘要翻译： 通过在浓硝酸中引入化学计量的硝酸盐前体并加热至近似干燥以合成粉末混合物，合成通式为MM'2S4的金属三元硫化物。 然后将混合物在受控条件下暴露于气态H 2 S气氛中以产生所需的硫化物。
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公开(公告)号：US5604438A
公开(公告)日：1997-02-18
申请号：US406213
申请日：1995-03-06
CPC分类号： G01N25/50 , G01N33/222
摘要： A high voltage differential is applied across two separated electrodes by aoltage supply. Between these electrodes is located a sample of the solid propellant or other energetic material. The voltage differential across the electrodes generates a spark of measurable voltage, current and time duration in the sample in order to foretell at what energy level sustained ignition of the sample occurs. This spark is measured by a voltage monitor which, upon reaching a predetermined level, sends a signal to a short-circuiting network. The short-circuiting network, after a predetermined time delay, shorts the electrical path across the electrodes thereby removing the voltage differential across the sample and ending the ignition test. An operator is then able to determine visually whether or not the spark of known voltage, current and time duration has created sustained ignition of the sample material. With this information much can be ascertained about the electrostatic hazards of energetic material, thereby making the handling of these materials less dangerous.
摘要翻译： 通过电压源在两个分离的电极之间施加高压差。 在这些电极之间设置固体推进剂或其他能量材料的样品。 电极两端的电压差会在样品中产生可测量的电压，电流和持续时间的火花，以便预测样品发生什么样的能量持续点燃。 该火花由电压监视器测量，电压监视器在达到预定水平时向短路网络发送信号。 在预定的时间延迟之后，短路网络使跨过电极的电路短路，从而消除了样品两端的电压差并结束点火测试。 然后，操作者能够目视确定已知电压，电流和持续时间的火花是否已经产生样品材料的持续点燃。 有了这些信息，可以确定高能材料的静电危害，从而使这些材料的处理更不危险。
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公开(公告)号：USH626H
公开(公告)日：1989-04-04
申请号：US892967
申请日：1986-08-04
申请人： Josephine Covino
发明人： Josephine Covino
IPC分类号： C04B35/111 , C04B35/19
CPC分类号： C04B35/19 , C04B35/111
摘要： A method of synthesizing ceramic oxides using the Sol-Gel process to control particle size distribution, crystal structure and to achieve the selective incorporation of transition metals within a ceramic oxide matrix in order to produce tailored oxides with specific particle morphology and near zero expansion optical ceramics.
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