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    Interfacial viscosification of aqueous solutions utilizing interpolymer complex
    2.
    发明授权
    Interfacial viscosification of aqueous solutions utilizing interpolymer complex 失效
    使用互聚物复合物的水溶液的界面粘度

    公开(公告)号：US4942189A

    公开(公告)日：1990-07-17

    申请号：US387184

    申请日：1989-07-31

    Applicant: Dennis G. Peiffer ,  Robert D. Lundberg ,  Ilan Duvdevani

    Inventor： Dennis G. Peiffer ,  Robert D. Lundberg ,  Ilan Duvdevani

    IPC: C08J3/00 ,  C08J3/07 ,  C08J3/09

    CPC classification number: C08J3/07 ,  C08J3/005 ,  C08J3/091 ,  Y10S524/924

    Abstract: The present invention relates to a process for the viscosification of an aqueous liquid which includes the steps of forming a solvent system of an organic liquid or oil and a polar cosolvent, the polar cosolvent being less than about 15 weight percent of the solvent system, a viscosity of the solvent system being less than about 1,000 cps; forming an interpolymer complex of neutralized sulfonated polymer (water insoluble) and copolymer of styrene/vinylpyridine in the solvent system to form a solution, a concentration of the water insoluble interpolymer complex polymer in the solution being about 0.01 to about 0.5 weight percent, a viscosity of the solution being less than about 200 cps; the admixing or contacting said solution with about 5 to about 500 volume percent water, the water being immiscible with the organic liquid and the polar cosolvent and interpolymer complex transferring from the organic liquid to the water phase, thereby causing the water phase to gel (i.e., thicken). The large increase in viscosity of the aqueous phase is directly attributed to the formation of a large number of minute water-filled particles dispersed in the continuous aqueous phase.

    Abstract translation: 本发明涉及一种水性液体的增稠方法，其包括形成有机液体或油和极性助溶剂的溶剂体系的步骤，极性助溶剂小于溶剂体系的约15重量％， 溶剂体系的粘度小于约1,000cps; 在溶剂体系中形成中和磺化聚合物（水不溶性）和苯乙烯/乙烯基吡啶的共聚物的互聚物络合物以形成溶液，溶液中水不溶性互聚物络合物聚合物的浓度为约0.01至约0.5重量％，粘度 的溶液小于约200cps; 将所述溶液与约5至约500体积％的水混合或接触，所述水与有机液体和极性共溶剂和互聚物复合物不混溶，从有机液体转移到水相，从而使水相凝胶化（即 ， 加粗）。 水相的粘度大幅度上升直接归因于形成分散在连续水相中的大量微小水分散的颗粒。

    Method for controlling viscosity of organic liquids and compositions thereof
    3.
    发明授权
    Method for controlling viscosity of organic liquids and compositions thereof 失效
    用于控制有机液体粘度的方法及其组合物

    公开(公告)号：US4737534A

    公开(公告)日：1988-04-12

    申请号：US720722

    申请日：1985-04-08

    Applicant: Robert D. Lundberg ,  Robert R. Phillips ,  Dennis G. Peiffer ,  Ilan Duvdevani

    Inventor： Robert D. Lundberg ,  Robert R. Phillips ,  Dennis G. Peiffer ,  Ilan Duvdevani

    IPC: C08J3/24 ,  C08L23/32 ,  C08L57/06 ,  C08K5/05 ,  C08K5/01 ,  C08L39/08 ,  C10M111/04

    CPC classification number: C08L23/32 ,  C08J3/246 ,  C08L57/06

    Abstract: The instant invention relates to a process for controlling the viscosity of organic liquids by incorporating in said liquid a minor amount of polymer complex, and optionally a cosolvent for the ionic groups of said polymer. The polymer complex comprises the reaction product of a metal neutralized sulfonated polymer and a basic nitrogen-containing polymer, wherein the polymer complex is substantially soluble in said organic liquid, and pendant sulfonate groups which are substantially insoluble in said organic liquid. The optional cosolvent is selected which will solubilize the pendant sulfonate groups and provide a reasonably homogeneous mixture of solvent, cosolvent and polymer complex. The preferred compositions prepared by the method of the instant invention comprise an organic liquid having a solubility parameter of from 6 to 10.5 in combination with a polymer complex containing from 0.2 up to 10.0 mole % sulfonate groups and nitrogen-containing groups, and optionally a nonvolatile alcohol or amine cosolvent.

    Abstract translation: 本发明涉及通过在所述液体中加入少量聚合物络合物和任选的所述聚合物的离子基团的共溶剂来控制有机液体的粘度的方法。 聚合物复合物包括金属中和的磺化聚合物和碱性含氮聚合物的反应产物，其中聚合物络合物基本上可溶于所述有机液体，以及基本上不溶于所述有机液体的侧链磺酸酯基团。 选择可选的共溶剂，其将溶解磺酸侧基，并提供溶剂，共溶剂和聚合物络合物的合理均匀的混合物。 通过本发明的方法制备的优选组合物包含溶解度参数为6至10.5的有机液体与含有0.2至10.0摩尔％磺酸盐基团和含氮基团的聚合物配合物以及任选的非挥发性的 醇或胺助溶剂。

    Method for controlling viscosity of organic liquids and compositions
    4.
    发明授权
    Method for controlling viscosity of organic liquids and compositions 失效
    控制有机液体和组合物粘度的方法

    公开(公告)号：US4715865A

    公开(公告)日：1987-12-29

    申请号：US806416

    申请日：1985-12-09

    Applicant: Kissho Kitano ,  Ilan Duvdevani ,  Donald N. Schulz

    Inventor： Kissho Kitano ,  Ilan Duvdevani ,  Donald N. Schulz

    IPC: C08F210/14 ,  C09K3/00 ,  C10L1/14 ,  C10L1/18 ,  C10L1/196 ,  C10L1/22 ,  C10L7/00

    CPC classification number: C10L1/1963 ,  C08F210/14 ,  C09K3/00 ,  C10L1/146 ,  C10L1/1973 ,  C10L1/2368

    Abstract: A method of viscosifying an organic liquid which comprises adding a sufficient quantity of a hydrolyzed Ziegler Natta-ester containing copolymer having a molecular weight of about 100,000 to about 10,000,000 to said organic liquid to increase the viscosity of said organic liquid, said copolymer having the formula: ##STR1## wherein R.sub.1 is an alkyl group having about 4 to about 6 carbon atoms, R.sub.2 is an alkylene group having about 3 to about 17 carbon atoms, x is about 95.0 to about 99.95 mole % and y is about 0.05 to about 5.0 mole %.

    Abstract translation: 一种增稠有机液体的方法，该方法包括向所述有机液体中加入足量的具有约100,000至约10,000,000分子量的含齐格列酮纳塔酯的共聚物，以增加所述有机液体的粘度，所述共聚物具有式 ：其中R 1为具有约4至约6个碳原子的烷基，R 2为具有约3至约17个碳原子的亚烷基，x为约95.0至约99.95摩尔％，y为约0.05至约5.0 摩尔％。

    Terpolymers of acrylamide, alkylacrylamide and betaine monomers
    5.
    发明授权
    Terpolymers of acrylamide, alkylacrylamide and betaine monomers 失效
    丙烯酰胺，烷基丙烯酰胺和甜菜碱单体的三元共聚物

    公开(公告)号：US4650848A

    公开(公告)日：1987-03-17

    申请号：US814252

    申请日：1985-12-30

    Applicant: Donald N. Schulz ,  Ilan Duvdevani ,  Jan Bock ,  Enock Berluche

    Inventor： Donald N. Schulz ,  Ilan Duvdevani ,  Jan Bock ,  Enock Berluche

    IPC: C08F220/56 ,  C08F20/56

    CPC classification number: C08F220/56

    Abstract: A water soluble terpolymer having the structure: ##STR1## wherein x is selected from the group consisting of ##STR2## wherein x is about 1 to about 95 mole percent; y is about 0.1 to about 5.0 mole percent; R.sub.1 is methyl or hydrogen; z is about 1 to about 30 mole percent; R.sub.2 is an alkyl group of 1-5 carbon atoms; R.sub.3 is an alkyl group of 3 to 4 carbon atoms; R.sub.4 is an alkyl group of 1-5 carbon atoms; and R.sub.5 is an alkyl group of 4-20.

    Abstract translation: 具有以下结构的水溶性三元共聚物：其中x选自由下列组成的组：其中x为约1至约95摩尔％; y为约0.1至约5.0摩尔％; R1是甲基或氢; z为约1至约30摩尔％; R2是1-5个碳原子的烷基; R3是3〜4个碳原子的烷基; R4是1-5个碳原子的烷基; R5为4-20的烷基。

    Antimisting system for hydrocarbon fluids
    6.
    发明授权
    Antimisting system for hydrocarbon fluids 失效
    碳氢化合物流体反倾销体系

    公开(公告)号：US4586937A

    公开(公告)日：1986-05-06

    申请号：US625973

    申请日：1984-06-29

    Applicant: Ilan Duvdevani ,  John A. Eckert ,  Donald N. Schulz ,  Kissho Kitano

    Inventor： Ilan Duvdevani ,  John A. Eckert ,  Donald N. Schulz ,  Kissho Kitano

    IPC: C08F210/14 ,  C10L1/14 ,  C10L1/18 ,  C10L1/196 ,  C10L1/22

    CPC classification number: C10L1/1963 ,  C08F210/14 ,  C10L1/146 ,  C10L1/1973 ,  C10L1/2368

    Abstract: An antimisting hydrocarbon solution comprising a hydrocarbon mixed with a copolymer of an alphaolefin and a vinyl alkylenecarboxylic acid, wherein the concentration of said copolymer in said hydrocarbon is about 0.05 to about 2 grams per 100 ml of said solution, wherein said copolymer has the formula: ##STR1## wherein R.sub.1 is an alkyl group having about 1 to about 25 carbon atoms, R.sub.2 is an alkylene group having about 3 to 17 carbon atoms, x is about 95.0 to about 99.99 mole % and y is about 0.01 to about 5 mole %.

    Abstract translation: 一种含有烃与α-烯烃和乙烯基亚烷基羧酸的共聚物混合的反应性烃溶液，其中所述烃中所述共聚物的浓度为每100ml所述溶液约0.05至约2克，其中所述共聚物具有下式： 其中R 1为具有约1至约25个碳原子的烷基，R 2为具有约3至17个碳原子的亚烷基，x为约95.0至约99.99摩尔％，y为约0.01至约5摩尔％ 。

    Blend compositions of sulfo EPDM's having improved compression set properties
    7.
    发明授权
    Blend compositions of sulfo EPDM's having improved compression set properties 失效
    具有改进的压缩永久变形特性的磺基EPDM的共混组合物

    公开(公告)号：US4543385A

    公开(公告)日：1985-09-24

    申请号：US566348

    申请日：1983-12-28

    Applicant: Pawan K. Agarwal ,  Ilan Duvdevani ,  Robert D. Lundberg

    Inventor： Pawan K. Agarwal ,  Ilan Duvdevani ,  Robert D. Lundberg

    IPC: C08L23/32 ,  C08L23/26

    CPC classification number: C08L23/32

    Abstract: This invention relates to extrusion and injection moldable type elastomeric compositions having improved compression set properties and having a viscosity at 200.degree. C. at 0.73 sec.sup.-1 of about 8.times.10.sup.3 to about 8.times.10.sup.5 poises. The compositions used for elastomeric articles include a major portion of neutralized sulfonated EPDM terpolymer and a minor portion of an unsulfonated EPDM terpolymer or EP copolymer and optionally less than about 150 parts by weight of a non-polar process oil per 100 parts of the sulfonated polymer; less than about 300 parts by weight of a filler per 100 parts of the sulfonated polymer; and a preferential plasticizer at about 1 to about 60 parts by weight per 100 parts of the sulfonated elastomeric polymer.These blend compositions can be readily processed due to their superior rheological properties on conventional plastic fabrication equipment into elastomeric articles having improved compression set properties characteristics.

    Abstract translation: 本发明涉及具有改进的压缩变定特性并且在200℃，0.73秒-1下的约8×10 3至约8×10 5泊的粘度的挤出和注射成型型弹性体组合物。 用于弹性体制品的组合物包括主要部分中和的磺化EPDM三元共聚物和少部分未磺化的EPDM三元共聚物或EP共聚物，以及任选地每100份磺化聚合物小于约150重量份的非极性加工油 ; 每100份磺化聚合物小于约300重量份的填料; 和每100份磺化弹性体聚合物约1至约60重量份的优选增塑剂。 这些共混组合物由于其在常规塑料制造设备上具有优异的流变性能而容易加工成具有改进的压缩永久变形特性特性的弹性体制品。

    Nonaqueous solvent soluble polyampholytes-viscosifier and shear thickening additive
    8.
    发明授权
    Nonaqueous solvent soluble polyampholytes-viscosifier and shear thickening additive 失效
    非水溶剂可溶性聚阴离子增稠剂和剪切增稠剂

    公开(公告)号：US4520158A

    公开(公告)日：1985-05-28

    申请号：US638302

    申请日：1984-08-06

    Applicant: Dennis G. Peiffer ,  Robert D. Lundberg ,  Ilan Duvdevani ,  Warren A. Thaler

    Inventor： Dennis G. Peiffer ,  Robert D. Lundberg ,  Ilan Duvdevani ,  Warren A. Thaler

    IPC: C08F8/44 ,  C08J3/09 ,  C10M151/02 ,  C08K5/01 ,  C08L39/00

    CPC classification number: C08J3/091 ,  C08F8/44 ,  C10M151/02 ,  C08J2325/08 ,  C10M2205/04 ,  C10M2217/028 ,  C10M2221/02

    Abstract: A process for increasing the viscosity of a hydrocarbon organic liquid under increasing shear rate which includes the step of:(a) forming a solution of said hydrocarbon organic liquid and a polyampholyte having about 1 to about 500 milliequivalents of sulfonate groups per 100 gms. of said polyampholyte, wherein the concentration of said polyampholyte is about 0.01 to about 20 wt. %, said polyampholyte having the formula: ##STR1## wherein X is about 40 to about 98 mole %, y is about 1 to about 50 mole %, and z is about 1 to about 50 mole %, wherein y and z are less than 60 mole %, and M is an amine or a metal cation selected from the group consisting of aluminum, iron, lead, Groups IA, IIA, IB and IIB of the Periodic Table of Elements; and(b) subjecting said solution to increasing shear rate to increase the viscosity of said solution by at least 10% as said shear rate increases.

    Abstract translation: 一种在增加的剪切速率下增加烃有机液体的粘度的方法，该方法包括以下步骤：（a）形成所述烃类有机液体的溶液和每100克具有约1至约500毫当量磺酸盐基团的多聚电解质。 的所述聚阴离子，其中所述聚阴离子的浓度为约0.01至约20wt。 ％，所述聚阴离子具有下式：其中X为约40至约98摩尔％，y为约1至约50摩尔％，z为约1至约50摩尔％，其中y和z小于 60摩尔％，M是选自元素周期表的铝，铁，铅，IA，IIA，IB和IIB族的胺或金属阳离子; 和（b）当所述剪切速率增加时，所述溶液经受所述溶液增加剪切速率以使所述溶液的粘度增加至少10％。

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