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公开(公告)号：US5756639A
公开(公告)日：1998-05-26
申请号：US666763
申请日：1996-06-19
摘要： A method for producing an epoxy polyetherpolyol having 15 to 75 wt. % epoxy comprising heating a polyol and catalyst to initiate condensation, removing water, introducing sufficient epoxy into the reaction mixture to give 15 to 75 wt. % epoxy in the product. Generally, between 0.5 and 1.19 moles of water per mole of polyol are removed. In one embodiment at least 95 wt. % of all of the polyol is introduced initially into the reaction zone. In another embodiment the condensation is terminated prior to 93 percent completion. Also provided are novel compositions suitable for drilling fluids, adhesives and coatings.
摘要翻译： 一种制备15〜75重量％的环氧聚醚多元醇的方法， ％环氧化物，包括加热多元醇和催化剂以引发缩合，除去水，将足够的环氧化合物引入反应混合物中，得到15至75wt。 ％环氧树脂在产品中。 通常，每摩尔多元醇除去0.5-1.19摩尔水。 在一个实施方案中，至少95wt。 所有的多元醇的百分数最初被引入反应区。 在另一个实施方案中，在完成93％之前终止冷凝。 还提供适用于钻井液，粘合剂和涂料的新型组合物。
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2.发明授权Process to prepare two phase foam compositions and two phase foam compositions 失效制备两相泡沫组合物和两相泡沫组合物的方法
公开(公告)号：US5646193A
公开(公告)日：1997-07-08
申请号：US560140
申请日：1995-11-17
申请人： Thomas Fairchild Brownscombe , Ronald Marshall Bass , Pui Kwan Wong , George Constantine Blytas , William Peter Gergen , Maryanne Mores
发明人： Thomas Fairchild Brownscombe , Ronald Marshall Bass , Pui Kwan Wong , George Constantine Blytas , William Peter Gergen , Maryanne Mores
CPC分类号： C08J9/283 , A61F13/15203 , A61L15/425
摘要： A process is provided for the production of a porous crosslinked polymeric foam comprising the steps of: (a) providing a first water-in-oil emulsion comprising (i) a first mixture of polymerizable monomers comprising at least one oil-soluble vinyl monomer and from about 2 to about 70 weight percent, based on the mixture, of a multifunctional unsaturated crosslinking monomer, (ii) at least 70 weight percent, based on the emulsion, of water as the internal phase (iii) an effective amount to produce the water-in-oil emulsion of a first surfactant, and (iv) a first polymerization initiator; (b) providing a second water-in-oil emulsion comprising (i) a mixture of polymerizable monomers comprising at least one oil-soluble vinyl monomer and from about 2 to about 70 weight percent, based on the mixture, of a second multifunctional unsaturated crosslinking monomer, (ii) at least 70 weight percent, based on the emulsion, of water as the internal phase (iii) an effective amount to produce the water-in-oil emulsion of a second surfactant, and (iv) a second polymerization initiator; (c) combining the first and second emulsions; and (d) curing said polymerizable monomers under conditions effective to polymerize and crosslink the polymer prior to significant diffusion between the emulsions. Polymeric foams can be prepared by this process that exhibit positive attributes of foams formed by curing of each of the emulsions individually.
摘要翻译： 提供了一种生产多孔交联聚合物泡沫体的方法，包括以下步骤：（a）提供第一种油包水乳液，其包含（i）包含至少一种油溶性乙烯基单体的可聚合单体的第一混合物和 基于该混合物，约2至约70重量％的多官能不饱和交联单体，（ii）基于乳液的至少70重量％的作为内相的水（iii）有效量的产生 第一表面活性剂的油包水乳液，和（iv）第一聚合引发剂; （b）提供第二种油包水乳液，其包含（i）包含至少一种油溶性乙烯基单体的可聚合单体和基于该混合物的约2-约70重量％的第二多官能不饱和单体的混合物 交联单体，（ii）基于乳液至少70重量％的作为内相的水（iii）有效量的产生第二表面活性剂的油包水乳液，和（iv）第二聚合 发起者 （c）组合第一和第二乳液; 和（d）在有效聚合和交联聚合物的条件下，在乳液显着扩散之前，使所述可聚合单体固化。 聚合物泡沫可以通过这种方法制备，其显示了通过单独固化每种乳液形成的泡沫的阳性。
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公开(公告)号：US5756772A
公开(公告)日：1998-05-26
申请号：US788486
申请日：1997-01-28
IPC分类号： C08G65/34 , C07D319/12
CPC分类号： C08G65/34 , Y02P20/127
摘要： Reduction of the adhesion of polyethercyclicpolyol (PECP) to metals by preparing the PECP by condensing polyol molecules by reactive distillation and replacing part of the polyol with an alcohol of lower hydroxyl content than the polyol.
摘要翻译： 通过聚合多元醇分子通过反应蒸馏制备PECP，通过用羟基含量低于多元醇的醇代替部分多元醇，来降低聚醚多元醇（PECP）对金属的粘附性。
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公开(公告)号：US5656576A
公开(公告)日：1997-08-12
申请号：US341713
申请日：1994-11-18
CPC分类号： C09K8/06
摘要： Reducing the adherence of polyethercyclicpolyol to metal by exposing the metal to a selected surfactant.
摘要翻译： 通过将金属暴露于选定的表面活性剂来降低聚醚多环多元醇对金属的粘附性。
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公开(公告)号：US07033504B1
公开(公告)日：2006-04-25
申请号：US10130855
申请日：2000-11-21
IPC分类号： B01D11/04
CPC分类号： B01D17/047 , C02F1/26 , C02F2101/32
摘要： Disclosed is a method for recovering and re-employing ionic surfactants from solutions, dispersions and emulsions of water and liquid hydrocarbons, by the addition of a second non-aqueous polar phase and an inorganic salt which changes the ionic strength of the surfactant and causes the surfactant to partition principally into the non-aqueous second polar phase. More specifically, the method applies to recovering hydrate growth inhibitor/modifying compounds, with cationic surfactants such as ammonium, phosphonium and sulphonium alkylated compounds from the effluent of hydrocarbon production wells; the effluent including water, hydrate inhibitor compound, at least one additional polar solvent and inorganic salt. Sufficient additional ions of inorganic salt, and if necessary, an alcohol/glycol are added to the effluent to form a second polar phase that is less polar than the aqueous phase, into which the hydrate inhibitor can then dissolve and be separated from the effluent.
摘要翻译： 公开了一种通过添加第二非水极性相和无机盐从溶液，分散体和水和液体烃的乳液中回收和重新使用离子表面活性剂的方法，其改变了表面活性剂的离子强度，并导致 表面活性剂主要分配到非水的第二极性相中。 更具体地说，该方法适用于从烃生产井的流出物中回收水合物生长抑制剂/改性化合物与阳离子表面活性剂如铵，鏻和锍烷基化化合物; 流出物包括水，水合物抑制剂化合物，至少一种另外的极性溶剂和无机盐。 向流出物中加入足够的无机盐附加离子和必要时的醇/二醇以形成比水相极性低的第二极性相，然后水合物抑制剂可溶解并与流出物分离。
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