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    Glyoxal free purified cationic polygalactomannan
    1.
    发明授权
    Glyoxal free purified cationic polygalactomannan 有权
    无乙二醛纯化阳离子聚半乳甘露聚糖

    公开(公告)号：US08580952B2

    公开(公告)日：2013-11-12

    申请号：US12986785

    申请日：2011-01-07

    申请人： Ugo Pfeiffer ,  Mauro Tenconi ,  Eva Baldaro ,  Valentina Langella ,  Giovanni Floridi ,  Giuseppe Li Bassi

    发明人： Ugo Pfeiffer ,  Mauro Tenconi ,  Eva Baldaro ,  Valentina Langella ,  Giovanni Floridi ,  Giuseppe Li Bassi

    IPC分类号： C08B37/00 ,  C07H1/00 ,  C07H3/00

    CPC分类号： C08B37/0087 ,  C08B37/0096

    摘要： A glyoxal and boron free purified cationic polygalactomannan may be prepared by reacting a polygalactomannan flour, a nonionically derivatized polygalactomannan flour, or a mixture thereof, with a cationising reagent, adjusting the pH to be from about 4 to about 6; cross-linking the cationic with glyoxal, and filtering and water washing the cationic polygalactomannan to produce a glyoxalated purified cationic polygalactomannan containing not more than 70% by weight of water. In some cases it may be desirable to introduce a buffering agent to the glyoxalated purified cationic polygalactomannan to regulate the pH to from 8.0 to about 9.5, when measured at 1% (dry matter) in water. In other cases, it may be desirable to remove water to produce glyoxal free purified cationic polygalactomannan in powder form. Such compounds are particularly useful in personal care products.

    摘要翻译： 乙二醛和无硼纯化的阳离子聚半乳甘露聚糖可以通过使聚半乳甘露聚糖粉末，非离子衍生化的聚半乳甘露聚糖粉末或其混合物与阳离子化试剂反应来制备，将pH调节至约4至约6; 将阳离子与乙二醛交联，并过滤并水洗阳离子聚半乳甘露聚糖以产生含有不超过70重量％水的乙二醛纯化阳离子聚半乳甘露聚糖。 在一些情况下，当在水中以1％（干物质）测量时，可能需要向乙醛酸化的纯化阳离子聚半乳甘露聚糖引入缓冲剂以将pH调节至8.0至约9.5。 在其他情况下，可能需要除去水以产生无乙醛酸的纯化的粉末形式的阳离子聚半乳甘露聚糖。 这些化合物特别适用于个人护理产品。

    PROCEDURE FOR THE PREPARATION OF GLYOXALATED CATIONIC GUAR
    2.
    发明申请
    PROCEDURE FOR THE PREPARATION OF GLYOXALATED CATIONIC GUAR 审中-公开
    制备GLYOXALATED阳离子防护眼镜的程序

    公开(公告)号：US20100004197A1

    公开(公告)日：2010-01-07

    申请号：US12515526

    申请日：2007-04-17

    申请人： Eva Baldaro ,  Mauro Tenconi ,  Giuseppe Li Bassi

    发明人： Eva Baldaro ,  Mauro Tenconi ,  Giuseppe Li Bassi

    IPC分类号： A61K8/73 ,  C08B37/00 ,  C11D1/66

    CPC分类号： C08B37/0096 ,  A61K8/737 ,  A61K2800/5426 ,  A61Q19/00 ,  C11D3/227

    摘要： Procedure for the preparation of cationic guar having DS comprised between 0.01 and 3, soluble at basic pH and suitable for the use in the cosmetic field and in household cleaning products comprising the following steps: a) 100 parts by weight of guar flour are reacted with 3-chloro-2-hydroxypropyl trimethylammonium chloride and sodium hydroxide, in from 5 to 500 parts of a water and alcohol mixture containing from 20 to 50% by weight of water; b) the mixture is acidified to a pH between 4 and 6; c) from 2.2 to 3 parts by weight of glyoxal are added, and the reaction is stirred for approximately 30 minutes; d) from 300 to 1200 parts by weight of ambient temperature water are added and mixed for 10 to 90 minutes; e) the mixture is filtered under vacuum and the product dried to obtain glyoxalated purified cationic guar.

    摘要翻译： 制备DS为0.01至3的阳离子瓜尔胶的程序，在碱性pH下可溶，适于在化妆品领域和家用清洁产品中使用，包括以下步骤：a）将100重量份瓜耳粉与 3-氯-2-羟基丙基三甲基氯化铵和氢氧化钠，其含量为5至500份含有20至50重量％水的水和醇混合物; b）将混合物酸化至4至6之间的pH; c）2.2〜3重量份乙二醛加入，将反应物搅拌约30分钟; d）从300至1200重量份的环境温度加入水并混合10至90分钟; e）将混合物在真空下过滤，产物干燥，得到乙醛酸化的纯化阳离子瓜尔胶。

    Procedure for the preparation of purified cationic guar
    4.
    发明授权
    Procedure for the preparation of purified cationic guar 有权
    制备纯化的阳离子瓜尔胶的方法

    公开(公告)号：US08501932B2

    公开(公告)日：2013-08-06

    申请号：US12515528

    申请日：2007-04-17

    申请人： Eva Baldaro ,  Raffaella Pelizzari ,  Mauro Tenconi ,  Giuseppe Li Bassi

    发明人： Eva Baldaro ,  Raffaella Pelizzari ,  Mauro Tenconi ,  Giuseppe Li Bassi

    IPC分类号： C08B37/00

    CPC分类号： C08B37/0096 ,  C11D3/227

    摘要： Procedure for the preparation of cationic guar having DS comprised between 0.01 and 3, free from boron and suitable for the use in the cosmetic field and in household cleaning products, comprising the following steps: a) 100 parts by weight of guar flour are reacted with 3-chloro-2-hydroxypropyl trimethylammonium chloride and sodium hydroxide in from 5 to 500 parts by weight of a water and alcohol mixture containing from 20 to 50% by weight of water; b) the amount of water and alcohol is regulated in order to obtain a dispersion containing from 65 to 95% by weight of a of water and alcohol mixture containing from 30 to 50% by weight of water and the dispersion is maintained under stirring at temperature comprised between 15 and 40° C. for at least 10 minutes; c) the mixture is filtered under vacuum and dried to obtain the purified cationic guar.

    摘要翻译： 制备DS含量为0.01至3，不含硼并适用于化妆品领域和家用清洁产品的DS的阳离子瓜尔胶的方法，包括以下步骤：a）将100重量份瓜耳粉与 5-氯-2-羟基丙基三甲基氯化铵和氢氧化钠，其含量为5至500重量份含有20至50重量％水的水和醇混合物; b）调节水和醇的量以获得含有65至95重量％的含有30至50重量％水的水和醇混合物的分散体，并将分散体在温度下保持搅拌 在15至40℃之间至少10分钟; c）将混合物在真空下过滤并干燥，得到纯化的阳离子瓜尔胶。

    GLYOXAL FREE PURIFIED CATIONIC POLYGALACTOMANNAN
    5.
    发明申请
    GLYOXAL FREE PURIFIED CATIONIC POLYGALACTOMANNAN 有权
    GLYOXAL FREE PURIFIED CTICIC POLYGALACTOMANNAN

    公开(公告)号：US20110166341A1

    公开(公告)日：2011-07-07

    申请号：US12986785

    申请日：2011-01-07

    申请人： Ugo Pfeiffer ,  Mauro Tenconi ,  Eva Baldaro ,  Valentina Langella ,  Giovanni Floridi ,  Giuseppe Li Bassi

    发明人： Ugo Pfeiffer ,  Mauro Tenconi ,  Eva Baldaro ,  Valentina Langella ,  Giovanni Floridi ,  Giuseppe Li Bassi

    IPC分类号： C08B37/00

    CPC分类号： C08B37/0087 ,  C08B37/0096

    摘要： A glyoxal and boron free purified cationic polygalactomannan may be prepared by reacting a polygalactomannan flour, a nonionically derivatized polygalactomannan flour, or a mixture thereof, with a cationising reagent, adjusting the pH to be from about 4 to about 6; cross-linking the cationic with glyoxal, and filtering and water washing the cationic polygalactomannan to produce a glyoxalated purified cationic polygalactomannan containing not more than 70% by weight of water. In some cases it may be desirable to introduce a buffering agent to the glyoxalated purified cationic polygalactomannan to regulate the pH to from 8.0 to about 9.5, when measured at 1% (dry matter) in water. In other cases, it may be desirable to remove water to produce glyoxal free purified cationic polygalactomannan in powder form. Such compounds are particularly useful in personal care products.

    摘要翻译： 乙二醛和无硼纯化的阳离子聚半乳甘露聚糖可以通过使聚半乳甘露聚糖粉末，非离子衍生化的聚半乳甘露聚糖粉末或其混合物与阳离子化试剂反应来制备，将pH调节至约4至约6; 将阳离子与乙二醛交联，并过滤并水洗阳离子聚半乳甘露聚糖以产生含有不超过70重量％水的乙二醛纯化阳离子聚半乳甘露聚糖。 在一些情况下，当在水中以1％（干物质）测量时，可能需要向乙醛酸化的纯化阳离子聚半乳甘露聚糖引入缓冲剂以将pH调节至8.0至约9.5。 在其他情况下，可能需要除去水以产生无乙醛酸的纯化的粉末形式的阳离子聚半乳甘露聚糖。 这些化合物特别适用于个人护理产品。