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    Quinacridone mixed-crystal pigments of the gamma phase
    2.
    发明授权
    Quinacridone mixed-crystal pigments of the gamma phase 有权
    喹吖啶酮混合晶体颜料的γ相

    公开(公告)号：US06312512B1

    公开(公告)日：2001-11-06

    申请号：US09482171

    申请日：2000-01-12

    申请人： Manfred Urban ,  Martin Boehmer ,  Joachim Weber ,  Dieter Schnaitmann ,  Margit Haberlick

    发明人： Manfred Urban ,  Martin Boehmer ,  Joachim Weber ,  Dieter Schnaitmann ,  Margit Haberlick

    IPC分类号： C09B4800

    CPC分类号： C09D11/32 ,  C09B48/00 ,  C09B67/0027 ,  C09B67/0036

    摘要： The invention relates to novel quinacridone mixed crystal pigments consisting of a) from 82.5 to 99% by weight of unsubstituted &ggr;-phase quinacridone of the formula (I) in which R1 and R2 are hydrogen atoms and b) from 1 to 17.5% by weight of one or more 2,9- and/or 3,10-substituted quinacridones of the formula (I) in which the substituents R1 and R2 are identical or different and are chlorine, bromine or fluorine atoms or C1-C4-alkyl, C1-C4-alkoxy or carboxamido groups which can be substituted by C1-C6-alkyl groups, and R1 can additionally be a hydrogen atom, and to pigment preparations comprising said quinacridone mixed crystal pigments.

    摘要翻译： 本发明涉及由以下组成的新颖的喹吖啶酮混合晶体颜料：a）82.5-99重量％的式（I）的未取代的γ-相喹吖啶酮，其中R 1和R 2是氢原子，和b）1至17.5重量％ 或更多的式（I）的2,9-和/或3,10-取代的喹吖啶酮，其中取代基R 1和R 2相同或不同，并且是氯，溴或氟原子或C 1 -C 4烷基，C 1 -C 4 可以被C1-C6烷基取代的烷氧基或甲酰氨基，R1可以另外是氢原子，以及包含所述喹吖啶酮混合晶体颜料的颜料制剂。

    Water-soluble perylene dyestuffs, their preparation and their use
    3.
    发明授权
    Water-soluble perylene dyestuffs, their preparation and their use 失效
    水溶性苝染料，其制备及其用途

    公开(公告)号：US5948910A

    公开(公告)日：1999-09-07

    申请号：US935098

    申请日：1997-09-25

    申请人： Wolfgang Bauer ,  Dieter Baumgart ,  Dieter Schnaitmann ,  Klaus-Peter Kreutzer ,  Walter Zoller

    发明人： Wolfgang Bauer ,  Dieter Baumgart ,  Dieter Schnaitmann ,  Klaus-Peter Kreutzer ,  Walter Zoller

    IPC分类号： C09B57/08 ,  C09B5/62 ,  C09D11/328 ,  D21H21/28 ,  C09B3/18 ,  C07D401/14

    CPC分类号： C09D11/328 ,  C09B5/62 ,  D21H21/28

    摘要： Water-soluble perylene dyestuffs, their preparation and their useThe present Application relates to water-soluble perylene dyestuffs of the formula ##STR1## in which R.sup.1 and R.sup.2 independently of one another are the radicals A--X--COOM or A--X--SO.sub.3 M;R.sup.3 and R.sup.4 independently of one another are the radicals R.sup.1 or R.sup.2, or are OR.sup.5 or NR.sup.6 R.sup.7 ;A is NR.sup.8 or S;X is a straight-chain or branched alkylene radical, a straight-chain or branched alkylene radical which is substituted by hydroxyl, carboxyl or amino, an arylene radical or an arylene radical which is optionally substituted by hydroxyl, carboxyl or sulfo;R.sup.5, R.sup.6 and R.sup.7 independently of one another are hydrogen, (C.sub.1 -C.sub.4)-alkyl or (C.sub.1 -C.sub.4)-alkyl which is substitituted by one or more hydroxyl, 2-hydroxyethoxy, (C.sub.1 -C.sub.4)-alkoxy or amino groups;R.sup.8 is hydrogen, methyl or ethyl andM is a monovalent cation or one equivalent of a polyvalent cation,processes for their preparation, their use for dyeing and printing naturally occurring and synthetic fiber materials, and recording liquids, in particular for the ink-jet process, and liquid formulations for dyeing paper in the pulp which comprise the dyestuffs according to the invention.

    摘要翻译： 水溶性苝染料及其制备及其用途本申请涉及下式的水溶性苝染料，其中R1和R2彼此独立地为基团A-X-COOM或A-X-SO3M; R 3和R 4彼此独立地是基团R 1或R 2，或者是OR 5或NR 6 R 7; A是NR8或S; X是直链或支链亚烷基，被羟基，羧基或氨基取代的直链或支链亚烷基，任选被羟基，羧基或磺基取代的亚芳基或亚芳基; R5，R6和R7彼此独立地是氢，（C1-C4） - 烷基或被一个或多个羟基，2-羟基乙氧基，（C1-C4） - 烷氧基或氨基取代的（C1-C4） - 烷基 ; R8是氢，甲基或乙基，M是一价阳离子或一当量的多价阳离子，其制备方法，它们用于染色和印刷天然存在的和合成的纤维材料，以及记录液体，特别是用于喷墨 工艺和用于在包含根据本发明的染料的纸浆中染色纸的液体制剂。

    Process for preparing linear unsubstituted .beta.-phase quinacridone pigments
    4.
    发明授权
    Process for preparing linear unsubstituted .beta.-phase quinacridone pigments 失效
    线性无取代β相喹吖啶酮颜料的制备方法

    公开(公告)号：US5755874A

    公开(公告)日：1998-05-26

    申请号：US834725

    申请日：1997-04-01

    申请人： Manfred Urban ,  Dieter Schnaitmann

    发明人： Manfred Urban ,  Dieter Schnaitmann

    IPC分类号： C09B67/20 ,  C09B67/52 ,  C09B48/00

    CPC分类号： C09B67/0027

    摘要： Process for preparing linear unsubstituted .beta.-phase quinacridone pigments A process for preparing linear unsubstituted .beta.-phase quinacridone pigments or pigment preparations, which comprises a) cyclizing 2,5-dianilinoterephthalic acid in polyphosphoric acid or polyphosphoric ester with a phosphorus pentoxide content of at least 84% by weight to form the quinacridone, b) subsequently hydrolyzing this quinacridone with water or with an aqueous mineral acid solution, preferably orthophosphoric acid solution, at a temperature of at least 40.degree. C., preferably from 60.degree. to 105.degree. C., to form the crude quinacridone pigment which is predominantly in the .alpha.-phase, c) then heating the crude .alpha.-phase quinacridone pigment to a temperature between 120.degree. and 200.degree. C. in the presence of a from 0.1 to 3% strength by weight, preferably from 0.2 to 2% strength by weight, inorganic base in water and alkali-stable organic solvents, for the change of phase into coarsely crystalline crude .beta.-phase pigment, and d) subjecting the coarsely crystalline crude .beta.-phase quinacridone pigment, for the fine division to form a pigment or prepigment, to dry or wet milling; and then isolating the resulting finely divided .beta.-phase pigment; e) or subjecting the finely divided .beta.-phase prepigment obtained in d) to a finish treatment in the presence of solvents, and then isolating the pigment.

    摘要翻译： 制备线性未取代的β-相喹吖啶酮颜料的方法制备线型未取代的β-相喹吖啶酮颜料或颜料制剂的方法，其包括：a）使多磷酸或多磷酸中的2,5-二苯胺基对苯二甲酸至少在五氧化二磷含量至少 84重量％以形成喹吖啶酮，b）随后用水或无机酸水溶液（优选正磷酸溶液）在至少40℃，优选60℃至105℃的温度下水解该喹吖啶酮。 ，以形成主要在α相中的粗喹吖啶酮颜料，c）然后在0.1至3％的强度存在下，将粗α-相喹吖啶酮颜料加热至120至200℃的温度， 重量，优选0.2-2％重量，无机碱在水和碱稳定的有机溶剂中，用于将相变为粗结晶的Cr udeβ相色素，和d）将粗结晶粗β相喹吖啶酮颜料进行细分，形成颜料或指色剂进行干或湿磨; 然后分离得到的细碎的β-相色素; e）或在d）中得到的细碎的β-相指示剂在溶剂存在下进行最终处理，然后分离颜料。

    Surface-treated quinacridone and dioxazine pigments
    5.
    发明授权
    Surface-treated quinacridone and dioxazine pigments 失效
    表面处理的喹吖啶酮和二恶嗪颜料

    公开(公告)号：US5746820A

    公开(公告)日：1998-05-05

    申请号：US837720

    申请日：1997-04-22

    申请人： Manfred Urban ,  Dieter Schnaitmann

    发明人： Manfred Urban ,  Dieter Schnaitmann

    IPC分类号： C09B67/14 ,  C09B67/08 ,  C09B67/20 ,  C09C3/08 ,  C09D7/12 ,  C09C1/02 ,  C08K5/00 ,  C08K5/34 ,  C09B48/00

    CPC分类号： C09B67/0009 ,  C09B67/0065

    摘要： The use of sulfuric monoesters of the formulae (I) and (II) R.sup.1 --O--(CH.sub.2 O).sub.n --SO.sub.3 .sup.- M.sup.+ (I) R.sup.1 --CO--NR.sup.2 --(CH.sub.2 O)(.sub.n+1)--SO.sub.3 .sup.- M.sup.+ (II) in which R.sup.1 is a straight-chain or branched alkyl group of 10 to 24 carbon atoms, R.sup.2 is a hydrogen atom or a C.sub.1 -C.sub.6 -alkyl group, M.sup.+ is a hydrogen ion, an alkali metal ion, 1/2 an alkaline earth metal ion, or an ammonium ion of the formula N.sup.+ R.sup.3 R.sup.4 R.sup.5 R.sup.6, where the substituents R.sup.3, R.sup.4, R.sup.5 and R.sup.6 independently of one another are each hydrogen atoms or C.sub.1 -C.sub.6 -alkyl groups, which alkyl groups can be substituted by 1 to 3 hydroxyl groups, and n is a number from 0 to 4; or of a mixture of at least two sulfuric monoesters of the formulae (I) and/or (II), for preparing surface-treated pigments from the classes of the quinacridones and dioxazines.

    摘要翻译： 式（I）和（II）的硫酸单酯使用R 1 -O-（CH 2 O）n -SO 3 -M +（I）R 1 -CO-NR 2 - （CH 2 O）（n + 1）-SO 3 -M + ），其中R 1是10-24个碳原子的直链或支链烷基，R2是氢原子或C1-C6烷基，M +是氢离子，碱金属离子，+ E， / 2 + EE为碱土金属离子，或式N + R3R4R5R6的铵离子，其中取代基R 3，R 4，R 5和R 6彼此独立地为氢原子或C 1 -C 6 - 烷基，该烷基 可以被1〜3个羟基取代，n为0〜4的数。 或由式（I）和/或（II）的至少两种硫酸单酯的混合物制备用于由喹吖啶酮和二恶嗪类制备表面处理的颜料。

    Pasty pigment preparations, preparation thereof and use thereof
    6.
    发明授权
    Pasty pigment preparations, preparation thereof and use thereof 失效
    调味色素制剂，其制备及其用途

    公开(公告)号：US5645636A

    公开(公告)日：1997-07-08

    申请号：US333886

    申请日：1994-11-03

    申请人： Manfred Schneider ,  Rainer Schunck ,  Dieter Schnaitmann ,  Udo Brost

    发明人： Manfred Schneider ,  Rainer Schunck ,  Dieter Schnaitmann ,  Udo Brost

    IPC分类号： C09B67/00 ,  C09B67/20 ,  C09D11/037 ,  C09D17/00 ,  C08K5/16

    CPC分类号： C09D11/037 ,  C09B67/0021 ,  C09B67/006

    摘要： The deliveries to the printing ink industry of pigment preparations in the form of flushed pastes increasingly take the form of containers. Given the required high pigment content of the pastes and the attendant high viscosity and thixotropy, there are very frequent problems with filling the containers and complaints concerning the emptying of the containers. There is a demand for a homogeneous, pumpable pigment paste having a long shelf life. According to the invention, this demand is met in the case of pigments based on arylpararosanillnesulfonic acids by the use of specific aids of the type of the condensation products of aliphatic amines or ammonium compounds with polyesters of hydroxy fatty acids as part of the flushing process of the pigment using the customary or slightly modified binder systems which for the same pigment contents bring about a distinctly lower viscosity and thixotropy. The printing properties are not adversely affected.

    摘要翻译： 以冲洗浆料形式向印刷油墨行业的色素制剂的交付越来越多地以容器的形式出现。 鉴于糊料所需的高颜料含量和伴随的高粘度和触变性，填充容器和关于容器排空的投诉存在非常频繁的问题。 需要具有长的保存期限的均匀的，可泵送的颜料浆料。 根据本发明，在通过使用脂肪族胺或铵化合物与羟基脂肪酸的聚酯的缩合产物类型的特定助剂作为冲洗过程的一部分的情况下，在基于芳基罗拉尼尼亚磺酸的颜料的情况下满足该需求 对于相同的颜料含量，使用常规或稍微改性的粘合剂体系的颜料导致明显较低的粘度和触变性。 印刷性能不会受到不利影响。

    Use of mixed-crystal pigments of the quinacridone series in electrophotographic toners and developers, powder coatings and inkjet inks
    8.
    发明授权
    Use of mixed-crystal pigments of the quinacridone series in electrophotographic toners and developers, powder coatings and inkjet inks 有权
    在电子照相调色剂和显影剂，粉末涂料和喷墨油墨中使用喹吖啶酮系列的混合颜料

    公开(公告)号：US06251553B1

    公开(公告)日：2001-06-26

    申请号：US09447519

    申请日：1999-11-23

    申请人： Ruediger Baur ,  Manfred Urban ,  Hans-Tobias Macholdt ,  Dieter Schnaitmann ,  Martin Boehmer

    发明人： Ruediger Baur ,  Manfred Urban ,  Hans-Tobias Macholdt ,  Dieter Schnaitmann ,  Martin Boehmer

    IPC分类号： G03G908

    CPC分类号： C09D11/32 ,  C09D5/035 ,  G03G9/092 ,  G03G9/122

    摘要： The use of mixed-crystal pigments of the quinacridone series consisting of a) from 85 to 99% by weight of unsubstituted &bgr;-phase quinacridone of the formula (I) in which R1 and R2 are hydrogen atoms, and b) from 1 to 15% by weight of one or more substituted quinacridones of the formula (I) in which the substituents R1 and R2 are identical or different and are chlorine, bromine or fluorine atoms or C1-C4-alkyl, C1-C4-alkoxy or carboxamido groups, which can be substituted by C1-C6-alkyl groups, and R1 can additionally be hydrogen, as colorants in electrophotographic toners and developers, powder coating materials, inkjet inks, electret fibers, and color filters.

    摘要翻译： 使用由以下组成的喹吖啶酮系列的混合颜料：a）85〜99重量％的式（I）的未取代的β相喹吖啶酮，其中R 1和R 2为氢原子，b）为1〜15％ 取代基R 1和R 2相同或不同并且为氯，溴或氟原子的一个或多个取代的式（I）喹吖啶酮的重量或C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基或甲酰胺基，其可以是 被C1-C6烷基取代，R1可以另外是氢，作为电子照相色调剂和显影剂中的着色剂，粉末涂料，喷墨油墨，驻极体纤维和滤色器。

    Process for the preparation of liquid pigment preparations
    9.
    发明授权
    Process for the preparation of liquid pigment preparations 失效
    液体颜料制剂的制备方法

    公开(公告)号：US5800607A

    公开(公告)日：1998-09-01

    申请号：US675448

    申请日：1996-07-03

    申请人： Dieter Schnaitmann ,  Martin Bohmer ,  Manfred Urban

    发明人： Dieter Schnaitmann ,  Martin Bohmer ,  Manfred Urban

    IPC分类号： C09B67/04 ,  C09B67/00 ,  C09B67/20 ,  C09B67/50

    CPC分类号： C09B67/0022

    摘要： Process for the preparation of pigment preparations, which comprises wet milling the crude pigments which are present in coarsely crystalline state, or prepigments or pigments which are present in a form in which they are difficult to disperse, in a concentration of from 20 to 60% by weight based on the total weight of the pigment preparation, in a flocculation-stable liquid medium and in a stirred ball mill which is operated with a peripheral stirrer speed of more than 12 m/s, under the action of nonmetallic grinding media with a diameter of less than or equal to 1.0 mm, until the desired degree of fine division is reached, and then isolating the pigment preparation.

    摘要翻译： 用于制备颜料制剂的方法，其包括湿法研磨以粗结晶状态存在的粗颜料或以其难以分散的形式存在的指示剂或颜料，浓度为20至60％ 基于颜料制剂的总重量，在絮凝稳定的液体介质中和在外部搅拌器速度大于12m / s的条件下操作的搅拌式球磨机中，在非金属研磨介质的作用下， 直径小于或等于1.0mm，直至达到所需的微细分割程度，然后分离颜料制剂。