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    Ether compounds as inhalant anesthetics
    1.
    发明授权
    Ether compounds as inhalant anesthetics 失效
    醚化合物作为吸入麻醉剂

    公开(公告)号：US3962460A

    公开(公告)日：1976-06-08

    申请号：US498975

    申请日：1974-08-20

    申请人： Louise S. Croix ,  Alex J. Szur

    发明人： Louise S. Croix ,  Alex J. Szur

    IPC分类号： C07C43/12 ,  A61K31/08

    CPC分类号： C07C43/12 ,  C07C43/123

    摘要： Aliphatic ether compounds having a formula selected from the group consisting of ##EQU1## wherein each of a and d is 2 or 3; each of b, c, e, i, j and k is 0 or 1; each of f and g is 0, 1, 2, or 3; h is 0, 1, or 2; a + b + = 3; d + e = 3; f + g + h = 3; i + j + k = 1; and X is F or Cl; with the provisos that when a and d are both 3, then i is 1, f is 0, 1, or 2, and g is 0, 1, or 3; when g is 2, then f is 1; when c is 1, then f is 3 and k is 0; when j is 1, then c is 1; and when both b and e are 1, then i is 1, are useful as solvents and dispersants for fluorinated materials. In addition, the compounds methyl 1-bromo-1,1,2,3,3,3-hexafluoroisopropyl ether and methyl 1,2-dichloro-1,1,3,3,3-pentafluoroisopropyl ether are useful as inhalation anesthetics.

    摘要翻译： 具有选自CFaClbBrcCF2 | PARALLEL FiBrjClkC-O-CHfClgFh和C-O-CH3 || CFdCleCF2X的式的脂族醚化合物，其中a和d各自为2或3; b，c，e，i，j和k中的每一个为0或1; f和g各自为0,1,2或3; h为0,1或2; a + b + = 3; d + e = 3; f + g + h = 3; i + j + k = 1; X为F或Cl; 条件是当a和d均为3时，则i为1，f为0,1或2，g为0,1或3; 当g为2时，f为1; 当c为1时，f为3，k为0; 当j为1时，则c为1; 当b和e都为1时，i为1，可用作氟化材料的溶剂和分散剂。 此外，化合物1-溴-1,1,2,3,3,3-六氟异丙醚和1,2-二氯-1,1,3,3,3-五氟异丙基甲基化合物可用作吸入麻醉剂。

    Anionic fluorochemical surfactants, process of coating and treated polymeric shapes
    2.
    发明授权
    Anionic fluorochemical surfactants, process of coating and treated polymeric shapes 失效
    阴离子含氟表面活性剂，涂层和处理聚合物形状的工艺

    公开(公告)号：US4208466A

    公开(公告)日：1980-06-17

    申请号：US942993

    申请日：1978-09-18

    申请人： Alex J. Szur

    发明人： Alex J. Szur

    IPC分类号： C07C41/03 ,  C07C43/13 ,  D06M13/165 ,  B32B27/34

    CPC分类号： C07C41/03 ,  D06M13/165 ,  Y10S516/03

    摘要： 6-Hydroxyhexyl perfluoroisopropyl ether is prepared by reaction of hexafluoroacetone and potassium fluoride to obtain an alcoholate which is then reacted with 1-chloro-6-hexanol. One mole of the ether may be reacted with about 1 mole to about 20 moles of ethylene oxide to produce a hydroxyethyl ether. One mole of 2,2,3,4,4,4-hexafluorobutanol may be reacted with from about 1 to about 5 moles of propylene oxide to produce a hydroxypropyl ether. One mole of hexafluorobutanol may also be reacted with about 1 to about 5 moles of propylene oxide and then about 1 mole to about 20 moles of ethylene oxide to produce a hydroxyethyl ether. The hydroxyhexyl ether, hydroxylpropyl ether and both hydroxyethyl ethers may be sulfated to produce anionic surfactants which are useful as antistatic agents and lubricants for polymeric shapes such as nylon films and filaments.

    摘要翻译： 通过六氟丙酮和氟化钾的反应制备6-羟基己基全氟异丙醚，得到醇化物，然后与1-氯-6-己醇反应。 1摩尔的醚可以与约1摩尔至约20摩尔的环氧乙烷反应以产生羟乙基醚。 1摩尔的2,2,3,4,4,4-六氟丁醇可以与约1至约5摩尔的环氧丙烷反应以产生羟丙基醚。 1摩尔六氟丁醇也可以与约1至约5摩尔环氧丙烷反应，然后与约1摩尔至约20摩尔环氧乙烷反应，生成羟乙基醚。 羟基己基醚，羟丙基醚和两羟乙基醚可以被硫酸化以产生可用作抗静电剂的阴离子表面活性剂和用于聚合物形状的润滑剂，例如尼龙膜和长丝。

    Anionic fluorochemical surfactants
    4.
    发明授权
    Anionic fluorochemical surfactants 失效
    阴离子含氟表面活性剂

    公开(公告)号：US4140709A

    公开(公告)日：1979-02-20

    申请号：US560719

    申请日：1975-03-21

    申请人： Alex J. Szur

    发明人： Alex J. Szur

    IPC分类号： C07C41/03 ,  C07C43/13 ,  D06M13/165 ,  C07C141/02

    CPC分类号： C07C43/137 ,  C07C41/03 ,  C07C41/16 ,  D06M13/165

    摘要： 6-Hydroxyhexyl perfluoroisopropyl ether is prepared by reaction of hexafluoroacetone and potassium fluoride to obtain an alcoholate which is then reacted with 1-chloro-6-hexanol. One mole of the ether may be reacted with about 1 mole to about 20 moles of ethylene oxide to produce a hydroxyethyl ether. One mole of 2,2,3,4,4,4-hexafluorobutanol may be reacted with from about 1 to about 5 moles of propylene oxide to produce a hydroxypropyl ether. One mole of hexafluorobutanol may also be reacted with about 1 to about 5 moles of propylene oxide and then about 1 mole to about 20 moles of ethylene oxide to produce a hydroxyethyl ether. The hydroxyhexyl ether, hydroxylpropyl ether and both hydroxyethyl ethers may be sulfated to produce anionic surfactants which are useful as antistatic agents and lubricants for polymeric shapes such as nylon films and filaments.

    摘要翻译： 通过六氟丙酮和氟化钾的反应制备6-羟基己基全氟异丙醚，得到醇化物，然后与1-氯-6-己醇反应。 1摩尔的醚可以与约1摩尔至约20摩尔的环氧乙烷反应以产生羟乙基醚。 1摩尔的2,2,3,4,4,4-六氟丁醇可以与约1至约5摩尔的环氧丙烷反应以产生羟丙基醚。 1摩尔六氟丁醇也可以与约1至约5摩尔环氧丙烷反应，然后与约1摩尔至约20摩尔环氧乙烷反应，生成羟乙基醚。 羟基己基醚，羟丙基醚和两羟乙基醚可以被硫酸化以产生可用作抗静电剂的阴离子表面活性剂和用于聚合物形状的润滑剂，例如尼龙膜和长丝。

    Cationic fluorochemical surfactants
    5.
    发明授权
    Cationic fluorochemical surfactants 失效
    阳离子含氟表面活性剂

    公开(公告)号：US4049668A

    公开(公告)日：1977-09-20

    申请号：US560697

    申请日：1975-03-21

    申请人： Alex J. Szur

    发明人： Alex J. Szur

    IPC分类号： B01F17/00 ,  C07C59/06 ,  C07C291/04 ,  C07D213/20

    CPC分类号： C07D213/20 ,  B01F17/0042 ,  C07C291/04 ,  C07C59/06 ,  Y10S524/913

    摘要： Cationic fluorochemical surfactants useful as antistatic agents and lubricants for polymeric shapes are prepared from 2,2,3,4,4,4-hexafluorobutanol or perfluorobutyric acid. Hexafluorobutanol is reacted with bromoundecanoic acid to obtain a bromoester which is then reacted with pyridine to obtain a cationic surfactant. Perfluorobutyric acid is esterified with methanol to obtain methyl perfluorobutyrate which is then reacted with dimethylaminopropylamine to obtain an amino-amide which is then reacted with hydrogen peroxide to obtain the N-oxide derivative which is neutralized with glycolic acid to obtain a cationic surfactant, a salt of the N-oxide derivative.

    摘要翻译： 用作抗静电剂的阳离子含氟表面活性剂和聚合物形状的润滑剂由2,2,3,4,4,4-六氟丁醇或全氟丁酸制备。 六氟丁醇与溴十一烷酸反应得到溴酯，然后与吡啶反应得到阳离子表面活性剂。 全氟丁酸用甲醇酯化，得到全氟丁酸甲酯，然后与二甲基氨基丙胺反应得到氨基酰胺，然后与过氧化氢反应得到N-乙氧基化物中和的N-氧化物衍生物，得到阳离子表面活性剂，盐 的N-氧化物衍生物。