Method and Device for Gas Purification by Means of Partial Condensation, and Method for Operating the Device
    81.
    发明申请
    Method and Device for Gas Purification by Means of Partial Condensation, and Method for Operating the Device 有权
    通过部分冷凝进行气体净化的方法和装置,以及操作装置的方法

    公开(公告)号:US20110030421A1

    公开(公告)日:2011-02-10

    申请号:US12514231

    申请日:2007-10-29

    CPC classification number: B01D53/002 B01D5/0015 B01D7/02 F28D7/0066 F28D7/1607

    Abstract: The subject matter of the invention is a method for purifying a foreign-substance-laden gas flow of the foreign substance, with the gas flow being conducted through a heat exchanger and being placed in thermal contact with a cooling medium in order to freeze and/or condense the foreign substance out, wherein the purification takes place in only one tube heat exchanger, through the interior space of which the gas flow is conducted from a first end region to a second end region, and here, is cooled by means of contact with a first group of tubes which are traversed by the coolant, and in that the gas flow, in the second end region, is directly deflected again and is conducted back through the interior space of the heat exchanger to the first end region through a second group of tubes while undergoing an exchange of heat with the gas flow flowing into the interior space. A corresponding device has a heat exchanger having at least two groups of tubes which run through an interior space of the heat exchanger from a first end region to a second end region of the heat exchanger, with it being possible for the gas flow to traverse the interior space of the heat exchanger from a gas flow inlet at the first end region to the second end region, and with a first group of the tubes being part of a substantially closed cooling medium circuit, and a second group of the tubes for recirculating the gas flow from the second end region of the heat exchanger being connected to a purified gas outlet in the first end region. In order to further reduce the operating temperature in the second end region, it is possible for additional cooling medium to be injected into the cooling medium circuit upstream of said second end region. It is even possible for the injection to take place by means of an injector, which then replaces a pump and cooler.

    Abstract translation: 本发明的主题是一种用于净化异物的异物载气的方法,其中气流通过热交换器传导并与冷却介质热接触以冷冻和/ 或将外来物质冷凝出去,其中纯化仅在一个管式热交换器中进行,其内部空间从第一端部区域传导到第二端部区域,并且这里通过接触来冷却 具有由冷却剂穿过的第一组管,并且在第二端区域中的气流再次被直接偏转,并且通过第二端部区域的热交换器的内部空间被引导回第一端部区域 同时与流入内部空间的气流进行热交换。 相应的装置具有热交换器,该换热器具有至少两组管,该组由热交换器的内部空间从热交换器的第一端部区域延伸到第二端部区域,气体流可以横穿 所述热交换器的内部空间从所述第一端部区域处的气体流入口到所述第二端部区域,并且所述第一组管是基本上封闭的冷却介质回路的一部分,以及用于再循环所述第二组管 来自热交换器的第二端区域的气流与第一端部区域中的净化气体出口连接。 为了进一步降低第二端区域的工作温度,另外的冷却介质可以在所述第二端部区域上游的冷却介质回路中被注入。 甚至可以通过注射器进行注射,然后注射器代替泵和冷却器。

    Adjustable path sublimator system and related method of use
    83.
    发明申请
    Adjustable path sublimator system and related method of use 审中-公开
    可调式升华器系统及相关使用方法

    公开(公告)号:US20060263279A1

    公开(公告)日:2006-11-23

    申请号:US11416504

    申请日:2006-04-27

    CPC classification number: B01D7/00 B01D7/02

    Abstract: A sublimator device is designed where the distance between the sublimation surface and the bottom of the device to be adjusted depending on the amount of substance in the bottom of the device and the rate of sublimation without stopping the process. The device has a threaded connector on the top that allows the condenser to be advanced or receded without stopping the sublimation process. Different embodiments of the sublimator device are disclosed and indications for the use of these devices during the sublimation process are discussed.

    Abstract translation: 设计升华装置,其中升华表面和装置的底部之间的距离将根据装置底部物质的量和升华速率而调整,而不停止该过程。 该设备在顶部具有螺纹连接器,允许冷凝器前进或后退,而不停止升华过程。 公开了升华装置的不同实施例,并且讨论了在升华过程中使用这些装置的指示。

    Apparatus for subliming or condensing a water-containing fluid in a closed space

    公开(公告)号:US06658851B2

    公开(公告)日:2003-12-09

    申请号:US10168191

    申请日:2002-10-21

    Abstract: An apparatus for subliming or condensing a water-containing fluid, which apparatus is provided with a tubular holder (1) having a longitudinal direction and at east one tube (2) extending in that longitudinal direction at least within the holder (1), wherein the holder is provided with at least one inlet (5) and at least one outlet (6), there being further provided at least one supply (3) and at least one discharge (4), which are in communication with the interior of the at least one tube (2), which on one side extends through a wall of the holder an is sealingly secured therein an don the other side within the holder terminates with a free end, closed with respect to the interior of the holder, which free end is guided so as to be slidable in longitudinal direction, by guide means which are located at a distance from the wall in which the tube is scalingly secured.

    Apparatus for subliming or condensing a water-containing fluid in a closed space
    85.
    发明申请
    Apparatus for subliming or condensing a water-containing fluid in a closed space 有权
    用于在封闭空间中升华或冷凝含水流体的装置

    公开(公告)号:US20030097842A1

    公开(公告)日:2003-05-29

    申请号:US10168191

    申请日:2002-10-21

    Abstract: An apparatus for subliming or condensing a water-containing fluid, which apparatus is provided with a tubular holder (1) having a longitudinal direction and at east one tube (2) extending in that longitudinal direction at least within the holder (1), wherein the holder is provided with at least one inlet (5) and at least one outlet (6), there being further provided at least one supply (3) and at least one discharge (4), which are in communication with the interior of the at least one tube (2), which on one side extends through a wall of the holder an is sealingly secured therein an don the other side within the holder terminates with a free end, closed with respect to the interior of the holder, which free end is guided so as to be slidable in longitudinal direction, by guide means which are located at a distance from the wall in which the tube is scalingly secured.

    Abstract translation: 一种用于升华或冷凝含水流体的装置,该装置设置有具有纵向方向的管状保持器(1)和至少在所述保持器(1)内沿所述纵向方向延伸的东部一个管(2),其中 所述保持器设置有至少一个入口(5)和至少一个出口(6),所述至少一个出口(6)还设置有至少一个供应源(3)和至少一个排出口(4) 至少一个管(2),其一侧延伸穿过保持器的壁,密封地固定在其中,托架内的另一侧终止于自由端,相对于保持器的内部封闭,自由端 通过引导装置引导端部被引导以沿纵向方向滑动,所述引导装置位于距管壁成一定距离的壁处。

    Cryogenic condensation system
    86.
    发明授权
    Cryogenic condensation system 有权
    低温冷凝系统

    公开(公告)号:US06505472B1

    公开(公告)日:2003-01-14

    申请号:US09931901

    申请日:2001-08-20

    Inventor: Alan Cheng Simon Ho

    CPC classification number: F28F9/0265 B01D7/02 B01D8/00 B01D53/002 B01D53/265

    Abstract: A method and condenser apparatus for cleaning a gas of condensable vapor employing a cryogenic liquid which is caused to boil evenly along the condenser length and wherein the gas flow through the condenser is in the downward direction in evenly divided flows countercurrently to the flow of boiled cryogen.

    Abstract translation: 一种用于使用低温液体清洗可冷凝蒸气的气体的方法和冷凝器装置,该低温液体沿着冷凝器长度均匀地沸腾,并且其中通过冷凝器的气体流在向下的方向上以与沸腾的冷冻剂流逆流的均匀分流 。

    Freeze-thaw air dryer
    87.
    发明授权
    Freeze-thaw air dryer 失效
    冻融空气干燥机

    公开(公告)号:US5119640A

    公开(公告)日:1992-06-09

    申请号:US602412

    申请日:1990-10-22

    CPC classification number: F26B21/086 B01D53/265 B01D7/02 F25B21/04

    Abstract: A freeze-thaw air dryer utilizes a heat pump to remove moisture from air by cooling the air to below the freezing point of water, causing the water to pass directly from the vapor state to the solid state and thereby to be removed from the flow of air. The vapor frozen on the cold surfaces is periodically thawed by either turning off or reversing the heat pump, and the condensate and thawed ice are automatically drained out of the device without interruption of the airflow. The geometry of the cold surfaces and the generally centripetal airflow path are designed expressly to cause a buildup of ice without impairing efficiency or blocking the airflow.

    Abstract translation: 冷冻融化空气干燥机利用热泵通过将空气冷却至低于冰点的水分来除去空气中的水分,导致水直接从蒸汽状态通过至固体状态,从而从 空气。 通过关闭或反转热泵,在冷表面上冷冻的蒸汽被周期性地解冻,并且冷凝物和解冻的冰被自动地排出设备而不会中断气流。 冷表面和一般向心气流路径的几何形状被明确地设计成导致冰的积聚而不损害效率或阻挡气流。

    Process and apparatus for fractional desublimation of vapor-phase solids
from gas-vapor mixtures
    88.
    发明授权
    Process and apparatus for fractional desublimation of vapor-phase solids from gas-vapor mixtures 失效
    气相混合物气相固体分馏的工艺和装置

    公开(公告)号:US4773923A

    公开(公告)日:1988-09-27

    申请号:US13184

    申请日:1987-02-09

    Applicant: Helmut Scharf

    Inventor: Helmut Scharf

    CPC classification number: B01D7/02 Y10S62/91

    Abstract: For the non-clogging, fractional desublimation of vapor-phase solids contained in a gas-vapor mixture, the gas-vapor mixture, exiting at high velocity from a nozzle, is mixed with a cooling gas, likewise exiting at high velocity from another nozzle. The gas-vapor mixture and the cooling gas flow toward each other, the axes of the two gaseous streams being a straight line. Fractional desublimation of the solids is attained by adjustment of flows leading to the regulation of the temperature and residence time of the cooled gas-vapor mixture. This desublimation system is capable of degrees of efficiency and solids purities higher than 99%.

    Abstract translation: 对于非阻塞,包含在气体 - 蒸汽混合物中的气相固体的分级抽出,从喷嘴以高速离开的气体 - 蒸气混合物与冷却气体混合,同样从高速度从另一个喷嘴 。 气体 - 蒸气混合物和冷却气体朝向彼此流动,两个气流的轴线是直线。 通过调节导致调节冷却的气体 - 蒸气混合物的温度和停留时间的流量来获得固体的分数分布。 这种desublimation系统的效率和固体纯度达99%以上。

    Vacuum freezing process with multiple phase transformations of low
pressure vapor
    89.
    发明授权
    Vacuum freezing process with multiple phase transformations of low pressure vapor 失效
    真空冷冻过程与低压蒸汽的多相转变

    公开(公告)号:US4420318A

    公开(公告)日:1983-12-13

    申请号:US315858

    申请日:1981-10-28

    CPC classification number: C02F1/22 B01D7/02 B01D9/04 C02F2103/08

    Abstract: The Vacuum Freezing Vapor Desublimation Desublimate Vaporization Process (denoted as VDDV Process) is an improved vacuum freezing process that is useful in separating solvent from a solution that contains one or more non-volatile solutes. It can be used in desalination of sea water and brackish water, renovation of waste water, and concentration of aqueous and non-aqueous solutions.Referring to sea water desalination, the process comprises the following steps: (a) feed sea water is flash vaporized under a reduced pressure to thereby form a first low pressure water vapor (3.5 torr) and an ice-brine slush; (b) the first low pressure water vapor is cooled without pressurization to form a mass of desublimate; (c) the ice-brine slush is separated into a mass of purified ice and a concentrated brine; (d) the desublimate is melted and vaporized to form a second low pressure water vapor that is at a pressure higher than the triple point pressure of water (4.58 torr); (d) the second low pressure water vapor is brought in contact with the purified ice to thereby condense the vapor and melt the ice. Both the condensate and the melt become product fresh water. The characteristic feature of the process is that a low pressure vapor is pressurized from a first pressure that is lower than the triple point pressure to a second pressure that is higher than the triple point pressure by first desubliming the vapor and then melting and vaporizing the desublimate. The need of a low pressure compressor has been eliminated.

    Abstract translation: 蒸发蒸发蒸发蒸发方法(表示为“VDDV工艺”)是一种改进的真空冷冻方法,可用于从含有一种或多种非挥发性溶质的溶液中分离溶剂。 可用于海水淡化,咸水淡化,废水净化,水溶液和非水溶液浓缩。 关于海水淡化,该方法包括以下步骤:(a)进料海水在减压下闪蒸,从而形成第一低压水蒸汽(3.5托)和冰盐水; (b)第一低压水蒸汽在不加压的情况下被冷却以形成大量的稀释物; (c)将冰盐水冰浆分离成大量纯净的冰和浓缩的盐水; (d)稀释物被熔化和蒸发以形成处于高于水的三重点压力(4.58托)的压力的第二低压水蒸汽; (d)使第二低压水蒸汽与纯净的冰接触,从而使蒸气冷凝并融化。 冷凝物和熔体均成为产品淡水。 该方法的特征在于,将低压蒸汽从低于三重点压力的第一压力加压到高于三重点压力的第二压力,首先使蒸气冷凝,然后将该稀释物 。 已经消除了对低压压缩机的需求。

    Process for the recovery of vaporized sublimates from gas streams
    90.
    发明授权
    Process for the recovery of vaporized sublimates from gas streams 失效
    从气流中回收蒸发的升华物的方法

    公开(公告)号:US4391617A

    公开(公告)日:1983-07-05

    申请号:US216934

    申请日:1980-12-16

    Applicant: Peter F. Way

    Inventor: Peter F. Way

    CPC classification number: C07C51/573 B01D7/02 C07C51/43

    Abstract: Sublimate vapors are recovered from gases in a heat-pipe exchanger system, operating alternately in a condensing mode and a melting mode, for condensing on the exchanger tube surfaces such sublimable vapors as phthalic anhydride, maleic anhydride, naphthalene and fatty acids from gases containing said vapors thereof during the condensing mode, and for melting out the accumulated sublimate solids during the melting mode. Multiple, such as two or more units may be used to provide continuous processing of the sublimate vapor-laden gas stream, at least one operating in the condensing mode while simultaneously at least one may operate in the alternate mode. The cooling of opposite heat-pipe exchanger ends to recover sublimate solids is economical and efficient with ambient air, either alone or with some warm recycle exchanger air to adjust the cooling temperature; and the heating to melt out the accumulated solids is effective with heated air or hot waste gases, such as combustion gases, preferably by incineration of residual sublimate tail gas from which the sublimate was condensed, or other hot combustion gases, but other sources of heating the air or gases may be optionally substituted. Important advantage is present in superior heat exchange efficiency using the heat-pipe exchanger for this service, in the ease of switching from heating to cooling of such exchangers for alternate operation in both condensing and melting modes, in the elimination of intermediary heat transfer media and the separate auxiliary equipment required for the heating and cooling cycles, in the utilization of waste heat from combustion gases, and in the great economy for sublimate storage tank vent condensers through elimination of both cooling water and steam requirements.

    Abstract translation: 升华蒸气从热交换器系统中的气体中回收,其以冷凝模式和熔融模式交替运行,用于在交换器管表面上冷凝,如来自含有所述蒸气的气体的邻苯二甲酸酐,马来酸酐,萘和脂肪酸的可升华蒸气 在冷凝模式期间其蒸气,并且在熔化模式期间熔化累积的升华固体。 可以使用多个,例如两个或更多个单元来提供升华的含气气流的连续处理,至少一个以冷凝模式工作,同时至少一个可以在交替模式下操作。 相对的热管交换器末端的冷却以恢复升华的固体,对于环境空气来说是经济和有效的,单独使用或与一些温暖的循环交换器空气调节冷却温度; 并且通过加热的空气或热的废气(例如燃烧气体),优选地通过焚烧升华物被冷凝的残余的升华尾气,或其它热的燃烧气体,但是其它的加热源 空气或气体可以任选地被取代。 在使用热交换器进行这种使用的优点的热交换效率方面存在重要的优点,即在冷凝和熔融模式中交替操作的这种交换器的加热到冷却的切换容易,消除中间传热介质和 加热和冷却循环所需的单独的辅助设备,利用来自燃烧气体的废热,以及通过消除冷却水和蒸汽要求,在经济上用于升华式储罐排气冷凝器。

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