Sulfo-fluorination of synthetic resins
    71.
    发明授权
    Sulfo-fluorination of synthetic resins 失效
    合成树脂的磺化氟化

    公开(公告)号:US3940520A

    公开(公告)日:1976-02-24

    申请号:US443460

    申请日:1974-02-19

    CPC classification number: D06M11/09 D06M11/11 D06M11/34

    Abstract: This invention relates to a process for improving the water wicking and moisture transport properties of synthetic resins, e.g., fiber form polyamides, polyesters, polyolefins, and polyacrylonitriles, which comprises sulfofluorinating said resins in a self-activating gaseous reaction medium containing from about 0.1-20% by volume elemental fluorine, 0.1-50% by volume of sulfur dioxide, 0-21% by volume oxygen, and the balance inert for providing from 1 .times. 10.sup.-.sup.9 to 1 .times. 10.sup.-.sup.3 milligrams fluorine and sulfur per square centimeter of resin surface.

    Abstract translation: 本发明涉及一种改善合成树脂(例如纤维形式聚酰胺,聚酯,聚烯烃和聚丙烯腈)的吸水性和湿气输送性能的方法,该方法包括在含有约0.1-约0.1重量份的自激活气态反应介质中使所述树脂磺化氟化, 20体积%的元素氟,0.1〜50体积%的二氧化硫,0〜21体积%的氧,余量为1×10 -9〜1×10 -3毫克的氟和 硫磺每平方厘米的树脂表面。

    Process for treating acrylic fibers to obtain carbonizable and graphitizable substrates
    72.
    发明授权
    Process for treating acrylic fibers to obtain carbonizable and graphitizable substrates 失效
    处理丙烯腈纤维以获得可碳化和可再生基材的方法

    公开(公告)号:US3817700A

    公开(公告)日:1974-06-18

    申请号:US24384072

    申请日:1972-04-13

    Applicant: MONSANTO CO

    Inventor: MENIKHEIM V

    CPC classification number: D01F9/225 D06M11/34

    Abstract: A PROCESS IS PROVIDED FOR PRODUCING A HEAT-STABILIZED CHAR OR SUBSTRATE FROM ACRYLIC FIBERS WHICH CAN BE CONVERTED INTO HIGH QUALITY CARBON OR GRAPHITE FIBERS. THE FIBERS ARE FIRST TREATED IN A POLYOL SOLUTION CONTAINING A BASIC NITRILE POLYMERIZATION CATALYST FOLLOWED BY AN AIROXIDATION AT TEMPERATURES OF 270*C. AND ABOVE. THE PREOXIDATION TREATMENT DRASTICALLY REDUCES THE TIME NORMALLY REQUIRED FOR EFFECTING THE NECESSARY OXIDATION. THE CARBONIZABLE OR GRAPHITIZABLE SUBSTRATED OBTAINED YIELD CARBON AND GRAPHITE FIBERS OF IMPROVED PROPERTIES.

    ACRYLIC FIBER STABILIZATION CATALYZED BY Co(II) AND Ce(III) CATIONS
    74.
    发明授权
    ACRYLIC FIBER STABILIZATION CATALYZED BY Co(II) AND Ce(III) CATIONS 失效
    由Co(II)和Ce(III)催化的丙烯腈纤维稳定剂

    公开(公告)号:US3656882A

    公开(公告)日:1972-04-18

    申请号:US3656882D

    申请日:1970-03-09

    Applicant: CELANESE CORP

    Inventor: RIGGS JOHN PERRY

    CPC classification number: D01F9/225 D06M11/34

    Abstract: A process is provided wherein the thermal stabilization of an acrylic fibrous material is accelerated by heating in an oxygencontaining atmosphere in the presence of a catalytic quantity of Co(II) and Ce(III) metallic cations which have been found capable of promoting the oxidative cross-linking of adjoining polymer molecules. The resulting stabilized fibrous materials are nonburning when subjected to an ordinary match flame, and may be utilized as fire resistant textile fibers, or optionally converted to a carbonized fibrous material by heating in an inert atmosphere at a more highly elevated temperature.

    Abstract translation: 提供了一种方法,其中通过在催化量的Co(II)和Ce(III)金属阳离子存在下在含氧气氛中加热来加速丙烯酸类纤维材料的热稳定性,已经发现能够促进 相邻聚合物分子的氧化交联。 所得到的稳定的纤维材料在经受普通匹配火焰时不燃,可用作耐火织物纤维,或通过在更高温度下在惰性气氛中加热任选地转化为碳化纤维材料。

    Process for oxidizing and carbonizing acrylic fibers
    75.
    发明授权
    Process for oxidizing and carbonizing acrylic fibers 失效
    氧化和碳化丙烯纤维的方法

    公开(公告)号:US3556729A

    公开(公告)日:1971-01-19

    申请号:US3556729D

    申请日:1969-03-24

    Applicant: MONSANTO CO

    CPC classification number: D06M11/34 D01F9/225 Y10S264/19

    Abstract: THIS INVENTION PROVIDES A PROCESS FOR PREOXIDIZING ACRYLIC FIBERS WHICH CAN BE CONVERTED INTO CARBON OR GRAPHITE FIBERS OF HIGH STRENGTH AND MODULUS. THE PROCESS INVOLVES FIRST HEATING THE FIBER, WHILE UNDER TENSION, TO A TEMPERATURE BELOW 250*C. IN AN ATMOSPHERE OF OXYGEN AND BROMINE FOR A TIME SUFFICIENT TO FORM A PERMEABLE SHEATH AROUND THE FIBER. THE FIBER IS NEXT HEATED IN AN OXYGEN ATMOSPHERE AT A TEMPERATURE ABOVE 250*C. FOR A TIME SUFFICIENT TO ALLOW COMPLETE PERMEATION OF OXYGEN THROUGHOUT THE CORE OF THE FIBER. THE OXIDIZED FIBERS ARE USEFUL FOR THE CONSTRUCTION OF FIREPROOF FABRICS AND MAY ALSO BE CARBONIZED OR GRAPHITIZED BY HEATING IN AN INERT ATMOSPHERE AT THE APPROPRIATE TEMPERATURES.

Patent Agency Ranking