Preparing method of high-modulus-low-shrinkage activated PET industrial yarn

    公开(公告)号:US11174575B2

    公开(公告)日:2021-11-16

    申请号:US17051442

    申请日:2019-10-28

    摘要: A type of high-modulus-low-shrinkage activated PET industrial yarn and preparing method thereof are disclosed. The preparing method is to manufacture filament from a modified polyester, which is the product of the esterification and the successive polycondensation reactions of evenly mixed terephthalic acid, ethylene glycol and tert-butyl branched heptanediol, through a series of processes composed of viscosity enhancing by solid state polycondensation, melting, metering, extruding, cooling, oiling, stretching, heat setting, relaxation heat-treating, oiling with activation oil, winding and pre-activation treatment. The relaxation heat-treating indicates passing the modified polyester yarns through a space with a certain temperature within 200-220° C. under a proper relaxation state; and the proper relaxation state means a 3.0-5.0% of overfeed for the winding. The improvement of activator efficiency by importing the tert-butyl branched diol into the polyester, together with the synergistic effect of heat setting temperature and high winding overfeed rate, will reduce the fiber thermal shrinkage.

    Method for Preparing Microporous PVA Fiber

    公开(公告)号:US20210214860A1

    公开(公告)日:2021-07-15

    申请号:US17144103

    申请日:2021-01-07

    发明人: Juhong Zeng

    摘要: The present application discloses a method for preparing microporous PVA fiber comprising the following steps: Step 1: preparing spinning solution, calcium hydroxide solution, and sodium sulfate solution; Step 2: cooling the spinning solution to 40-60° C., and adding a foaming agent thereto to provide the PVA spinning stock solution; Step 3: spinning into the sodium sulfate solution so that the fiber containing the reaction product of the foaming agent and the mirabilite is dehydrated to provide a primary PVA fiber; Step 4: reacting the fiber with the calcium hydroxide solution to provide a secondary fiber; Step 5: foaming and pore forming; and Step 6: cleaning and drying to provide the final product of microporous PVA fiber.

    Fibers with modified cross sectional profile

    公开(公告)号:US10557217B2

    公开(公告)日:2020-02-11

    申请号:US15578593

    申请日:2016-06-02

    摘要: A method for making a fiber reinforcement with variations in transverse cross section is disclosed. The method includes forming a fiber comprising polymeric material and exposing the fiber to a heat treatment, such that at least a portion of the polymeric material at or near said surface of said fiber is at or above the melting point temperature and substantially all of the polymeric material at or near the core is below the melting point temperature. The method further includes cooling the fiber to a temperature below the melting point temperature.

    Method to manufacture microfibers and microcapillaries

    公开(公告)号:US10450677B2

    公开(公告)日:2019-10-22

    申请号:US16250963

    申请日:2019-01-17

    IPC分类号: D01F6/96 D01D10/02 D01D5/24

    摘要: A parylene microcapillary is manufactured by drawing a polyethylene carbonate (PEC) fiber from a 0° C. solution of 12-25% PEC in chloroform to create a PEC fiber that has a constant diameter over several centimeters. Parylene is deposited in a chamber over the PEC fiber, and then the coated PEC fiber is heated above 180° C. This heating melts and decomposes the PEC fiber such that it self-expels from the coating, leaving a microcapillary. The self-expulsion allows for meters-long lengths of microcapillaries. Alternatively, a serpentine fiber channel of PEC is created by deposition, photolithography, and etching within a sandwich of parylene. It is heated above 180° C. to expel the PEC leaving a hollow channel within a mass of parylene. The resulting microcapillaries may have residues of cyclic ethylene carbonate remaining from the decomposed PEC.