Abstract:
A container assembly for use in a high-pressure press having a central pressure cell and a method of sealing a central pressure cell. The container assembly includes a container that receives a sample to be pressed, and a gasket distinct from the container, the gasket meeting the container at an interface. The container and the gasket are dimensioned to locate the interface within the central pressure cell.
Abstract:
A press, an automated loading system for a press and related methods are provided including a loading system having a first assembly configured to carry a reaction cell to an anvil of a press base and a second assembly configured to assist in positioning and orientating the reaction cell on the anvil. In one embodiment, the first assembly may include a trolley displaceable along a guide member to carry the reaction cell to the anvil. The first and second assemblies may each include guide members that are displaceable relative to the anvil that are configured to position the reaction cell at a desired location and orientation on the anvil. In one embodiment, each of the guide members include arms that engage distinct sides of a cubic reaction cell. A clearing mechanism may also be incorporated to clear the surface of the anvil during operation of the system.
Abstract:
Methods for forming cutting elements comprising polycrystalline materials, methods for forming polycrystalline compacts for cutting elements of a drilling tool, methods for forming polycrystalline diamond compacts, and resulting polycrystalline compacts and cutting elements are disclosed. Grains of a hard material are introduced to a press and subjected to a high-pressure, high-temperature (HPHT) process to sinter the grains. The system conditions (i.e., temperature and pressure) are then adjusted past a phase or state change point, after which, at least one of the system conditions is held during an anneal stage before the system conditions are adjusted to final levels. The resulting compacts and cutting elements may therefore include inter-granularly bonded hard material grains with a more stable microstructure (e.g., less stressed microstructure) than a polycrystalline compact and cutting element formed without an anneal stage during the HPHT process.
Abstract:
A high-pressure high-temperature cell including two or more thermal insulation layers is described. A high-pressure high-temperature cell including a current path through a thermal insulation layer, the current path being electrically connected to a heating element and having an indirect path through the thermal insulation layer, is also described. High-pressure high-temperature press systems including the foregoing the high-pressure high-temperature cells alone or in combination are also disclosed.
Abstract:
A cartridge assembly for connection to the frame of a high pressure, high temperature press, comprising a front end. The front end may comprise a back up with a conical portion intermediate and coaxial with an anvil and a piston. The anvil may comprise a proximal end in contact with the back-up and a distal end being adapted to form part of a pressurized chamber within the frame. The back-up may comprise a truncated cylinder comprising a first and second interface that are joined by a peripheral cylindrical wall. The cylindrical wall may also comprise a portion extending normally from the periphery of the first interface to a net concave portion of the cylindrical wall. The net concave portion may extend from the normal portion of the cylindrical wall to the periphery of the second interface which abuts the anvil.
Abstract:
A cartridge assembly for connection to the frame of a high pressure, high temperature press, comprising a front end. The front end may comprise a back up with a conical portion intermediate and coaxial with an anvil and a piston. The anvil may comprise a proximal end in contact with the back-up and a distal end being adapted to form part of a pressurized chamber within the frame. The back-up may comprise a truncated cylinder comprising a first and second interface that are joined by a peripheral cylindrical wall. The cylindrical wall may also comprise a portion extending normally from the periphery of the first interface to a net concave portion of the cylindrical wall. The net concave portion may extend from the normal portion of the cylindrical wall to the periphery of the second interface which abuts the anvil.
Abstract:
The present invention includes a hydraulic cartridge and unitary frame connection for a high pressure high temperature press apparatus with the hydraulic cartridge having a cylindrical base and truncated hollow conical section The truncated section has an external threadform with a taper between about 2.650 and 5.650 inches per foot. The unitary frame having an opening with an internal threadform extending axially substantially between an outer surface and an inner reaction chamber defined by the unitary frame and the internal threadform being threadedly mated with the external threadform of the hydraulic cartridge such that a load is substantially equally distributed across the external threadform.
Abstract:
High pressure synthesis of various crystals such as diamond, cBN and the like can be carried out using reaction assemblies suitable for use in methods such as temperature gradient methods. The reaction assembly can be oriented substantially perpendicular to gravity during application of high pressure. Orienting the reaction assembly in this manner can avoid detrimental effects of gravity on the molten catalyst, e.g., convection, hence increasing available volumes for growing high quality crystals. Multiple reaction assemblies can be oriented in series or parallel, each reaction assembly having one or more growth cells suitable for growth of high quality crystals. Additionally, various high pressure apparatuses can be used. A split die design allows for particularly effective results and control of temperature and growth conditions for individual crystals.