Preparation of tertiary amines
    24.
    发明授权
    Preparation of tertiary amines 失效
    叔胺的制备

    公开(公告)号:US5925793A

    公开(公告)日:1999-07-20

    申请号:US117316

    申请日:1993-09-07

    申请人: Herbert Mueller

    发明人: Herbert Mueller

    CPC分类号: C07C209/16

    摘要: A process for the preparation of dialkylamines of the general formula I, ##STR1## in which R.sup.1, R.sup.2, and R.sup.3 denote C.sub.1 -C.sub.12 alkyl, by the reaction of a dialkylamine of the general formula II ##STR2## in which R.sup.1 and R.sup.2 denote C.sub.1 -C.sub.12 alkyl, with alcohols R.sup.3 --OH in the presence of a (copper chromite/alkaline-earth metal chromite)-containing hydrogenation/dehydrogenation catalyst, in which the reaction is carried out in the liquid phase over a fixed bed catalyst in the presence of the water formed during the reaction at temperatures ranging from 180.degree. to 210.degree. C. and pressures ranging from 40 to 120 bar.

    摘要翻译: 通过使通式II的二烷基胺(其中R 1和R 2表示C 1 -C 12烷基)与其中R 1,R 2和R 3表示C 1 -C 12烷基的二烷基胺反应制备通式I的二烷基胺的方法与 在含有亚铬酸铜/碱土金属铬铁酸盐的氢化/脱氢催化剂存在下,在固相床催化剂的存在下,在水中形成的水​​中进行反应,得到醇R3-OH 反应温度范围为180°至210°C,压力范围为40至120巴。

    Method and apparatus for cleaning the dents of a weaving reed
    25.
    发明授权
    Method and apparatus for cleaning the dents of a weaving reed 失效
    用于清洁编织芦苇的凹痕的方法和装置

    公开(公告)号:US5634981A

    公开(公告)日:1997-06-03

    申请号:US386809

    申请日:1995-02-08

    CPC分类号: D03J1/002 D03D47/278

    摘要: Avivage deposits on and between the dents of a reed, especially in an air weaving loom, are removed by heating at least a portion of the reed dents in the vicinity of the weft insertion channel to a temperature sufficient to melt the avivage which can then be discharged from the reed dents and the spaces between the reed dents by dripping downwardly, for example, into a collecting trough.

    摘要翻译: 通过将纬纱插入通道附近的至少一部分芦苇浆加热到足以熔化空气的温度来除去芦苇,特别是空气编织织机的凹陷之间和之间的空气沉积物, 例如,通过向下滴落从芦苇凹陷和芦苇凹陷之间的空间排出到收集槽中。

    Loom method and apparatus for avoiding beat up markings in a fabric
    27.
    发明授权
    Loom method and apparatus for avoiding beat up markings in a fabric 失效
    用于避免织物中的殴打标记的织机方法和装置

    公开(公告)号:US5404916A

    公开(公告)日:1995-04-11

    申请号:US123646

    申请日:1993-09-17

    摘要: When a faulty weft thread must be removed after it has been bound into the fabric and beat-up, it is necessary to perform a so-called reverse weaving operation following the stopping of the normal weaving operation in response to a stop signal signifying that a faulty weft thread has been detected. For this purpose the loom main shaft and the heald drive shaft are rotated for a number of rotational degrees in the same direction in which these shafts are rotated just prior to the stopping of a weaving operation in response to the above mentioned signal. Next, the drive between the main shaft and the heald shaft is interrupted. Next, the main shaft and thus also the reed shaft and with it the reed, are rotated back within a predetermined angular range between two successive reed beat-up motions. During this time the heald shaft is rotated back, preferably to the so-called detection point with a higher r.p.m., or rather with a higher angular speed than the main shaft. This function is accomplished by an auxiliary step-up transmission gear between the main shaft and the heald shaft. The auxiliary gear is bypassed during normal operation when there is no weft fault and it is connected in series during the operation for removing of a faulty weft thread.

    摘要翻译: 当纬纱线已经被束缚在织物中并被打倒之后,必须去除有缺陷的纬纱,因此在停止正常编织操作之后,需要执行所谓的反向编织操作,该停止信号表示 已检测到纬纱错误。 为此,织机主轴和综丝驱动轴在刚好在响应于上述信号的织造操作停止之前沿相同的方向旋转多个旋转度。 接下来,主轴和综框之间的驱动被中断。 接下来,主轴以及簧片轴与簧片一起在两个连续的簧片打纬运动之间的预定角度范围内回转。 在此期间,综丝回转,优选地以较高的r.p.m.或更高的角速度比主轴更靠近所谓的检测点。 该功能由主轴和综框之间的辅助升压传动齿轮实现。 在没有纬纱故障的情况下,辅助齿轮在正常运行期间被旁路,并且在拆卸故障纬纱的操作期间串联连接。

    Thermoplastic polyurethane elastomers with a low degree of organic
carbon migration
    28.
    发明授权
    Thermoplastic polyurethane elastomers with a low degree of organic carbon migration 失效
    具有低有机碳迁移量的热塑性聚氨酯弹性体

    公开(公告)号:US5247049A

    公开(公告)日:1993-09-21

    申请号:US952373

    申请日:1992-09-28

    CPC分类号: C08G18/4854 C08G18/6674

    摘要: The invention relates to thermoplastic polyurethane elastomers obtainable by reaction ofa) unmodified and/or modified organic polyisocyanates, preferably 4,4'-diisocyanatodiphenylmethane, withb) polyoxybutylene glycols and/or polyoxybutylene/polyoxyalkylene glycols with a molecular weight of from 150 to 1800 and a content of crown ethers, preferably those of the formula (--CH.sub.2 CH.sub.2 CH.sub.2 CH.sub.2 O--).sub.m, where m is from 3 to 6, not exceeding 0.06% of the total weight andc) chain extenders with a molecular weight of from 60 to 400, preferably 1,4-butanediol,to a process for the preparation thereof and to the use thereof for producing molded articles and sheets for use in the medical or hygiene sector and in the foodstuffs sector.

    摘要翻译: 本发明涉及通过a)未改性和/或改性的有机多异氰酸酯,优选4,4'-二异氰酸根合二苯基甲烷与b)聚氧丁烯二醇和/或分子量为150至1800的聚氧丁烯/聚氧亚烷基二醇反应而获得的热塑性聚氨酯弹性体 和冠醚的含量,优选式(-CH2CH2CH2CH2O-)m的那些,其中m为3至6,不超过总重量的0.06%,和c)分子量为60至400的扩链剂, 优选1,4-丁二醇,其制备方法及其用于生产用于医疗或卫生部门和食品部门的模塑制品和片材的用途。

    Preparation of high purity polymers of tetrahydrofuran
    29.
    发明授权
    Preparation of high purity polymers of tetrahydrofuran 失效
    四氢呋喃的高纯度聚合物的制备

    公开(公告)号:US5112943A

    公开(公告)日:1992-05-12

    申请号:US591061

    申请日:1990-10-01

    申请人: Herbert Mueller

    发明人: Herbert Mueller

    摘要: A process is described for the preparation of high purity polymers or copolymers obtained by cationic polymerization of tetrahydrofuran and, if desired, alkylene oxide, in which hydrogen having a bubble diameter of less than 50 .mu.m is passed into the polymers in the presence of a hydrogenation catalyst.

    摘要翻译: 描述了制备通过四氢呋喃的阳离子聚合获得的高纯度聚合物或共聚物的方法,并且如果需要,在其中存在下将气泡直径小于50μm的氢气进​​入聚合物的环氧烷烃 氢化催化剂。

    Preparation of 1,2,4-butanetriol
    30.
    发明授权
    Preparation of 1,2,4-butanetriol 失效
    制备1,2,4-丁三醇

    公开(公告)号:US4973769A

    公开(公告)日:1990-11-27

    申请号:US306309

    申请日:1989-02-03

    IPC分类号: C07C29/149 C07C31/22

    CPC分类号: C07C31/22 C07C29/149

    摘要: 1,2,4-Butanetriol is prepared by catalytic hydrogenation of malic esters over a copper-containing catalyst by passing the esters over the fixed-bed catalyst at from 130.degree. to 190.degree. C. under hydrogen partial pressures of from 100 to 300 bar while substantially avoiding the formation of a gas phase.

    摘要翻译: 通过在130至190℃的氢分压下将酯超过固定床催化剂,在含铜催化剂上催化氢化苹果酸酯,制备1,2,4-丁三醇。 同时基本上避免气相的形成。