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公开(公告)号：US20080269352A1
公开(公告)日：2008-10-30
申请号：US12097064
申请日：2006-12-05
申请人： Jurgen Falkowski , Markus Dierker , Michael Neuss , Karl Heinz Schmid , Stephan Wurkert , Lars Zander
发明人： Jurgen Falkowski , Markus Dierker , Michael Neuss , Karl Heinz Schmid , Stephan Wurkert , Lars Zander
摘要： A process is provided for the production of linear saturated alkanes from one or more primary alcohols, wherein the carbon chain of the one or more primary alcohols has one carbon atom more than the alkane, including conducting reductive dehydroxymethylation of one or more primary fatty alcohols containing 8 to 24 carbon atoms, at a temperature ranging from 100 to 300° C. and pressures from 1 to 250 bar in the presence of hydrogen and a catalyst, and removing water formed during the reaction.
摘要翻译： 提供了一种从一种或多种伯醇生产线性饱和烷烃的方法，其中一种或多种伯醇的碳链比烷烃多一个碳原子，包括进行一种或多种含有主要脂肪醇的一级脂肪醇的还原性脱羟甲基化 8至24个碳原子，在100至300℃的温度和1至250巴的压力下，在氢气和催化剂存在下，以及除去反应期间形成的水。
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12.发明授权Alkyl and/or alkenyloligoglycoside preparations having reduced magnesium salt concentrations 有权具有降低的镁盐浓度的烷基和/或烯醇降糖苷制剂公开(公告)号：US07045494B2
公开(公告)日：2006-05-16
申请号：US10481841
申请日：2002-06-12
摘要： A process for making an alkyl and/or alkenyl oligoglycoside preparation having a magnesium salt concentration of less than about 10 ppm involving the steps of: (a) providing an alkyl and/or alkenyl oligoglycoside preparation having an active substance content of from about 10 to 70% by weight, based on the weight of the preparation; (b) providing an acid component; (c) adjusting the pH of the alkyl and/or alkenyl oligoglycoside preparation to from about 4 to 9.5 by combining the acid component with the alkyl and/or alkenyl oligoglycoside preparation to form a pH-modified alkyl and/or alkenyl oligoglycoside preparation; (d) providing a column charged with an ion exchange resin; and (e) purifying the pH-modified alkyl and/or alkenyl oligoglycoside preparation by passing it through the column of step (d) at a viscosity of from about 20 to 6,000 mPas, and at a temperature of from about 20 to 90° C. to form the alkyl and/or alkenyl oligoglycoside preparation having a magnesium salt concentration of less than about 10 ppm.
摘要翻译： 制备镁盐浓度小于约10ppm的烷基和/或烯基低聚糖苷制剂的方法，包括以下步骤：（a）提供活性物质含量为约10至10重量％的烷基和/或烯基低聚糖苷制剂， 70重量％，基于制剂的重量; （b）提供酸组分; （c）通过将酸组分与烷基和/或链烯基低聚糖苷制剂组合以形成pH-改性的烷基和/或烯基低聚糖苷制剂，将烷基和/或链烯基低聚糖苷制剂的pH调节至约4至9.5; （d）提供带有离子交换树脂的柱; 和（e）通过使pH值为约20至6,000mPa·s的粘度和约20至90℃的温度通过步骤（d）的柱来纯化pH-改性的烷基和/或烯基低聚糖苷制剂 形成镁盐浓度小于约10ppm的烷基和/或烯基低聚糖苷制剂。
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13.发明授权Hydroxy mixed ethers having a high degree of ethoxylation, compositions containing the same and anti-foam uses therefor 有权具有高乙氧基化度的羟基混合醚，含有相同的组合物和抗泡沫用途公开(公告)号：US06921744B2
公开(公告)日：2005-07-26
申请号：US10470898
申请日：2002-02-01
CPC分类号： C11D3/0026 , C08G65/2609 , C11D1/721 , C11D1/825 , C11D3/2068
摘要： Hydroxy mixed ethers of the general formula (I): R1O[CH2CH2O]xCH2CH(OH)R2 (I) wherein R1 represents a linear or branched, alkyl or alkenyl group having from 4 to 22 carbon atoms; R2 represents a linear or branched, alkyl or alkenyl group having from 2 to 22 carbon atoms; and x represents a number of from 40 to 80, are described along with compositions containing such hydroxy mixed ethers in conjunction with other surfactants. Also described are various anti-foaming uses for such ethers and compositions containing the same.
摘要翻译： 通式（I）的羟基混合醚：<？in-line-formula description =“In-line formula”end =“lead”？> R 1 O [CH 2] （O）2 CH 2 OH（OH）R 2（I）其中R 1表示具有4至22个碳原子的直链或支链烷基或链烯基; R 2表示具有2至22个碳原子的直链或支链烷基或链烯基; 和x表示40至80的数量，以及含有这种羟基混合醚与其它表面活性剂结合的组合物。 还描述了用于这种醚和包含其的组合物的各种消泡用途。
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公开(公告)号：US20080207933A1
公开(公告)日：2008-08-28
申请号：US12116355
申请日：2008-05-07
IPC分类号： C07C237/00
CPC分类号： A61Q19/10 , A61K8/42 , A61K8/442 , A61Q5/00 , A61Q5/006 , A61Q5/02 , A61Q15/00 , C07C233/36 , C07C233/38 , C11D1/62
摘要： Quaternary surfactants of the formula (I), wherein R1CO is a linear or branched, saturated or unsaturated, optionally hydroxy-functionalized acyl radical having 6 to 22 carbon atoms and 0, 1, 2 or 3 double bonds, R2 is a CH2COOH radical, an alkyl radical having 1 to 4 carbon atoms, a CH2CH2OH or a CH2CH2OCH2CH2OH group, and X is halide, alkyl sulfate, alkyl carbonate or alkyl phosphate, are useful as surfactants in cosmetic and pharmaceutical preparations. Aqueous solutions above 50% by weight of the surfactants are flowable and pumpable.
摘要翻译： 式（I）的季铵盐表面活性剂，其中R 1 CO是具有6至22个碳原子和0,1,2或3个碳原子的直链或支链，饱和或不饱和的任选羟基官能化的酰基 双键，R 2是CH 2 COOH基团，具有1至4个碳原子的烷基，CH 2 CH 2 CH 2， 2 OH或CH 2 CH 2 OCH 2 CH 2 OH基，X是 卤化物，烷基硫酸盐，碳酸烷基酯或磷酸烷基酯可用作化妆品和药物制剂中的表面活性剂。 高于50重量％的表面活性剂的水溶液是可流动的和可泵送的。
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公开(公告)号：US07145001B1
公开(公告)日：2006-12-05
申请号：US10111863
申请日：2000-10-18
申请人： Manfred Weuthen , Karl Heinz Schmid
发明人： Manfred Weuthen , Karl Heinz Schmid
摘要： A process for making solid sugar surfactants involving: (a) providing a glycose component; (b) acetalizing the glycose component with a fatty alcohol to form a technical mixture containing excess fatty alcohol and alkyl and/or alkenyl oligoglycoside; and (c) contacting the technical mixture with an extractant to form a solid phase containing the extractant, a predominant part of alkyl and/or alkenyl oligoglycoside and a small amount of fatty alcohol, and a liquid phase containing a predominant part of the fatty alcohol.
摘要翻译： 制备固体糖表面活性剂的方法，其包括：（a）提供糖苷组分; （b）用脂肪醇使糖分成分缩醛以形成含有过量脂肪醇和烷基和/或烯基低聚糖苷的技术混合物; 和（c）使技术混合物与萃取剂接触以形成含有萃取剂的固相，主要部分为烷基和/或烯基低聚糖苷和少量脂肪醇，以及含有主要部分脂肪醇的液相 。
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公开(公告)号：US06846796B2
公开(公告)日：2005-01-25
申请号：US10257700
申请日：2001-04-06
申请人： Karl Heinz Schmid
发明人： Karl Heinz Schmid
摘要： Surfactant granules are made by the process comprising the steps of (1) mixing an aqueous nonionic surfactant paste and an aqueous solution of an organic polymeric carrier; (2) simultaneously granulating and drying the mixture from step (1) in a fluidized bed to form a granulated nonionic surfactant. The surfactant granules are dust-free, flowable, storage-stable, show no tendency toward clumping and are readily soluble in cold water.
摘要翻译： 通过包括以下步骤的方法制备表面活性剂颗粒：（1）将非水性非离子表面活性剂浆料和有机聚合物载体的水溶液混合; （2）在流化床中同时对来自步骤（1）的混合物进行造粒和干燥以形成颗粒状非离子表面活性剂。 表面活性剂颗粒是无尘的，可流动的，储存稳定的，没有显示出结块的倾向，并且易溶于冷水。
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公开(公告)号：US06610752B1
公开(公告)日：2003-08-26
申请号：US09685117
申请日：2000-10-10
IPC分类号： B01D1904
CPC分类号： C11D17/0034 , C11D3/0026 , C11D3/373 , C11D11/0082
摘要： Defoamer granules containing support materials and silicones for solid laundry detergent, dishwashing detergent and cleaning compositions, obtainable by applying silicones in the form of aqueous emulsions to an added intermediate product of support materials and simultaneously drying and granulating the products in a fluidized bed, with the proviso that at least 85% by weight of the particles have a mean diameter below 1.5 mm, are described.
摘要翻译： 消泡剂颗粒含有用于固体衣物洗涤剂，洗碗洗涤剂和清洁组合物的载体材料和硅氧烷，可通过将水乳液形式的硅氧烷施加到添加的载体材料的中间产物并同时在流化床中干燥和造粒产物， 条件是至少85重量％的颗粒的平均直径低于1.5mm。
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公开(公告)号：US09839797B2
公开(公告)日：2017-12-12
申请号：US12097064
申请日：2006-12-05
申请人： Jürgen Falkowski , Markus Dierker , Michael Neuβ , Karl Heinz Schmid , Stephan Würkert , Lars Zander
发明人： Jürgen Falkowski , Markus Dierker , Michael Neuβ , Karl Heinz Schmid , Stephan Würkert , Lars Zander
摘要： A process is provided for the production of linear saturated alkanes from one or more primary alcohols, wherein the carbon chain of the one or more primary alcohols has one carbon atom more than the alkane, including conducting reductive dehydroxymethylation of one or more primary fatty alcohols containing 8 to 24 carbon atoms, at a temperature ranging from 100 to 300° C. and pressures from 1 to 250 bar in the presence of hydrogen and a catalyst, and removing water formed during the reaction.
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公开(公告)号：US08715629B2
公开(公告)日：2014-05-06
申请号：US10553165
申请日：2004-04-07
摘要： The disclosed invention relates to a cosmetic composition containing at least one branched oligo-α-olefin, characterized in that the side chains at one branch point at least are ethyl, propyl or longer branched alkyl chains, the branched oligo-α-olefin being obtainable by oligomerization of a) at least one branched α-olefin containing 5 to 18 carbon atoms, b) at least one linear α-olefin containing 4 to 10 carbon atoms, c) a mixture of a branched α-olefin containing 4 to 18 carbon atoms and a linear α-olefin containing 3 to 18 carbon atoms or d) a mixture of various branched α-olefins containing 4 to 18 carbon atoms and linear α-olefins containing 3 to 18 carbon atoms in the presence of a catalyst selected from the group consisting of organic acids, cationic ion exchangers, silica gels, layer silicates, inorganic acids or Lewis-acid-based catalysts. The specific oligo-α-olefins are distinguished by particularly high spreading power, by an improved sensory impression of the final cosmetic formulation and by particularly good stability in antiperspirant/deodorant formulations.
摘要翻译： 所公开的发明涉及含有至少一种支链低聚-α-烯烃的化妆品组合物，其特征在于，一个分支点的侧链至少为乙基，丙基或更长支链的烷基链，所述支链低聚-α-烯烃可获得 a）至少一种含有5至18个碳原子的支链α-烯烃的低聚，b）至少一种含有4-10个碳原子的直链α-烯烃，c）含有4-18个碳原子的支链α-烯烃的混合物 原子和含有3至18个碳原子的直链α-烯烃或d）含有4至18个碳原子的各种支链α-烯烃和含有3至18个碳原子的直链α-烯烃的混合物在催化剂存在下，选自 由有机酸，阳离子交换剂，二氧化硅凝胶，层状硅酸盐，无机酸或路易斯酸类催化剂组成的组。 具体的低聚-α-烯烃通过特别高的铺展力，通过改进的最终化妆品制剂的感官印象以及在止汗/除臭剂制剂中特别好的稳定性来区分。
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公开(公告)号：US07807614B2
公开(公告)日：2010-10-05
申请号：US12116355
申请日：2008-05-07
CPC分类号： A61Q19/10 , A61K8/42 , A61K8/442 , A61Q5/00 , A61Q5/006 , A61Q5/02 , A61Q15/00 , C07C233/36 , C07C233/38 , C11D1/62
摘要： Quaternary surfactants of the formula (I), wherein R1CO is a linear or branched, saturated or unsaturated, optionally hydroxy-functionalized acyl radical having 6 to 22 carbon atoms and 0, 1, 2 or 3 double bonds, R2 is a CH2COOH radical, an alkyl radical having 1 to 4 carbon atoms, a CH2CH2OH or a CH2CH2OCH2CH2OH group, and X is halide, alkyl sulfate, alkyl carbonate or alkyl phosphate, are useful as surfactants in cosmetic and pharmaceutical preparations. Aqueous solutions above 50% by weight of the surfactants are flowable and pumpable.
摘要翻译： 式（I）的季铵盐表面活性剂，其中R 1 CO是具有6至22个碳原子和0,1,2或3个双键的直链或支链，饱和或不饱和的任选的羟基官能化酰基，R 2是CH 2 COOH基团， 具有1至4个碳原子的烷基，CH 2 CH 2 OH或CH 2 CH 2 OCH 2 CH 2 OH基团，X为卤化物，烷基硫酸盐，碳酸烷基酯或磷酸烷基酯，可用作化妆品和药物制剂中的表面活性剂。 高于50重量％的表面活性剂的水溶液是可流动的和可泵送的。
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