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公开(公告)号：US4728682A
公开(公告)日：1988-03-01
申请号：US781615
申请日：1985-09-30
申请人： Josephine Covino , Marian E. Hills
发明人： Josephine Covino , Marian E. Hills
CPC分类号： C01B17/20 , C01F17/00 , C01F17/0037 , C01G9/006 , C01P2002/70
摘要： Metal ternary sulfides of the general formula MM'.sub.2 S.sub.4 are synthesized by introducing stoichiometric amounts of nitrate precursors in concentrated nitric acid and heating to approximate dryness to yield a homogeneous powder mixture. The mixture is then exposed to a gaseous H.sub.2 S atmosphere under controlled conditions to produce the desired sulfide.
摘要翻译： 通过在浓硝酸中引入化学计量的硝酸盐前体并加热至近似干燥以合成粉末混合物，合成通式为MM'2S4的金属三元硫化物。 然后将混合物在受控条件下暴露于气态H 2 S气氛中以产生所需的硫化物。
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公开(公告)号：US5035756A
公开(公告)日：1991-07-30
申请号：US296162
申请日：1989-01-10
申请人： Josephine Covino
发明人： Josephine Covino
CPC分类号： C06B33/00 , F42B39/20 , Y10S149/114
摘要： A thermite mixture with a low autoignition temperature for venting ordnancease sidewalls during fuel fire, having increased density, tensile strength and elasticity.
摘要翻译： 具有低自燃温度的铝热混合物，用于在燃料火灾期间排出弹药壳侧壁，具有增加的密度，拉伸强度和弹性。
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公开(公告)号：US4637864A
公开(公告)日：1987-01-20
申请号：US846788
申请日：1986-03-28
IPC分类号： C25B1/00
CPC分类号： C25B1/00
摘要： This invention comprises a method of synthesizing ternary phosphide compos of the general formula M(II)M(IV)P.sub.2 by fused salt electrolysis in which a melt powder mixture containing phosphorus compounds is introduced into an electrolytic apparatus containing a liquid group II metal cathode and a group IV metal or semiconductor source. Electrolysis occurs under controlled conditions in which oxygen is excluded as an impurity to produce the desired ternary phosphide compounds.
摘要翻译： 本发明包括通过熔盐电解合成通式M（II）M（Ⅳ）P2的三元磷化合物的方法，其中将含有磷化合物的熔融混合物引入包含液体II族金属阴极的电解装置中， IV族金属或半导体源。 电解发生在控制条件下，其中排除氧作为杂质以产生所需的三元磷化合物。
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公开(公告)号：USH626H
公开(公告)日：1989-04-04
申请号：US892967
申请日：1986-08-04
申请人： Josephine Covino
发明人： Josephine Covino
IPC分类号： C04B35/111 , C04B35/19
CPC分类号： C04B35/19 , C04B35/111
摘要： A method of synthesizing ceramic oxides using the Sol-Gel process to control particle size distribution, crystal structure and to achieve the selective incorporation of transition metals within a ceramic oxide matrix in order to produce tailored oxides with specific particle morphology and near zero expansion optical ceramics.
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公开(公告)号：US6039929A
公开(公告)日：2000-03-21
申请号：US990261
申请日：1997-12-15
申请人： Ilzoo Lee , Josephine Covino
发明人： Ilzoo Lee , Josephine Covino
CPC分类号： C01B33/26
摘要： A process for producing monoclinic celsian comprising the steps of forming a mixture of an alkoxide of silica, an alkoxide of aluminum, and a salt of barium; adding a catalyst of a fluorine containing compound to the mixture; calcining the catalyzed mixture; and, heat treating the calcined mixture. This process uses a sol-gel process to progressively increase the amount of monoclinic phase in relation to the hexagonal celsian. Additionally, a process for producing monoclinic strontium aluminosilicate is disclosed.
摘要翻译： 一种生产单斜晶体的方法，包括以下步骤：形成二氧化硅的醇盐，铝的醇盐和钡盐的混合物; 向混合物中加入含氟化合物的催化剂; 煅烧催化混合物; 并对煅烧的混合物进行热处理。 该方法使用溶胶 - 凝胶法逐渐增加单斜晶相相对于六边形凝胶相的量。 另外，公开了一种生产单斜晶硅酸锶铝硅酸盐的方法。
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