Invention Application
- Patent Title: POLY-LYSINE DERIVATIVE AND ITS USE IN SOLID-BASED COMPOSITIONS
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Application No.: US16612202Application Date: 2018-04-17
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Publication No.: US20210289773A1Publication Date: 2021-09-23
- Inventor: Markus Kalt , Helmut Witteler , Tina Schroeder-Grimonpot , Markus Meise , Hans-Peter Seelmann-Eggebert , Frank Klippel
- Applicant: BASF SE
- Applicant Address: DE Ludwigshafen am Rhein
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen am Rhein
- Priority: EP17170900.9 20170512,EP17192942.5 20170925,EP17209244.7 20171221
- International Application: PCT/EP2018/059702 WO 20180417
- Main IPC: A01N25/10
- IPC: A01N25/10 ; A01N43/54 ; A01N25/14 ; C08G69/10 ; C08G69/04 ; C08G69/48

Abstract:
Described herein is a poly-lysine derivative obtained by a process including heating an aqueous lysine solution to boiling, increasing a temperature of the aqueous lysine solution to a reaction temperature in the range of about 105° C. to about 180° C., and keeping the reaction temperature in the range of about 105° C. to about 180° C. until (i) a melt viscosity of the reaction mixture is in the range of about 350 mPa*s to about 6,500 mPa*s, and (ii) an amine number in the range of about 100 mg KOH/g to about 500 mg KOH/g is achieved. The process also includes adding alkyl-carboxylic acid or alkenyl-carboxylic acid in amounts of 2.5 mol % to 10 mol %, and increasing or keeping the reaction temperature in the range of about 105° C. to about 180° C. until number of free alkyl-carboxylic acid or alkenyl-carboxylic acid is ≤9% by weight.
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