Process for the preparation of mesophase pitches
    2.
    发明授权
    Process for the preparation of mesophase pitches 失效
    制备中间相沥青的方法

    公开(公告)号:US4820401A

    公开(公告)日:1989-04-11

    申请号:US48376

    申请日:1987-05-11

    摘要: A process for the preparation of an excellent mesophase pitch suitable for use as a spinning pitch for the production of high performance carbon fibers is disclosed. The mesophase pitch can satisfy the four remarkable characteristics at the same time, i.e., a softening point of below 320.degree. C. as determined by Mettler method, a mesophase content of above 90% as examined on a polarized microscope, a quinoline insoluble content of less than 20%, and a xylene soluble content of less than 20%. The mesophase pitch is particularly homogeneous and is easily spinnable. The process can be characterized by a preliminary extraction step, a continuous heat treatment step, and an extraction step. In some cases, the preliminary extraction step can be omitted. Graphite fibers having a tensile strength of about 400 Kg/mm.sup.2 and a modulus of elasticity of above 60 ton/mm.sup.2 can be obtained from the mesophase pitch. Further, even carbon fibers prepared at a carbonization temperature of 1000.degree. C. have a tensile strength of about 300 Kg/mm.sup.2.

    Impregnation pitch with improved filterability and process for its
manufacture
    10.
    发明授权
    Impregnation pitch with improved filterability and process for its manufacture 失效
    浸渍沥青具有改进的过滤性能及其制造方法

    公开(公告)号:US4997542A

    公开(公告)日:1991-03-05

    申请号:US170332

    申请日:1988-03-18

    IPC分类号: C10C3/10 C10C1/19 C10C3/02

    CPC分类号: C10C1/19

    摘要: An impregnation pitch having a Kraemer-Sarnow softening point ranging from about 60.degree. C. to 80.degree. C., a content of quinoline-insoluble substances less than or equal to 7% by weight, and a filterability index greater than or equal to 4.5. A process for the manufacture thereof, wherein a tar or a pitch having a Kraemer-Sarnow softening point not exceeding 60.degree. C. and a content of quinoline-insoluble substances below or equal to 7% by weight is subjected to a thermal treatment capable of removing constituents with a molecular mass of below 1,200.

    摘要翻译: 一种浸渍沥青,其克拉美 - 萨尔诺软化点为约60℃至80℃,喹啉不溶物质含量小于或等于7重量%,过滤性指数大于或等于4.5 。 一种其制造方法,其特征在于,具有不超过60℃Kraemer-Sarnow软化点的焦油或沥青和低于或等于7重量%的喹啉不溶物质的含量经受能够 去除分子量低于1200的成分。