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    Method for producing basic metal nitrate
    3.
    发明申请
    Method for producing basic metal nitrate 有权
    碱性金属硝酸盐的生产方法

    公开(公告)号：US20040131529A1

    公开(公告)日：2004-07-08

    申请号：US10468039

    申请日：2004-02-17

    发明人： Shogo Tomiyama ,  Xingxi Zhou

    IPC分类号： C01G003/08

    CPC分类号： C01G3/08 ,  C01G1/08

    摘要： A process in which a basic metal nitrate is obtained in a high yield is provided. A process for producing a basic metal nitrate, which comprises adding an aqueous solution of a metal nitrate or an aqueous solution of a mixture of a metal nitrate and a water-soluble additive and an alkali solution to a reaction vessel in which a reaction solvent whose pH at 20null C. is adjusted to 6 or less is present, and conducting the reaction with stirring.

    摘要翻译： 提供了以高产率获得碱金属硝酸盐的方法。 一种碱金属硝酸盐的制造方法，其特征在于，在反应容器中加入金属硝酸盐水溶液或金属硝酸盐与水溶性添加剂和碱溶液的混合物的水溶液， 在20℃下的pH调节至6以下，搅拌下进行反应。

    Double salt of ammonium nitrate, gas generating agent containing the same and production method thereof
    4.
    发明申请
    Double salt of ammonium nitrate, gas generating agent containing the same and production method thereof 审中-公开
    硝酸铵双盐，含有其的气体发生剂及其制备方法

    公开(公告)号：US20030057398A1

    公开(公告)日：2003-03-27

    申请号：US10145795

    申请日：2002-05-14

    发明人： Tadamasa Harada

    IPC分类号： A01N001/00

    CPC分类号： C06B31/00 ,  C01B21/48 ,  C01G1/08 ,  C01G3/08 ,  C06D5/06

    摘要： An oxidized comprising a double salt represented by the chemical formula: M(NO3)inNH4NO3. M is a metal element forming a nitrate salt usually containing water of crystallization, i is a numerical value corresponding to the valency of the metal element M, and n is a molar number from 1 to 20. Mixing a metal nitrate containing water of crystallization with ammonium nitrate , and, further drying produces the above-mentioned double salt.

    摘要翻译： 氧化的，包含由化学式：M（NO 3）在NH 4 NO 3中表示的双盐。 M是形成通常含有结晶水的硝酸盐的金属元素，i是对应于金属元素M的化合价的数值，n是1至20的摩尔数。将含有结晶水的金属硝酸盐与 硝酸铵，进一步干燥得到上述复盐。

    Process for preparing metal nitrates from the corresponding metals
    6.
    发明授权
    Process for preparing metal nitrates from the corresponding metals 失效
    从相应的金属制备金属硝酸盐的方法

    公开(公告)号：US06468494B2

    公开(公告)日：2002-10-22

    申请号：US09726067

    申请日：2000-11-29

    申请人： Thomas E. Nappier ,  Alex T. Magdics

    发明人： Thomas E. Nappier ,  Alex T. Magdics

    IPC分类号： C01B2148

    CPC分类号： C01G53/00 ,  C01G1/08 ,  C01G51/00 ,  C01G51/006 ,  C01G53/006

    摘要： The invention relates to a process for preparing metal nitrates from the corresponding metal wherein the metal is selected from silver, cadmium, bismuth and the metals of atomic number 24-30. The process comprises (A) providing a reactor containing (a) the metal, (b) nitric acid, and (c) water wherein the initial concentration of the nitric acid in the water in the reactor is from about 50% to about 80% by weight, and the reactor is free of (1) added fuming nitric acid, (2) added chromium compounds when the metal is iron, and (3) added oxygen, and when the metal is nickel the reactor contains less than 500 g/l of any added nickel nitrate hexahydrate, and (B) maintaining the temperature within the reactor at a temperature to facilitate the formation of the metal nitrate and to maintain the produced metal nitrate in the molten state; (C) maintaining the pressure within the reactor at between atmospheric pressure up to about 100 psig; and (D) recovering the metal nitrate from the reactor, provided that when the metal is iron, any recovered iron nitrate is not recycled. The process of the present Invention results in the formation of metal nitrates and more particularly aqueous solutions of metal nitrates containing reduced amounts of ammonium nitrate.

    摘要翻译： 本发明涉及从相应的金属制备金属硝酸盐的方法，其中金属选自银，镉，铋和原子序号为24-30的金属。 该方法包括（A）提供包含（a）金属，（b）硝酸和（c）水的反应器，其中反应器中水中硝酸的初始浓度为约50％至约80％ ，并且反应器不含（1）加入的发烟硝酸，（2）当金属为铁时加入的铬化合物，和（3）加入氧，当金属为镍时，反应器含有小于500g / 的任何添加的硝酸镍六水合物，和（B）将反应器内的温度保持在有助于形成金属硝酸盐并维持所产生的金属硝酸盐处于熔融状态的温度; （C）将反应器内的压力保持在大气压至约100psig之间; 和（D）从反应器中回收金属硝酸盐，条件是当金属为铁时，任何回收的硝酸铁不被再循环。 本发明的方法导致金属硝酸盐的形成，更特别是含有减少量的硝酸铵的金属硝酸盐的水溶液的形成。

    Fixation of nitrogen using silicon oxide catalysts
    7.
    发明授权
    Fixation of nitrogen using silicon oxide catalysts 失效
    使用氧化硅催化剂固氮

    公开(公告)号：US4308246A

    公开(公告)日：1981-12-29

    申请号：US226592

    申请日：1981-01-21

    申请人： Paul Harteck

    发明人： Paul Harteck

    IPC分类号： C01B21/48 ,  C01F11/38 ,  C01G1/08

    CPC分类号： C01B21/48 ,  C01F11/38 ,  C01G1/08

    摘要： A process for the fixation of nitrogen comprising, combining a gaseous nitrogen and oxygen at a total pressure of above 100 atmospheres with a solid oxide which can produce a nitrate, in the presence of an oxide of silicon catalyst for the acceleration of a reaction between nitrogen and oxygen to produce nitrogen oxides, initially heating the combination to a temperature of between 600.degree. C. to 800.degree. C. and below the dissociation pressure of the nitrate to start an exothermic reaction for producing nitrogen oxides from the nitrogen and oxygen and for producing nitrate from the solid oxide and to establish an equilibrium between the nitrogen, oxygen, nitrogen oxides, solid oxide and nitrate. The reacting combination in equilibrium is then cooled and either the nitrate or the nitrogen oxides are removed from the reaction as products.

    摘要翻译： 一种用于固氮的方法，其包括：在硅催化剂氧化物存在下，将总气压为100多个大气压的气态氮和氧气与可产生硝酸盐的固体氧化物混合，以加速氮气之间的反应 和氧气以产生氮氧化物，最初将组合物加热至600℃至800℃的温度并低于硝酸盐的解离压力，以开始从氮气和氧气产生氮氧化物的放热反应并产生 硝酸盐，固体氧化物和氮，氧，氮氧化物，固体氧化物和硝酸盐之间的平衡。 然后将平衡中的反应组合冷却，并将硝酸盐或氮氧化物作为产物从反应中除去。