Sensor technique for black liquor oxidation control
    1.
    发明授权
    Sensor technique for black liquor oxidation control 有权
    用于黑液氧化控制的传感器技术

    公开(公告)号:US08009277B2

    公开(公告)日:2011-08-30

    申请号:US12290122

    申请日:2008-10-27

    IPC分类号: G01N21/01 G01N21/33 D21C7/12

    摘要: A method for determining simultaneously from an oxidized black liquor sample an amount of sulfide, an amount of total dissolved solids, and an amount of effective alkali present in the sample, wherein the sulfide amount, the total dissolved solids amount, and the effective alkali amount are determined by subjecting the sample to attenuated total reflection (ATR) ultraviolet/visible (UV/V) spectroscopy over a wavelength of from about 190 to about 500 nm. Data from analyzing oxidized black liquor samples, and from analyzing one or more black liquor samples which may be subjected to black oxidation, may be used in a black liquor oxidation (BLOX) system for monitoring and/or controlling sulfur emissions from a kraft process.

    摘要翻译: 一种从氧化黑液样品同时测定硫化物的量,总溶解固体的量和样品中存在的有效碱的量的方法,其中硫化物量,总溶解固体量和有效碱量 通过在约190至约500nm的波长下对样品进行衰减全反射(ATR)紫外/可见光(UV / V)光谱测定。 来自分析氧化黑液样品和分析一种或多种可能进行黑色氧化的黑液样品的数据可用于黑液氧化(BLOX)系统中,用于监测和/或控制来自硫酸盐法的硫排放。

    Sensor technique for black liquor oxidation control
    2.
    发明申请
    Sensor technique for black liquor oxidation control 有权
    用于黑液氧化控制的传感器技术

    公开(公告)号:US20090122307A1

    公开(公告)日:2009-05-14

    申请号:US12290122

    申请日:2008-10-27

    IPC分类号: G01J3/00 G01R35/00

    摘要: A method for determining simultaneously from an oxidized black liquor sample an amount of sulfide, an amount of total dissolved solids, and an amount of effective alkali present in the sample, wherein the sulfide amount, the total dissolved solids amount, and the effective alkali amount are determined by subjecting the sample to attenuated total reflection (ATR) ultraviolet/visible (UV/V) spectroscopy over a wavelength of from about 190 to about 500 nm. Data from analyzing oxidized black liquor samples, and from analyzing one or more black liquor samples which may be subjected to black oxidation, may be used in a black liquor oxidation (BLOX) system for monitoring and/or controlling sulfur emissions from a kraft process.

    摘要翻译: 一种从氧化黑液样品同时测定硫化物的量,总溶解固体的量和样品中存在的有效碱的量的方法,其中硫化物量,总溶解固体量和有效碱量 通过在约190至约500nm的波长下对样品进行衰减全反射(ATR)紫外/可见(UV / V)光谱测定。 来自分析氧化黑液样品和分析一种或多种可能进行黑色氧化的黑液样品的数据可用于黑液氧化(BLOX)系统中,用于监测和/或控制来自硫酸盐法的硫排放。

    Method for rapidly determining a pulp kappa number using spectrophotometry
    3.
    发明授权
    Method for rapidly determining a pulp kappa number using spectrophotometry 失效
    使用分光光度法快速测定纸浆卡伯值的方法

    公开(公告)号:US06475339B1

    公开(公告)日:2002-11-05

    申请号:US09586324

    申请日:2000-06-02

    IPC分类号: D21C712

    CPC分类号: D21C3/228

    摘要: A system and method for rapidly determining the pulp kappa number through direct measurement of the potassium permanganate concentration in a pulp-permanganate solution using spectrophotometry. Specifically, the present invention uses strong acidification to carry out the pulp-permanganate oxidation reaction in the pulp-permanganate solution to prevent the precipitation of manganese dioxide (MnO2). Consequently, spectral interference from the precipitated MnO2 is eliminated and the oxidation reaction becomes dominant. The spectral intensity of the oxidation reaction is then analyzed to determine the pulp kappa number.

    摘要翻译: 通过使用分光光度法直接测定高锰酸钾溶液中的高锰酸钾浓度来快速测定纸浆卡伯值的系统和方法。 具体地,本发明使用强酸化在纸浆高锰酸盐溶液中进行纸浆高锰酸盐氧化反应,以防止二氧化锰(MnO 2)的沉淀。 因此,消除了来自沉淀的MnO 2的光谱干扰,氧化反应成为主导的。 然后分析氧化反应的光谱强度以确定纸浆卡伯值。