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公开(公告)号：US4411712A
公开(公告)日：1983-10-25
申请号：US426432
申请日：1982-09-29
申请人： William G. Marancik
发明人： William G. Marancik
CPC分类号： H01L39/2409 , Y10S505/823 , Y10S505/921 , Y10T29/49014
摘要： An improved method for manufacture of multifilamentary superconductors of the A.sub.3 B type having the A-15 crystal structure, such as Nb.sub.3 Sn, is disclosed in which rods or wires of the A material are disposed throughout a matrix consisting of Cu and the B material in substantially elemental form. The matrix is formed by compaction of powders of Cu; powders of the B may be mixed therewith or the B material may be infiltrated into pores between the individual Cu particles after compaction. The resultant composite has A, B and Cu distributed uniformly throughout its volume and can be worked to any desired final shape and size for heat treatment to form the A.sub.3 B material without intermediate annealing steps.
摘要翻译： 公开了一种用于制造具有A-15晶体结构的例如Nb 3 Sn的A3B型多丝超导体的改进方法，其中A材料的棒或线遍布整个由Cu组成的基体和基本上元素的B材料 形成。 该基体通过Cu的粉末的压实而形成; 可以将B的粉末与其混合，或者B物质可能在压实后渗入各个Cu颗粒之间的孔中。 所得的复合材料具有均匀分布在其体积中的A，B和Cu，并且可以加工成任何期望的最终形状和尺寸用于热处理以形成A3B材料，而无需中间退火步骤。
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2.发明授权公开(公告)号：US07089647B2
公开(公告)日：2006-08-15
申请号：US10782408
申请日：2004-02-19
申请人： Robert Hentges , Jeff Parrell , William G. Marancik , Seung Hong
发明人： Robert Hentges , Jeff Parrell , William G. Marancik , Seung Hong
IPC分类号： H01L39/24
CPC分类号： H01L39/2403 , H01L39/2406 , H01L39/2409 , Y10T29/49014 , Y10T29/49117
摘要： A method for increasing the copper to superconductor ratio of a superconductor core wire by forming a copper-based strip about the core wire which at least partially encloses the core wire in contact therewith by deforming the strip longitudinally into a U shape nested about the wire; and soldering the wire and strip in the assembly of step (a) to form a strong mechanical, electrical and thermal bond therebetween.
摘要翻译： 一种用于通过围绕芯线形成铜基条来提高超导体芯线的铜与超导体比的方法，所述铜线条至少部分地包围与其接触的芯线，通过使所述带纵向变形成围绕所述线嵌套的U形; 以及在步骤（a）的组件中焊接所述线材和条带以在它们之间形成强烈的机械，电和热粘合。
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3.发明授权Method for increasing the copper to superconductor ratio in a superconductor wire 有权在超导体线中增加铜与超导体比的方法公开(公告)号：US06932874B2
公开(公告)日：2005-08-23
申请号：US10690850
申请日：2003-10-22
申请人： William G. Marancik , Seung Hong
发明人： William G. Marancik , Seung Hong
CPC分类号： H01L39/2406 , H01L39/2409 , Y10T29/49014
摘要： A method for producing a superconductor having a high copper to superconductor composition (Cu/SC) ratio by cross-sectional area. An assembly is prepared formed of one or more fine filaments of a superconductor composition or of a precursor component for a superconductor alloy composition, which filaments are embedded in a copper-based matrix. The assembly is electroplated with copper to increase the Cu/filament ratio in the resulting product, and thereby increase the said Cu/SC ratio to improve the stability of the final superconductor.
摘要翻译： 一种通过横截面积制造具有高铜 - 超导体组成（Cu / SC）比的超导体的方法。 制备由超导体组合物的一个或多个细长丝或超导体合金组成的前体组分形成的组件，该细丝嵌入铜基基质中。 组件用铜电镀以增加所得产物中的Cu /丝比，从而增加所述Cu / SC比以提高最终超导体的稳定性。
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公开(公告)号：US07562433B2
公开(公告)日：2009-07-21
申请号：US11235705
申请日：2005-09-26
申请人： Seung Hong , William G. Marancik , Jeff Parrell , Michael Field , Kenneth Marken , Youzhu Zhang
发明人： Seung Hong , William G. Marancik , Jeff Parrell , Michael Field , Kenneth Marken , Youzhu Zhang
CPC分类号： B21C37/047 , B21C33/002 , B82Y30/00 , Y10S977/762 , Y10S977/84 , Y10S977/888 , Y10T29/49014 , Y10T29/49801 , Y10T29/49812 , Y10T29/49826 , Y10T29/49885
摘要： A method for fabrication of nanometer scale metal fibers, followed by optional further processing into cables, yarns and textiles composed of the primary nanofibers. A multicomponent composite is first formed by drilling a billet of matrix metal, and inserting rods of the metal desired as nanofibers. Hexed or round rods can also be inserted into a matrix metal can. The diameter of this composite is then reduced by mechanical deformation methods. This composite is then cut to shorter lengths and reinserted into another billet of matrix metal, and again the diameter is reduced by mechanical deformation. This process of large scale metal stacking followed by mechanical deformation is repeated until the desired fiber size scale is reached, the fibers being contained in the matrix metal. After size reduction, the composite metal wires may be further processed into built up configurations, depending on intended application, by stranding, cabling, braiding, weaving, knitting, felting, etc., to form yarns or textiles. After the built up configuration is formed, the matrix metal is removed by chemical etching, leaving a cable, yarn or textile composed of the primary nanofibers.
摘要翻译： 一种用于制造纳米级金属纤维的方法，随后可选地进一步加工成由初级纳米纤维组成的电缆，纱线和纺织品。 首先通过钻取基体金属坯料，并将所需金属棒作为纳米纤维插入，形成多组分复合材料。 六边形或圆形的杆也可插入矩阵金属罐中。 然后通过机械变形方法减小该复合材料的直径。 然后将该复合材料切割成更短的长度并重新插入到另一个基体金属坯料中，再次通过机械变形减小直径。 重复这种大规模金属堆叠的机械变形过程，直到达到所需的纤维尺寸，纤维被包含在基质金属中。 尺寸缩小后，复合金属丝可根据用途，绞合，电缆布线，编织，编织，编织，毡化等进一步加工成内衬构造，以形成纱线或纺织品。 在形成构建构造之后，通过化学蚀刻去除基质金属，留下由初级纳米纤维组成的电缆，纱线或纺织物。
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公开(公告)号：US3958327A
公开(公告)日：1976-05-25
申请号：US465970
申请日：1974-05-01
CPC分类号： H01L39/14 , Y10S505/92 , Y10T29/49014 , Y10T428/12812
摘要： A superconducting compound of the A-15 crystal structure type is obtained in a composite by a high temperature diffusion between a first metallic component and a second metallic component contained in a bronze alloy. Stability is achieved by including in the composite a quantity of high-conductivity normal material. Diffusion of the second metallic component into the normal material with a resultant degradation of conductivity of the normal material is prevented by placing an impervious barrier layer between the bronze alloy and the normal material. In a specific embodiment, the barrier layer takes the form of an annular shell comprising at least two sectors of dissimilar metals, one of which reacts with a component of the bronze alloy to form a layer of said superconducting compound, and the other of which is substantially non-reactive. Thus, a discontinuous superconducting ring is formed on the barrier layer which prevents flux trapping.
摘要翻译： 通过在青铜合金中包含的第一金属组分和第二金属组分之间的高温扩散，在复合材料中获得A-15晶体结构类型的超导化合物。 通过在复合材料中包含一定数量的高导电率普通材料来实现稳定性。 通过在青铜合金和普通材料之间放置不透水的阻挡层来防止第二金属成分扩散到正常材料中，导致正常材料的导电性降低。 在一个具体实施方案中，阻挡层采取环形壳的形式，其包括至少两个异种金属部分，其中之一与青铜合金的组分反应形成一层所述超导化合物，另一个是 基本上无反应性。 因此，在阻挡层上形成不连续的超导环，防止磁通捕获。
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公开(公告)号：US4447946A
公开(公告)日：1984-05-15
申请号：US282832
申请日：1981-07-13
申请人： William G. Marancik
发明人： William G. Marancik
IPC分类号： H01L39/24
CPC分类号： H01L39/2409 , Y10S505/921 , Y10T29/49014
摘要： Nb wire and Sn plated Cu wire and/or Sn plated Cu foil strip are fabricated into a composite that is mechanically worked to form a multifilament superconductor precursor that does not require intermediate anneals and that has required amounts of Sn distributed throughout its cross section for efficient reaction with the Nb filaments.
摘要翻译： Nb线和Sn镀Cu线和/或Sn镀铜箔条被制成复合材料，其被机械加工以形成不需要中间退火的复丝超导体前体，并且其需要量的Sn分布在整个横截面上用于有效 与铌丝反应。
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公开(公告)号：US4101731A
公开(公告)日：1978-07-18
申请号：US716312
申请日：1976-08-20
申请人： William G. Marancik
发明人： William G. Marancik
CPC分类号： H01L39/14 , Y10S505/887 , Y10T29/49014
摘要： A composite multifilament superconducting structure is provided, which includes an elongated substrate-carrying, longitudinally-directed, sputtered discrete filament of an A-15 type intermetallic superconductor. In a preferable procedure, a plurality of spaced, generally longitudinal grooves are formed on the surface of an elongated filamentary substrate, preferably a metal wire. The walls of the grooves on the substrate surface are shaped to undercut the curvilinear surface of the substrate located between two adjacent grooves so that at least some of the wall portions of the grooves are geometrically shadowed during the subsequent sputtering step in which a superconductor is sputtered onto the substrate. In particular, a film of a suitable superconducting intermetallic compound having A-15 crystalline structure, such as Nb.sub.3 Ge, is thereupon sputtered onto the grooved substrate and deposits at the bottom of the grooves and at the surface portions of the substrate between grooves. The shadowed wall portions remain substantially deposit-free so that the resultant spaced deposits extend as distinct lines or bands along the substrate to thereby constitute the superconductive filaments. A plurality of such substrates may, if desired, be consolidated into a further composite structure, by bundling the substrates and passing same through a molten metal. The resultant structure may then be sized to yield as a final product a composite of the substrates bearing the superconducting filaments in a surrounding matrix of the metal.
摘要翻译： 提供了一种复合复丝超导结构，其包括A-15型金属间超导体的细长衬底承载的纵向引导的溅射离散细丝。 在优选的过程中，在细长的丝状基底，优选金属线的表面上形成多个间隔开的大致纵向凹槽。 衬底表面上的凹槽的壁被成形为切割位于两个相邻凹槽之间的基底的曲线表面，使得在随后的溅射步骤期间凹槽的至少一些壁部分被几何遮蔽，其中超导体被溅射 到基板上。 特别地，具有A-15晶体结构的合适的超导金属间化合物如Nb 3 Ge的膜随后溅射到带槽的基底上并沉积在凹槽的底部和凹槽之间的基板的表面部分处。 阴影的壁部分保持基本上无沉积，使得所得到的间隔开的沉积物沿着衬底延伸为不同的线或带，从而构成超导细丝。 如果需要，多个这样的基底可以通过将基底捆扎并通过熔融金属固结成另一个复合结构。 然后可以将所得结构的尺寸设定为产生在金属的周围基质中承载超导细丝的基底的复合物作为最终产品。
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8.发明授权
公开(公告)号：US4073666A
公开(公告)日：1978-02-14
申请号：US721739
申请日：1976-09-09
CPC分类号： H01L39/2409 , Y10S505/821 , Y10S505/919 , Y10S505/92 , Y10S505/921 , Y10T29/49014
摘要： A method and article produced thereby are disclosed wherein the method produces a multi-filament superconductor having an insulation capable of withstanding extended heat treatment. According to the invention, a plurality of superconductor forming rods and a plurality of rods of normally conductive material are packed into a can made of a ductile material such as copper and having its interior lined with a valve metal such as tantalum. This assembly is extruded and drawn to a desired size as is known in the art. The ductile metal exterior layer is then removed to expose the valve metal. The exposed valve metal is thereafter oxidized to form an insulating oxide.
摘要翻译： 公开了一种由此制造的方法和制品，其中该方法产生具有能够承受延长热处理的绝缘体的复丝超导体。 根据本发明，多个超导体形成棒和多个常规导电材料棒被包装在由诸如铜的延性材料制成的罐中，并且其内部衬有诸如钽的阀金属。 如本领域已知的那样，将该组件挤出并拉伸至所需的尺寸。 然后移除延性金属外层以暴露阀金属。 然后暴露的阀金属被氧化以形成绝缘氧化物。
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公开(公告)号：US5534219A
公开(公告)日：1996-07-09
申请号：US249945
申请日：1994-05-27
申请人： William G. Marancik , Seungok Hong , Rouyi Zhou
发明人： William G. Marancik , Seungok Hong , Rouyi Zhou
CPC分类号： H01L39/2409
摘要： A method for producing a multifilamentary superconductor containing niobium-tin (Nb.sub.3 Sn). A fully bonded niobium/copper composite billet is formed having a plurality of longitudinally extending channels which are symmetrically distributed with reference to transverse cross-sections of the billet, each channel being filled with an inert removable filler material. The inert filler material is removed to open the longitudinally extending channels in the billet. Tin or a tin alloy is inserted into the channels, and the niobium/copper composite billet with the inserted tin or tin alloy is cold drawn to the desired final dimensions. The drawn composite is then heated to effect in situ formation of the niobium-tin.
摘要翻译： 一种含有铌锡（Nb3Sn）的复丝超导体的制造方法。 形成完全结合的铌/铜复合坯料，其具有多个纵向延伸的通道，其相对于坯料的横截面对称地分布，每个通道填充有惰性的可移除的填充材料。 去除惰性填充材料以打开坯料中纵向延伸的通道。 将锡或锡合金插入通道中，并将具有插入的锡或锡合金的铌/铜复合钢坯冷拉至所需的最终尺寸。 然后将拉制的复合材料加热以实现铌锡的原位形成。
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10.发明授权
公开(公告)号：US4860431A
公开(公告)日：1989-08-29
申请号：US157402
申请日：1988-02-17
申请人： William G. Marancik , Seung-Ok Hong
发明人： William G. Marancik , Seung-Ok Hong
IPC分类号： H01L39/24
CPC分类号： H01L39/2409 , Y10T29/49014
摘要： The centers of a plurality of copper tubes are filled with an alloy of tin with a minor amount of aluminum and drawn to form Cu-Sn wires which are cabled around a core Nb wire; a plurality of these strands are provided in a copper tube, or a copper foil or finely wound copper wire and drawn to produce a multifilament wire; heat treatment is applied to cause the tin to diffuse and form the intermetalic Nb.sub.3 Sn at the surface of the Nb filaments to produce the ultimate superconducting wire product. The addition of a small quantity of Al to the Sn facilitates processing and improves the final product properties.
摘要翻译： 多个铜管的中心用锡与少量的铝的合金填充并被拉伸以形成连接在芯Nb线周围的Cu-Sn线; 在铜管或铜箔或细卷绕的铜线中设置多个这些线，并被拉制以产生复丝线; 施加热处理使锡在Nb丝表面扩散并形成金属间Nb 3 Sn，以产生最终的超导线产品。 向Sn中添加少量的Al有助于加工并提高最终产品性能。
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