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公开(公告)号：US20230151134A1
公开(公告)日：2023-05-18
申请号：US17995384
申请日：2020-04-03
发明人： Fuguo LI , Yang LIU , Ming JIANG , Chengqun QIN , Shiqiang FANG
IPC分类号： C08F283/06 , B01J19/24 , C08G18/65
CPC分类号： C08F283/06 , B01J19/2465 , C08G18/65 , B01J2219/00105
摘要： A reaction system for preparing polymer polyol and a method for preparing polymer polyol. The reaction system comprises a reactor, a first circulation unit, a second circulation unit, and a flow direction switching unit, wherein the reaction cavity of the reactor is divided into a first reaction chamber and a second reaction chamber by a partition plate, and the top of the partition plate is provided with an overflow port to communicate the first reaction chamber and the second reaction chamber with each other; the first circulation unit enables the material in the first reaction chamber to circulate between the discharge port of the first reaction chamber and the feed port of the first reaction chamber; the second circulation unit enables the material in the second reaction chamber to circulate between the discharge port of the second reaction chamber and the feed port of the second reaction chamber. The polymer polyol prepared by the reaction system has a low-viscosity effect, and by using the polymer polyol prepared by the method, a polyurethane foam having excellent mechanical properties and high hardness can be obtained.
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公开(公告)号：US20220017448A1
公开(公告)日：2022-01-20
申请号：US17294102
申请日：2018-12-26
发明人： Fuguo LI , Yang LIU , Changxun JU , Bin LIU , Chengqun QIN , Xunkun WU , Jing LI , Bing ZHENG , Lunpeng WANG
摘要： A stable dispersant and an application thereof in preparing copolymer polyols, the preparation method for the stable dispersant including the steps of 1) contacting a polyol with a dianhydride compound for reaction so as to prepare an adduct; 2) performing a ring-opening addition reaction on the adduct obtained in step 1) and an epoxy compound to prepare a stable dispersant; the dianhydride compound does not contain a double bond that may copolymerize with an olefinically unsaturated monomer, while the epoxy compound contains a double bond that may copolymerize with an olefinically unsaturated monomer, the polyol is a polyester polyol and/or a polyether polyol, preferably being a polyether polyol. The stable dispersant obtained by means of the described preparation method has a multi-active site anchoring function, and is applied to the synthesis of copolymer polyols to obtain copolymer polyols having relatively uniform particle size.
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3.发明申请公开(公告)号：US20220017682A1
公开(公告)日：2022-01-20
申请号：US17295581
申请日：2018-12-26
发明人： Fuguo LI , Changxun JU , Yang LIU , Chengqun QIN , Bin LIU , Xunkun WU , Jing LI , Ye SUN , Bing ZHENG , Lunpeng WANG
摘要： A macromonomeric stabilizer, a preparation method thereof, a method for preparing a polymeric polyol using same, and the polymeric polyol prepared. Also disclosed are a soft polyurethane foam obtained by foaming a composition of the polymeric polyol prepared and a polyisocyanate, and a molded product comprising the soft polyurethane foam. The preparation method of the macromonomeric stabilizer comprises the following steps: reacting a polyol with a tricarboxylate not comprising a polymerizable ethylenically unsaturated double bond, or a derivative thereof, to form an adduct; and reacting the resulting adduct with an epoxide comprising a polymerizable ethylenically unsaturated double bond. The macromonomeric stabilizer of the present invention has a low viscosity, comprises a plurality of active sites, and can be directly used in subsequent reactions. The preparation method of the macromonomeric stabilizer can be carried out under normal pressure, without the need for end-blocking with ethylene oxide.
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公开(公告)号：US20210355263A1
公开(公告)日：2021-11-18
申请号：US17288834
申请日：2018-12-26
发明人： Fuguo LI , Yang LIU , Changxun JU , Naihua JIANG , Bin LIU , Chengqun QIN , Lunpeng WANG
IPC分类号： C08G18/63 , C08F283/06 , C08G18/76 , C08G18/48 , C08G18/40 , C08G18/32 , C08G18/66 , C08J9/12
摘要： Provided are a modified polyether polyol and the use thereof in polyurethane foam materials. The method for preparing a modified polyether polyol comprises the following steps: 1) reacting a compound A with a polyether polyol, wherein the compound A is an anhydride and/or dicarboxylic acid compound containing a polymerizable double bond, preferably selected from one or two of maleic anhydride and itaconic anhydride, preferably maleic anhydride; and 2) reacting the product obtained in step 1) with an epoxy compound containing a polymerizable double bond in the presence of a catalyst, in order to prepare the modified polyether polyol. The modified polyether polyol obtained by means of the preparation method has more active sites, uses the polymerizable double bond for blocking, is used as a dispersion stabilizer for the synthesis of copolymer polyols, and has the characteristics of a better dispersion stability, filterability and a low viscosity.
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